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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Samoshkina Yu. E., Edelman I. S., Chou H., Lin H. -C., Dwivedi G. D., Petrov D. A., Zharkov S. M., Zeer G. M., Molokeev M. S.
Заглавие : Structure and physical properties of hydrogenated (Co + Al)-doped ZnO films: Comparative study with co-doped ZnO films
Место публикации : Mater. Sci. Eng. B. - 2021. - Vol. 264. - Ст.114943. - ISSN 09215107 (ISSN), DOI 10.1016/j.mseb.2020.114943
Примечания : Cited References: 52. - H.C. thanks the Ministry of Science and Technology of Taiwan for financial support [grant number MOST 108-2112-M-110-003]. The scanning electron microscopy investigations were conducted in the SFU Joint Scientific Center supported by Ministry of Science and Higher Education of the Russian Federation [state assignment number FSRZ-2020-0011]. X-ray diffraction data were obtained using analytical equipment of Krasnoyarsk Regional Center of Research Equipment of Federal Research Center “Krasnoyarsk Science Center SB RAS”
Аннотация: (Co + Al)-doped ZnO films have been synthesized by the RF magnetron sputtering. Films of this composition have first been obtained in mixed atmosphere of Ar + H2. High hydrogen concentration of 20–50% has been used together with high enough substrate temperature of 450 °C. The used technological conditions affected the morphology, chemical composition, optical, electric, and magnetic properties of the films to an even more than in the case of Co-doped ZnO films synthesized under the same conditions and studied earlier. The films exhibit ferromagnetic behavior at room temperature with much greater magnetization and magneto-optical activity compared to the Co-doped films. At the same time, the hydrogenated films show an increase in electric conductivity in comparison with samples synthesized in the atmosphere of Ar + O2. The magnetic nature of the hydrogenated films has been associated with the defect-related mechanism.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Ivantsov R. D., Petrov D. A., Ivanova O. S., Edelman I. S., Zharkov S. M., Velikanov D. A., Lin, Chun-Rong
Заглавие : Magnetooptics of nanocomposites based on iron chalcogenide nanoparticles
Коллективы : Asian School-Conference on Physics and Technology of Nanostructured Materials, Азиатская школа-конференция по физике и технологии наноструктурированных материалов
Место публикации : Solid State Phenom. - 2020. - Vol. 312. - P.160-165. - ISSN 1012-0394, DOI 10.4028/www.scientific.net/SSP.312.160. - ISSN 1662-9779
Примечания : Cited References: 13. - The reported study was funded by Russian Foundation for Basic Research, Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund of Science, to the research project: № 19-42-240005 «Features of the electronic structure, magnetic properties and optical excitations in nanocrystals of the multifunctional magnetic chalcogenides Fe3S4 and FeSe», by Joint Research Project of Russian Foundation for Basic Research № 19-52-52002 and Ministry of Science and Technology, Taiwan MOST № 108-2923-M-153-001-MY3 and № 106-2112-M-153-001-MY3.
Аннотация: Morphology, structure, magnetic properties and magnetic circular dichroism (MCD) were studied for the FexSy and FexSey nanoparticles (NPs) synthesized with the polyol mediated and the thermal decomposition processes, correspondingly, at different regimes. For all NPs samples, but Fe3S4, MCD was measured for the first time. It has been shown that in the case of sulfides, the character of the MCD spectrum changes as the NPs phase composition transforms from Fe3S4 to FeS with the synthesis temperature increase. At the same time, the shape of the MCD spectrum is almost independent of the NPs phase in the case of iron selenides.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Пряжников М. И., Минаков А. В., Лямкин А. И., Редькин В. Е., Жарков, Сергей Михайлович, Зеер Г. М.
Заглавие : Экспериментальное исследование коэффициентов переноса водных суспензий наноалмазов
Место публикации : Коллоид. журн. - 2020. - Т. 82, № 6. - С. 725-732. - ISSN 0023-2912, DOI 10.31857/S0023291220060105
Примечания : Библиогр.: 31. - Работа выполнена в рамках государственного задания Министерства науки и высшего образования РФ (проект № FSRZ-2020-0012)
Аннотация: В работе представлены результаты экспериментальных исследований коэффициентов вязкости, теплопроводности, электропроводности и спектров поглощения суспензий ультрадисперсных алмазов. В экспериментах использовали суспензии частиц детонационных наноалмазов УДА-С и УДП-А, а также алмазографитового порошка УДП-АГ. Концентрацию наноалмазов в дистиллированной воде варьировали от 0.5 до 5 мас. %. Показано, что технология очистки порошков алмаза от побочных продуктов синтеза существенно сказывается на физико-химических свойствах водных суспензий этих порошков.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Ivantsov R. D., Petrov D. A., Ivanova O. S., Edelman I. S., Zharkov S. M., Velikanov D. A., Chun-Rong Lin
Заглавие : Magnetooptics of nanocomposites based on iron chalcogenide nanoparticles
Коллективы : Asian School-Conference on Physics and Technology of Nanostructured Materials, Азиатская школа-конференция по физике и технологии наноструктурированных материалов
Место публикации : The Fifth Asian School-Conference on Physics and Technology of Nanostructured Materials: Proceedings. - VLadivostok: Dalnauka Publishing, 2020. - Ст.IV.03.05o. - P.105. - ISBN 978-5-8044-1698-1
Примечания : The reported study was funded by Russian Foundation for Basic Research, Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund of Science, to the research project: № 19-42-240005, by Joint Research Project of Russian Foundation for Basic Research № 19-52-52002 and Ministry of Science and Technology, Taiwan MOST № 108-2923-M-153-001-MY3 and № 106-2112-M-153-001-MY3.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Карпов И. В., Ушаков А. В., Лепешев, Анатолий Александрович, Дёмин В. Г., Федоров Л. Ю., Гончарова Е. А., Зеер Г. М., Жарков, Сергей Михайлович, Абкарян А. К.
Заглавие : Исследование микроструктурных особенностей, фазового состава и магнитных свойств композитов на основе YBCO и добавок несверхпроводящего компонента СuО, полученного в плазме дугового разряда низкого давления
Место публикации : Материаловедение. - 2020. - № 6. - С. 27-32. - ISSN 1684-579X, DOI 10.31044/1684-579X-2020-0-6-27-32
Примечания : Библиогр.: 12
Аннотация: Разработан метод, позволяющий формировать на поверхности дисперсных частиц порошка ВТСП-керамики несверхпроводящего покрытия, состоящего из самоорганизующихся кристаллов CuO, размеры которых менее длины когерентности, т.е. в пределах нескольких десятков нанометров. Показано, что сочетание самоорганизующихся структур в виде «усов» и наночастиц, появляющихся в результате совместного спекания порошков YBa2Cu3O7-x и электродуговых нанопорошков CuO, приводит к существенному увеличению плотности тока и появлению пик-эффекта в области сильных магнитных полей. Очень высокая плотность тока возникает из сложного пиннинга вихрей, где дефекты в виде «усов» обеспечивают большую энергию пиннинга, а наночастицы подавляют крип потока. Регулирование морфологии подобных структур возможно простым изменением концентрации нанодисперсных добавок. Показано, что наиболее оптимальной является добавка CuO в количестве 20% (мас.).A method has been developed, that allows one to form a non-superconducting coating on the surface of dispersed particles of an HTSC ceramic powder consisting of self-organizing CuO crystals whose sizes are less than the coherence length, i.e. within a few tens of nanometers. It was found out that the combination of self-organizing structures in the form of «whiskers» and nanoparticles resulting from the joint sintering of YBa2Cu3O7-x powders and CuO nanocrystals led to a significant increase in current density and the appearance of a peak effect in the region of strong magnetic fields. A very high current density arises from complex pinning of vortices, where defects in the form of «whiskers» provide a large pinning energy, and nanoparticles suppress creep flux. Morphology of such structures can be regulated by a simple change in the concentration of nanodispersed additives. It was determined that the addition of CuO in an amount of 20 wt.% was the most optimal.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Moiseenko E. T., Zharkov S. M., Altunin R. R., Belousov O. V., Solovyov L. A., Yumashev V. V., Volochaev M. N., Zeer G. M.
Заглавие : Peculiarities of Intermetallic Phase Formation in the Process of a Solid State Reaction in (Al/Cu)n Multilayer Thin Films
Место публикации : JOM. - 2021. - Vol. 73, Is. 2. - P.580-588. - ISSN 10474838 (ISSN), DOI 10.1007/s11837-020-04522-9
Примечания : Cited References: 44. - This work was supported by the Russian Science Foundation under Grant #18-13-00080. The electron microscopy investigations were conducted in the SFU Joint Scientific Center whose infrastructure was supported by the State assignment (#FSRZ-2020-0011) of the Ministry of Science and Higher Education of the Russian Federation. The preparation of cross-section samples for TEM investigations was conducted in the Krasnoyarsk Regional Center of Research Equipment of Federal Research Center “Krasnoyarsk Science Center SB RAS”
Аннотация: Phase formation in a solid state reaction in Al/Cu bilayer and multilayer thin films was studied by the methods of in situ transmission electron microscopy, electron diffraction, simultaneous thermal analysis and x-ray diffraction. It was established that the phase formation sequences in the (Al/Cu)n (n = 2, 15) multilayer thin films (θ-Al2Cu → γ1-Al4Cu9 → η2-AlCu) and Al/Cu bilayer thin films (θ-Al2Cu → η2-AlCu → γ1-Al4Cu9) were different. It was assumed that the phase formation process in the thin films was strongly affected by a number of copper/aluminum interfaces due to the changes of aluminum and copper diffusion current.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Жарков, Сергей Михайлович, Алтунин, Роман Русланович, Моисеенко, Евгений Тимофеевич
Заглавие : Твердофазная реакция в тонкопленочной системе Al/Ag
Коллективы : Научный совет по электронной микроскопии РАН, Федеральный научно-исследовательский центр "Кристаллография и фотоника" РАН, Институт проблем технологии микроэлектроники и особочистых материалов РАН, "Курчатовский институт", научно-исследовательский центр, Российская конференция по электронной микроскопии (28; 2020 ; 5-10 сент.; Черноголовка, Московская обл.), Школа молодых ученых (6; 2020 ; 5-10 сент.; Черноголовка, Московская обл.)
Место публикации : XXVIII Российская конференция по электронной микроскопии (РКЭМ-2020): сб. тез. докладов : в 3-х т. - 2020. - Т. 2. - P.228-229. - ISBN 978-5-6045073-2-2, DOI 10.37795/RCEM.2020.82.12.017
Примечания : Библиогр.: 1
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Patrin G. S., Mataev M. M., Seitbekova, K. Zh., Shiyan Ya. G., Yarikov S. A., Zharkov S. M.
Заглавие : Magnetic and resonance properties of the Y0.5Sr0.5Cr0.5Mn0.5O3 polycrystal
Коллективы : Ministry of Education and Science of the Republic of KazakhstanGovernment of the Republic of KazakhstanMinistry of Education and Science of the Republic of Kazakhstan [05130165]
Место публикации : Phys. Solid State. - 2020. - Vol. 62, Is. 8. - P.1350-1354. - ISSN 1063-7834, DOI 10.1134/S1063783420080272. - ISSN 1090-6460(eISSN)
Примечания : Cited References: 20. - This study was supported by the Ministry of Education and Science of the Republic of Kazakhstan, project no. 05130165 and carried out in the framework of the cooperation agreement between the Siberian Federal University and the Kazakh National Women's Teacher Training University
Предметные рубрики: CHROMIUM
TRANSITION
Аннотация: The magnetostatic and magnetic resonance properties of the Y0.5Sr0.5Cr0.5Mn0.5O3 polycrystalline system have been experimentally investigated. The predominance of the intracrystalline ferromagnetic interaction and the antiferromagnetic character of the intercrystallite interaction have been established. The magnetic resonance spectrum in the magnetically ordered region consists of two lines. The high-field line corresponds to the interacting parts of polycrystal shells and the low-field peak is related to the disordered system of ferromagnetic particles.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mikhlin Y. L., Nasluzov V., Ivaneeva A., Vorobyev S., Likhatski M., Romanchenko A., Krylov A. S., Zharkov S. M., Meira D. M.
Заглавие : Formation, evolution and characteristics of copper sulfide nanoparticles in the reactions of aqueous cupric and sulfide ions
Место публикации : Mater. Chem. Phys. - 2020. - Vol. 255. - Ст.123600. - ISSN 02540584 (ISSN), DOI 10.1016/j.matchemphys.2020.123600
Примечания : Cited References: 74. - This research was supported by the Russian Foundation for Basic Research , project 18-03-00526a . We thank the ESRF for allocating beamtime, and the BM23 staff for their help during the experiments. Facilities of the Krasnoyarsk Regional Research Equipment Centre of SB RAS were employed in the work
Аннотация: Colloidal copper sulfides produced in reactions of aqueous copper and sulfide ions are important for many materials applications, environment and mineral processing. Here, CuxS nanoparticles formed and aged at varying copper sulfate to sodium sulfide ratios were studied using in situ UV–vis–NIR spectroscopy, dynamic light scattering, X-ray absorption spectroscopy, ex situ TEM, X-ray photoelectron spectroscopy and Raman scattering, and DFT + U calculations. It was established that the ratio of aqueous Cu2+ to S2− ions of 1:2 is critical for the reaction, which yields disordered covellite-like 4–6 nm Cu0.7S nanoparticles comprised polysulfide species at this and higher sulfide concentrations; upon aging, the particles release sulfur and transform to chalcocite-like structure (Cu2-xS, x  1). Conversely, at the “excess” of copper ions, Cu2-xS-type particles grew into 12–14 nm “covellitic” nanoparticles. The optical absorbance at 1100–1200 nm commonly attributed to localized surface plasmon resonance increased with time and was lowest for Cu2+/S2−
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Petrov D. A., Lin C. R., Ivantsov R. D., Ovchinnikov S. G., Zharkov S. M., Yurkin G. Yu., Velikanov D. A., Knyazev Yu. V., Molokeev M. S., Tseng Y. T., Lin E. S., Edelman I. S., Baskakov A. O., Starchikov S. S., Lyubutin I. S.
Заглавие : Characterization of the iron oxide phases formed during the synthesis of core-shell FexOy@C nanoparticles modified with Ag
Место публикации : Nanotechnology. - 2020. - Vol. 31, Is. 39. - Ст.395703. - ISSN 13616528 (ISSN), DOI 10.1088/1361-6528/ab9af2
Примечания : Cited References: 46. - The reported study was funded by Joint Research Project of Russian Foundation for Basic Research № 19-52-52002 and Ministry of Science and Technology, Taiwan MOST № 108-2923-M-153-001-MY3 and № 106-2112-M-153-001-MY3. The samples of series 1 were studied with the support of the Ministry of Science and Higher Education of the Russian Federation within the State assignment FSRC «Crystallography and Photonics» RAS. The electron microscopy investigations were conducted in the SFU Joint Scientific Center supported by the State assignment (#FSRZ-2020-0011) of the Ministry of Science and Higher Education of the Russian Federation
Аннотация: Core–shell FexOy@C nanoparticles (NPs) modified with Ag were studied with x-ray diffraction, transmission electron microscopy, energy dispersive elemental mapping, Mössbauer spectroscopy, static magnetic measurements, and optical magnetic circular dichroism (MCD). FexOy@C NPs synthesized by the pyrolysis process of the mixture of Fe(NO3)3 centerdot 9H2O with oleylamine and oleic acid were added to a heated mixture of oleylamine and AgNO3 in different concentrations. The final product was a mixture of iron oxide crystalline NPs in an amorphous carbon shell and Ag crystalline NPs. The iron oxide NPs were presented by two magnetic phases with extremely close crystal structures: Fe3O4 and γ-Fe2O3. Ag is shown to form crystalline NPs located very close to the iron oxide NPs. An assumption is made about the formation of hybrid FexOy@C-Ag NPs. Correlations were obtained between the Ag concentration in the fabricated samples, their magnetic properties and the MCD spectrum shape. Introducing Ag led to a approximately linear decrease of the NPs saturation magnetization depending upon the Ag concentration, it also resulted into the MCD spectrum shift to the lower light wave energies. MCD was also studied for the Fe3O4@C NPs synthesized earlier with the same one-step process using different heat treatment temperatures, and MCD spectra were compared for two series of NPs. A possible contribution of the surface plasmon excitation in Ag NPs to the MCD spectrum of the FexOy@C-Ag NPs is discussed.
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11.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Патрин, Геннадий Семёнович, Матаев М. М., Сейтбекова К. Ж., Шиян, Ярослав Германович, Яриков, Станислав Алексеевич, Жарков, Сергей Михайлович
Заглавие : Магнитные и резонансные свойства поликристалла Y0.5Sr0.5Cr0.5Mn0.5O3
Место публикации : Физ. тверд. тела. - 2020. - Т. 62, Вып. 8. - С. 1204-1208. - ISSN 0367-3294, DOI 10.21883/FTT.2020.08.49602.089
Примечания : Библиогр.: 20. - Настоящие исследования ведутся при финансовой поддержке Министерства образования и науки Республики Казахстан (грант No 05130165) и в рамках договора о сотрудничестве между Сибирским федеральным университетом и Казахским государственным женским педагогическим университетом
Аннотация: Представлены результаты экспериментальных исследований магнитостатических и магниторезонансных свойств поликристаллической системы Y0.5Sr0.5Cr0.5Mn0.5O3. Получено, что преобладающим является внутрикристаллическое ферромагнитное взаимодействие, при этом межкристаллическое взаимодействие носит антиферромагнитный характер. Спектр магнитного резонанса в магнитоупорядоченной области состоит из двух линий. Высокополевая линия относится к взаимодействующим частям оболочек поликристаллитов, а низкополевой пик связан с неупорядоченной системой ферромагнитных частиц.
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12.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Pryazhnikov M. I., Minakov A. V., Lyamkin A. I., Red’kin V. E., Zharkov S. M., Zeer G. M.
Заглавие : Experimental Study of Transport Coefficients of Aqueous Suspensions of Nanodiamonds
Место публикации : Colloid J. - 2020. - Vol. 82, Is. 6. - P.705-712. - ISSN 1061933X (ISSN), DOI 10.1134/S1061933X20060101
Примечания : Cited References: 31. - This work was carried out within the framework of the state order of the Ministry of Science and Higher Education of the Russian Federation (project no. FSRZ-2020-0012)
Аннотация: This article presents experimental data on the coefficients of viscosity and thermal and electrical conductivities, as well as the absorption spectra, of suspensions of ultradispersed diamonds. Suspensions of UDA-S and UDP-A detonation nanodiamond particles, as well as UDP-AG diamond–graphite powder, are used in the experiments. The concentration of nanodiamonds in distilled water is varied within a range of 0.5–5 wt %. It is shown that the technology of purification diamond powders from side products of their synthesis substantially affects the physicochemical properties of aqueous suspensions of these powders.
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13.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Orlov Yu. S., Sokolov A. Е., Dudnikov V. A., Shulga K. V., Volochaev M. N., Zharkov S. M., Shestakov N. P., Vysotin M. A., Ovchinnikov S. G.
Заглавие : Contribution of the multiplicity fluctuation in the temperature dependence of phonon spectra of rare-earth cobaltites
Место публикации : Molecules. - 2020. - Vol. 25, Is. 18. - Ст.4316. - ISSN 14203049 (ISSN), DOI 10.3390/molecules25184316
Примечания : Cited References: 34. - This work was supported by the Russian Science Foundation grant 18-02-00022. The scanning electron microscopy investigations were conducted in the SFU Joint Scientific Center, supported by the State assignment (#FSRZ-2020-0011) of the Ministry of Science and Higher Education of the Russian Federation. The other research was carried out at the Krasnoyarsk Regional Center of Research Equipment of the Federal Research Center “Krasnoyarsk Science Center SB RAS”
Аннотация: We have studied, both experimentally and theoretically, the unusual temperature dependence of the phonon spectra in NdCoO3, SmCoO3 and GdCoO3, where the Co3+ ion is in the low-spin (LS) ground state, and at the finite temperature, the high-spin (HS) term has a nonzero concentration nHS due to multiplicity fluctuations. We measured the absorption spectra in polycrystalline and nanostructured samples in the temperature range 3–550 K and found a quite strong breathing mode softening that cannot be explained by standard lattice anharmonicity. We showed that the anharmonicity in the electron–phonon interaction is responsible for this red shift proportional to the nHS concentration.
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14.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Markovskaya, Dina, V, Zhurenok, Angelina, V, Kurenkova, Anna Yu, Kremneva, Anna M., Saraev, Andrey A., Zharkov S. M., Kozlova, Ekaterina A., Kaichev, Vasily V.
Заглавие : New titania-based photocatalysts for hydrogen production from aqueous-alcoholic solutions of methylene blue
Место публикации : RSC Adv. - 2020. - Vol. 10, Is. 56. - P.34137-34148. - ISSN 2046-2069(eISSN), DOI 10.1039/d0ra07630a
Примечания : Cited References: 57. - The XPS and XRD experiments were performed using facilities of the shared research center "National center for investigation of catalysts" at Boreskov Institute of Catalysis. The authors are grateful to Dr S. Cherepanova for the XRD study and Dr T. Larina and Dr D. Selishchev for the UV-vis measurements. The TEM investigations were conducted in the SFU Joint Scientific Center supported by the State assignment (#FSRZ-2020-0011) of the Ministry of Science and Higher Education of the Russian Federation
Предметные рубрики: Ray absorption-edge
In-situ
Ag nanoparticles
Chemical-states
XPS analysis
Аннотация: A series of CuOx–TiO2 photocatalysts were prepared using fresh and thermally activated Evonik Aeroxide P25 titanium dioxide. The photocatalysts were characterized by X-ray diffraction, transmission electron microscopy, X-ray photoelectron spectroscopy, XANES, diffuse reflectance spectroscopy, and N2 adsorption technique. Photocatalytic activity of the samples was tested in hydrogen production from aqueous-alcoholic solutions of methylene blue under UV radiation (λ = 386 nm). It was found for the first time the synergistic effect of hydrogen production from two substrates—dye and ethanol. The maximum hydrogen production rate in the system water–ethanol–methylene blue was 1 μmol min−1, which is 25 times higher than a value measured in a 10% solution of ethanol in water. The thermal activation of titania also leads to a change in the rate of hydrogen production. The highest catalytic activity was observed for a CuOx–TiO2 photocatalyst based on titania thermally-activated at 600 °C in air. A mechanism of the photocatalytic reaction is discussed.
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15.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Быкова, Людмила Евгеньевна, Жарков, Сергей Михайлович, Мягков, Виктор Григорьевич, Балашов, Юрий Юрьевич, Патрин, Геннадий Семёнович
Заглавие : Формирование интерметаллида Cu6Sn5 в тонких пленках Cu/Sn
Место публикации : Физ. тверд. тела. - 2021. - Т. 63, Вып. 12. - С. 2205-2209. - ISSN 0367-3294, DOI 10.21883/FTT.2021.12.51685.139
Примечания : Библиогр.: 16. - Исследование выполнено при финансовой поддержке Российского фонда фундаментальных исследований (грант No 19-43-240003). Электронно-микроскопические исследования проведены в Красноярском региональном центре коллективного пользования ФИЦ КНЦ СО РАН и лаборатории электронной микроскопии ЦКП СФУ, поддержанной в рамках государственного задания Министерства науки и высшего образования Российской Федерации (код научной темы FSRZ-2020-0011)
Аннотация: Исследовано формирование интерметаллида Cu6Sn5 в двухслойных тонких пленках Sn(55 nm)/Cu(30 nm) при нагреве непосредственно в колонне просвечивающего электронного микроскопа (режим дифракции электронов) от комнатной температуры до 300°C с фиксацией электронограмм. Полученные в результате твердофазной реакции пленки были монофазными и состояли из гексагональной η-Cu6Sn5 фазы. Установлен температурный интервал образования η-Cu6Sn5 фазы (95-260°C). На основании проведенной оценки эффективного коэффициента взаимной диффузии при реакции (5·10-16 m2/s) предположено, что основным механизмом образования тонких пленок Cu6Sn5 является диффузия по границам зерен и дислокациям. Ключевые слова: тонкие пленки, интерметаллид Cu6Sn5, просвечивающая электронная микроскопия, дифракция электронов.
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16.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Lin C. -R., Ivanova O. S., Petrov D. A., Sokolov A. Е., Chen Y. -Z., Gerasimova M. A., Zharkov S. M., Tseng Y. -T., Shestakov N. P., Edelman I. S.
Заглавие : Amino-functionalized Fe3O4@SiO2 core-shell magnetic nanoparticles for dye adsorption
Место публикации : Nanomaterials. - 2021. - Vol. 11, Is. 9. - Ст.2371. - ISSN 20794991 (ISSN), DOI 10.3390/nano11092371
Примечания : Cited References: 35. - The authors are thankful for the financial support the Russian Foundation for Basic Research, Grant № 19-52-52002, Ministry of Science and Technology of Taiwan, Grants MOST № 108-2923-M-153-001-MY3 and № 109-2112-M-153-003-, the Russian Foundation for Basic Research with Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund of Science, the research project number 19-42-240005: “Features of the electronic structure, magnetic properties and optical excitations in nanocrystals of the multifunctional magnetic chalcogenides Fe3S4 and FeSe”. We thank also the SFU Joint Scientific Center supported by the State assignment (#FSRZ-2020-0011) of the Ministry of Science and Higher Education of the Russian Federation, where the Transmission Electron Microscopy studies were carried out
Аннотация: Fe3O4@SiO2 core-shell nanoparticles (NPs) were synthesized with the co-precipitation method and functionalized with NH2 amino-groups. The nanoparticles were characterized by X-ray, FT-IR spectroscopy, transmission electron microscopy, selected area electron diffraction, and vibrating sample magnetometry. The magnetic core of all the nanoparticles was shown to be nanocrystalline with the crystal parameters corresponding only to the Fe3O4 phase covered with a homogeneous amorphous silica (SiO2) shell of about 6 nm in thickness. The FT-IR spectra confirmed the appearance of chemical bonds at amino functionalization. The magnetic measurements revealed unusually high saturation magnetization of the initial Fe3O4 nanoparticles, which was presumably associated with the deviations in the Fe ion distribution between the tetrahedral and octahedral positions in the nanocrystals as compared to the bulk stoichiometric magnetite. The fluorescent spectrum of eosin Y-doped NPs dispersed in water solution was obtained and a red shift and line broadening (in comparison with the dye molecules being free in water) were revealed and explained. Most attention was paid to the adsorption properties of the nanoparticles with respect to three dyes: methylene blue, Congo red, and eosin Y. The kinetic data showed that the adsorption processes were associated with the pseudo-second order mechanism for all three dyes. The equilibrium data were more compatible with the Langmuir isotherm and the maximum adsorption capacity was reached for Congo red.
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17.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Chzhan A. V., Podorozhnyak S. A., Zharkov S. M., Gromilov S. A., Patrin G. S.
Заглавие : Induced magnetic anisotropy of Co-P thin films obtained by electroless deposition
Место публикации : J. Magn. Magn. Mater. - 2021. - Vol. 537. - Ст.168129. - ISSN 03048853 (ISSN), DOI 10.1016/j.jmmm.2021.168129
Примечания : Cited References: 28. - The work is partially supported by the RFBR Foundation (10-02-00161-a project). The study has been carried out within the framework of the state task of the Ministry of science and higher education of the Russian Federation (topic No. FSRZ-2020-0011)
Аннотация: Co1−x-Px films (x = 0.02–0.05) deposited on cover glass by electroless plating from aqueous solutions in a continuous magnetic field with the strength of 2.5 kOe are presented. It has been found that in the pH range from 7.2 to 9.3, two special areas can be distinguished, they are characterized by the deposition of films with qualitatively different parameters in them. So, the change of the pH of working solutions from 7.2 to 8.7 causes the increase in the value of the induced magnetic anisotropy constant KU from 2.5 × 105 erg/cm3 to 6 × 105 erg/cm3. If the value of the hydrogen index is still increasing, an uneven drop to 5 × 104 erg/cm3 is observed. In the same way, the coercivity HC changes; at first it grows from 700 Oe to 1.5 kOe, and then it drops to Oe units. The concentration of phosphorus in the range of 7.2 to 8.7 increases linearly from 2 to 3 wt%, and in the range of 8.7 to 9.3, it increases from 3 to 5 wt%. The x-ray diffraction data show that the samples obtained at pH8.7 are characterized by the presence of the hcp phase of Co (α-Co). The observed reflections of films obtained at pH 8.7 indicate the fcc-Co (β-Co) with the diffraction peak blurring: the greater the pH value of the samples obtained, the more the diffraction peak blurring. It is shown that the induced magnetic anisotropy in high-coercivity films relates to the modification of the Co lattice. The lattice passes from a distorted fcc to an hcp structure during the growth of crystallites in a magnetic field. The induced magnetic anisotropy appears in films that were obtained in the high pH field due to the ordering of magnetic ions pairs.
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18.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Ivantsov R. D., Chun-Rong Lin, Knyazev Yu. V., Ying Zhen Chen, Zharkov S. M., Lin E. S., Chen B.Y., Yaw-Teng Tseng, Edelman I. S.
Заглавие : Morphology and magnetic properties of iron sulphides nanoparticles synthesized by the thermal decomposition method with different surfactants
Коллективы : "Новое в магнетизме и магнитных материалах", международная конференция, Научный совет по физике конденсированных сред РАН, МИРЭА - Российский технологический университет, Московский государственный университет им. М.В. Ломоносова, Магнитное общество России
Место публикации : Новое в магнетизме и магнитных материалах: сборник трудов XXIV международной конференции/ прогр. ком.: Р. С. Исхаков, С. Г. Овчинников [и др.]. - 2021. - Секция 11: Магнитные наноструктуры. - Ст.11-25-28
Примечания : Библиогр.: 4
Аннотация: Morphology, magnetic, and structural properties were investigated of the iron sulphides (FexSy) nanoparticles fabricated by the thermal decomposition method using oleylamine, 1-hexadecylamine and octadecylamine surfactants. The presence of surfactant layer is confirmed by FT-IR spectroscopy and thermo-gravimetric analysis. The structural analysis and Mцssbauer spectroscopy of synthesized nanoparticles showed in main Fe3S4 phase with inclusions of Fe9S11 in cases of OLA and HDA surfactants and significant admixture of FeS2 and even Fe2O3 in case of ODA surfactant. Deviations of iron ions distribution among crystal positions from that in bulk pure greigite and the pronounce changes in the magnetic circular dichroism (MCD) spectra are explained with the influence of surfactants on the particles formation process as well with the role of the boundary between magnetic core and organic shell.
Материалы конференции,
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19.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Lin, Chun-Rong, Ivanova O. S., Edelman I. S., Knyazev Yu. V., Zharkov S. M., Petrov D. A., Sokolov A. Е., Svetlitsky E. S., Velikanov D. A., Solovyov, Leonid A., Chen, Ying-Zhen, Tseng, Yaw-Teng
Заглавие : Carbon double coated Fe3O4@C@C nanoparticles: Morphology features, magnetic properties, dye adsorption
Коллективы : Russian Foundation for Basic ResearchRussian Foundation for Basic Research (RFBR) [19-52-52002]; Ministry of Science and Technology of TaiwanMinistry of Science and Technology, Taiwan [108-2923-M-153-001-MY3, 109-2112-M-153-003]; Joint Scientific Center of the Siberian Federal University [FSRZ-2020-0011]; Ministry of Science and Higher Education of the Russian Federation
Место публикации : Nanomaterials. - 2022. - Vol. 12, Is. 3. - Ст.376. - ISSN 2079-4991(eISSN), DOI 10.3390/nano12030376
Примечания : Cited References: 44. - The work was supported financially by the Russian Foundation for Basic Research, Grant No. 19-52-52002 and Ministry of Science and Technology of Taiwan, Grants MOST No. 108-2923-M-153-001-MY3 and No. 109-2112-M-153-003-. The support was obtained also from the Joint Scientific Center of the Siberian Federal University supported by the State assignment (#FSRZ-2020-0011) of the Ministry of Science and Higher Education of the Russian Federation, where the Transmission Electron Microscopy studies were carried out
Предметные рубрики: SOLID-PHASE EXTRACTION
FE3O4 NANOPARTICLES
PROFILE REFINEMENT
Аннотация: This work is devoted to the study of magnetic Fe3O4 nanoparticles doubly coated with carbon. First, Fe3O4@C nanoparticles were synthesized by thermal decomposition. Then these synthesized nanoparticles, 20–30 nm in size were processed in a solution of glucose at 200 °C during 12 h, which led to an unexpected phenomenon – the nanoparticles self-assembled into large conglomerates of a regular shape of about 300 nm in size. The morphology and features of the magnetic properties of the obtained hybrid nanoparticles were characterized by transmission electron microscopy, differential thermo-gravimetric analysis, vibrating sample magnetometer, magnetic circular dichroism and Mössbauer spectroscopy. It was shown that the magnetic core of Fe3O4@C nanoparticles was nano-crystalline, corresponding to the Fe3O4 phase. The Fe3O4@C@C nanoparticles presumably contain Fe3O4 phase (80%) with admixture of maghemite (20%), the thickness of the carbon shell in the first case was of about 2–4 nm. The formation of very large nanoparticle conglomerates with a linear size up to 300 nm and of the same regular shape is a remarkable peculiarity of the Fe3O4@C@C nanoparticles. Adsorption of organic dyes from water by the studied nanoparticles was also studied. The best candidates for the removal of dyes were Fe3O4@C@C nanoparticles. The kinetic data showed that the adsorption processes were associated with the pseudo-second order mechanism for cationic dye methylene blue (MB) and anionic dye Congo red (CR). The equilibrium data were more consistent with the Langmuir isotherm and were perfectly described by the Langmuir–Freundlich model.
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20.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Izotov A. V., Belyaev B. A., Boev N. M., Burmitskikh A. V., Skomorokhov G. V., Zharkov S. M., Solovev P. N.
Заглавие : Ferromagnetic resonance line broadening and shift effect in nanocrystalline thin magnetic films: Relation with crystalline and magnetic structure
Коллективы : RFBRRussian Foundation for Basic Research (RFBR); Government of Krasnoyarsk Territory; Krasnoyarsk Regional Fund; JSC "NPP "Radiosviaz" [20-42-242901]; Ministry of Science and Higher Education of the Russian Federation [075-11-2019-054, FSRZ-2020-0011]
Место публикации : J. Alloy. Compd. - 2022. - Vol. 900. - Ст.163416. - ISSN 0925-8388, DOI 10.1016/j.jallcom.2021.163416. - ISSN 1873-4669(eISSN)
Примечания : Cited References: 52. - The reported study was funded by RFBR, the Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund and JSC "NPP "Radiosviaz", project number 20-42-242901 and was supported by the Ministry of Science and Higher Education of the Russian Federation, agreement number 075-11-2019-054 dated 22.11.2019.; The electron microscopy investigations were conducted in the SFU Joint Scientific Center whose infrastructure was supported by the State assignment (#FSRZ-2020-0011) of the Ministry of Science and Higher Education of the Russian Federation
Предметные рубрики: SUSCEPTIBILITY
RIPPLE
ANISOTROPIES
ALLOYS
Аннотация: With the rapid development of telecommunication technologies and highly integrated electronic devices, researchers show great interest in nanocrystalline soft magnetic thin films with unique characteristics for microwave applications. An important direction of the current research in this field is the study of high-frequency magnetization dynamics that directly depends on the damping processes in a magnetic medium. This paper reports on the effect of sharp broadening and shift of the ferromagnetic resonance (FMR) line revealed experimentally in a 40-nm-thick nanocrystalline permalloy (Fe20Ni80) thin film at a frequency of about 5 GHz. The effect arises only in films with crystallite size exceeding some critical value Dcr. The micromagnetic simulation demonstrates that exchange and dipolar interactions between randomly oriented crystallites form in the film a quasiperiodic magnetic structure with a characteristic wavelength in the range from 36 nm to 3.3 µm. An analysis of the two-magnon scattering model and simulation results shows that the formed magnetic structure provides the energy transfer from uniform magnetization oscillations (uniform FMR) to spin waves, which results in an additional energy dissipation channel and, consequently, sharp FMR line broadening. A theoretical estimate of the critical crystallite size Dcr based on this model yields a value of ~14.3 nm for 40-nm-thick Fe20Ni80 films.
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