Рубрики:
MECHANOCHEMICAL SYNTHESIS
MECHANICAL-PROPERTIES
NANOCOMPOSITE POWDER
ALLOYS
NANOCRYSTALLINE
MICROSTRUCTURE
FERROMAGNETS
MECHANOCHEMICAL SYNTHESIS
MECHANICAL-PROPERTIES
NANOCOMPOSITE POWDER
ALLOYS
NANOCRYSTALLINE
MICROSTRUCTURE
FERROMAGNETS
Аннотация: The evolution of the magnetic properties of composite Al2O3/Co(P) particles during ball milling and dynamic compaction is investigated. To prepare starting composite particles, the Al2O3 granules were coated with a Co95P5 shell by electroless plating. The magnetic and structural properties of the composite particles are characterized by scanning electron microscopy, X-ray diffraction, and the use of the Physical Property Measurement System. The use of composite core-shell particles as starting powder for mechanoactivation allows to decrease treatment duration to 1 h and to produce a more homogeneous bulk sample than in the case of the mixture of Co and Al2O3 powders. The magnetic properties of the milled composite particles are correlated with changes in the microstructure. Reduction in grain size of Co during milling leads to an increase of the volume fraction of superparamagnetic particles and to a decrease of the saturation magnetization. The local magnetic anisotropy field depends on the amount of hcp-Co phase in sample. The anisotropy field value decreases from 8.4 kOe to 3.8 kOe with an increase in milling duration up to 75 min. The regimes of dynamic compaction were selected so that the magnetic characteristics-saturation magnetization and coercive field-remained unchanged. (C) 2014 AIP Publishing LLC.
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Держатели документа:
Kirensky Inst Phys SB RAS, Krasnoyarsk, Russia
Krasnoyarsk Inst Railways Transport, Krasnoyarsk, Russia
Inst Sicherheitsforsch & Reaktortech, D-52425 Julich, Germany
Krasnoyarsk Sci Ctr SB RAS, Krasnoyarsk, Russia
Доп.точки доступа:
Denisova, E. A.; Денисова, Елена Александровна; Kuzovnikova, L. A.; Кузовникова, Людмила Александровна; Iskhakov, R. S.; Исхаков, Рауф Садыкович; Bukaemskiy, A. A.; Eremin, E. V.; Еремин, Евгений Владимирович; Nemtsev, I. V.; Немцев, Иван Васильевич; Russian Foundation of Basic Research [13-03-00476-a]