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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Pogoreltsev E. I., Bogdanov E. V., Melnikova S.V., Flerov I. N., Laptash N. M.
Заглавие : (NH4)3HfF7: Crystallooptical and calorimetric studies of a number of successive phase transitions
Место публикации : J. Fluor. Chem.: Elsevier, 2017. - Vol. 204. - P.45-49. - ISSN 00221139 (ISSN), DOI 10.1016/j.jfluchem.2017.10.004
Примечания : Cited References: 14
Аннотация: Single crystals of (NH4)3HfF7 were grown. Polarising optical observations as well as measurement of the heat capacity and birefringence Δn(Т) were performed in the temperature range of 200–310 K. Reversible phase transitions at temperatures T0 = 290 K, Т1 = 280.5 K, Т2 ≈ 273 K, Т3 = 266 K, Т4 = 259 K, Т5 = 231 K, Т6 = 229 K were found. Observations in polarised light make it possible to suggest a sequence of changes in the symmetry groups for these transitions: Fm3m ⟵Т0→ cub. ⟵Т1→ mmm (1) ⟵Т2→ mmm (2) ⟵Т3→ mmm (3) ⟵Т5→ 2/c. The T-p phase diagram was studied and the temperature boundaries of the stability of the distorted crystalline phases were determined. A significant change of the entropy at successive phase transitions ΣΔS = 10.6 J/mol K indicates a disordering of the initial cubic phase.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mel'nikova S. V., Molokeev M. S., Laptash N. M., Misyul S. V.
Заглавие : A non-typical sequence of phase transitions in (NH4)3GeF7: optical and structural characterization
Коллективы : RFBR [15-02-02009 a]
Место публикации : Dalton Trans.: Royal Society of Chemistry, 2016. - Vol. 45, Is. 12. - P.5321-5327. - ISSN 1477-9226, DOI 10.1039/c5dt04907e. - ISSN 1477-9234(eISSN)
Примечания : Cited References:25. - The reported study was partially supported by RFBR, research project no. 15-02-02009 a
Предметные рубрики: Crystal-structure
Powder diffraction
NH4F
Fluorination
Аннотация: Single crystals of germanium double salt (NH4)3GeF7 = (NH4)2GeF6·NH4F = (NH4)3[GeF6]F were grown and studied by the methods of polarization optics and X-ray diffraction. The birefringence Δn = (no − ne), the rotation angle of the optical indicatrix ϕ(T) and unit cell parameters were measured in the temperature range 100–400 K. Three structural phase transitions were found at the temperatures: T1↓ = 279.2 K (T1↑ = 279.4 K), T2↑ = 270 K (T2↓ = 268.9 K), T3↓ = 218 K (T3↑ = 227 K). An unusual sequence of symmetry transformations with temperature change was established: P4/mbm (Z = 2) (G1) ↔ Pbam (Z = 4) (G2) ↔ P21/c (Z = 4) (G3) ↔ Pa (Z = 8) (G4). The crystal structures of different phases were determined. The experimental data were additionally interpreted by a group-theoretical analysis of the complete condensate of order parameters taking into account the critical and noncritical atomic displacements. Strengthening of the N–H⋯F hydrogen bonds can be a driving force of the observed phase transitions.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Aleksandrov K. S., Melnikova S. V., Kokov I. T.
Заглавие : Phase-transitions in CS2CDI4 from measurements of birefringence and dielectric-properties
Место публикации : Fiz. Tverd. Tela: MEZHDUNARODNAYA KNIGA, 1987. - Vol. 29, Is. 8. - P.2487-2490. - ISSN 0367-3294
Примечания : Cited References: 8
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Aleksandrov K. S., Melnikova S. V., Misyul S. V.
Заглавие : Successive phase-transitions in ferroelastic cs2rbdyf6 with elpasolite-type structure
Место публикации : Phys. Status Solidi A. - 1987. - Vol. 104, Is. 2. - P.545-548. - ISSN 0031-8965, DOI 10.1002/pssa.2211040205
Примечания : Cited References: 6
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Aleksandrov K. S., Mel'nikova S. V., Kruglik A. I.
Заглавие : X-ray and optic investigations of phase-transition in cslicro4 crystal
Место публикации : Ferroelectrics: Gordon Breach SCI Publ LTD, 1988. - Vol. 81, Is. 1. - P.153-156. - ISSN 0015-0193, DOI 10.1080/00150198808008833
Примечания : Cited References: 2
Аннотация: The study of optical properties and X-ray investigations were carried out in CsLiCrO4crystal. It was found (is discussed) an unusual 4 temperature dependence of optical indicatrix rotation and monoclinic angles.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Aleksandrov K. S., Melnikova S.V., Kruglik A. I.
Заглавие : X-ray and optical study of ferroelastic phase transition in CsLiCrO4 crystal
Коллективы : European meeting on ferroelectricity
Место публикации : Sixth European meeting on ferroelectrisity: abstracts. - Poznan, 1987. - P.329
Материалы конференции
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Aleksandrov K. S., Melnikova S.V., Kruglik A. I.
Заглавие : X-ray and optical study of ferroelastic phase transition in CsLiCrO4 single crystal
Место публикации : Acta crystallographica Section A: Foundations and Advances. - 1987. - Vol. 43. - Ст.C-93
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mel'nikova S. V., Aleksandrov K. S., Anistratov A. T., Beznosikov B. V.
Заглавие : Birefringence and structural phase transitions in ABCl//3-type crystals
Место публикации : Sov. Phys. Solid State. - 1977. - Vol. 19, Is. 1. - P.18-20; Phys. Solid State
Ключевые слова (''Своб.индексиров.''): electrooptical effects--crystals
Аннотация: The refractive indices and birefringence of CsPbCl//3, TlMnCl//3, and CsSrCl//3 were determined a wide temperature range, which included phase transition points. Relatively high values of the photoelastic and acoustooptic characteristics were obtained: the th acoustooptic figure of merit M//2 was 12 multiplied by (times) 10** minus **1**8 cgs units for TlMnCl//3 and 98 multiplied by (times) 10** minus **1**8 cgs units for CsPbCl//3. A strong influence of partial Sr for Ca substitution on the properties and transition temperatures was observed. A phenomenological theory was used to analyze the relationship between the birefringence anomalies and the theromodynamic parameters of the transitions. A comparison was made with KMnF//3 and SrTiO//3.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Aleksandrov K. S., Anistratov A. T., Mel'nikova S. V., Zinenko V. I., Shabanova L. A., Beznosikov B. V.
Заглавие : Birefringence, twinning and structural phase transitions in ABCl3 single crystals
Коллективы : International meeting on ferroelectricity
Место публикации : Ferroelectrics. - 1978. - Vol. 20, Spesial issue. - P.305-307. - DOI 10.1080/00150197808237245
Аннотация: The temperature investigations of birefringence, twinning and elasticity of CsPbCl3, CsSrCl3, TlMnCl3, RbCdCl3, CsCaCl3 and RbMnCl3, were carried out. A group-theoretical analysis is made and the description of phase transitions is given.
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10.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Chekanova L. A., Denisova E. A., Mel'nikova S. V., Iskhakov R. S.
Заглавие : Composite magnetic materials based on porous templates with different pores morphology: synthesis and magnetic properties
Коллективы : Euro-Asian Symposium "Trends in MAGnetism": Nanomagnetism
Место публикации : V Euro-Asian simposium "Trend in MAGnetism": Nanomagnetism: abstracts. - Vladivostok: FEFU, 2013. - С. 169. - ISBN 978-5-7444-3124-2
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11.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Flerov I. N., Tressaud A., Aleksandrov K. S., Couzi M., Gorev M. V., Grannec J., Melnikova S. V., Chaminade J. P., Misul S. V., Voronov V. N.
Заглавие : Effect of B3+ ion size on the phase transitions in Rb2KB3+F6 elpasolites series
Место публикации : Ferroelectrics: Gordon breach SCI publ LTD, 1991. - Vol. 124, Is. 1. - P.309-314. - ISSN 0015-0193, DOI 10.1080/00150199108209457
Аннотация: The physical properties of Rb2KScF6 crystal characterized by the medium size of B3+ atom in Rb2KB3+F6 series are studied. The two successive phase transitions from cubic into tetragonal and then into monoclinic phases are found. The results are discussed in view of the influence of B3+ atom size on structural transformations.
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12.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Bogdanov E. V., Pogoreltsev E. I., Gorev M. V., Mel'nikova S. V., Molokeev M. S., Laptash N. M., Flerov I. N.
Заглавие : Effect of the size of the central atom on the stability of crystalline phases in solid solutions (NH4)3TixSn1-xF7
Колич.характеристики :8 с
Место публикации : J. Solid State Chem. - 2023. - Vol. 328. - Ст.124373. - ISSN 00224596 (ISSN), DOI 10.1016/j.jssc.2023.124373. - ISSN 1095726X (eISSN)
Примечания : Cited References: 20. - The study was supported by a grant from the Russian Science Foundation № 23-22-00115, https://rscf.ru/project/23-22-00115/X-ray and dilatometric data and SEM images were obtained using the equipment of the Krasnoyarsk Regional Center for Collective Use of the Federal Research Center — Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of Sciences. We are grateful to Dr. A.V. Shabanov for examination of the SEM images
Аннотация: The effect of a change in internal pressure as a result of partial substitution of the central atom on the realization and stability of the initial and distorted crystalline phases in (NH4)3TixSn1-xF7 solid solutions has been studied. It was found that at a Ti concentration in the range of x = 0.15–0.40, the reconstructive transition Pm-3m ↔ Pa-3 is transformed into a sequence of phase transitions Pm-3m ↔ P4/mbm ↔ P4/mnc ↔ Pa-3. In the (NH4)3Ti0.15Sn0.85F7 solid solution, the first-order phase transition between two cubic phases at T0 = 352 K is characterized by a significant volume jump δ(ΔV/V0) ≈ 1 %, comparable with that in (NH4)3SnF7. An increase of the Ti concentration leads to a strong decrease in the stability of the Pm-3m cubic phase: the first tetragonal P4/mbm phase appears in (NH4)3Ti0.4Sn0.6F7 at T0 = 400 K, which proves the existence of the predicted high-temperature cubic phase in (NH4)3TiF7. In solid solutions, a decrease in birefringence and entropy of phase transitions was observed in comparison with the initial compounds with Sn and Ti as central atoms. The role of critical parameters (unit cell volume, temperature, external pressure) in the formation of cubic and distorted phases is discussed.
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13.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Gudim I. A., Mikhashenok N. V., Vasiliev A. D., Melnikova S. V., Pavlovskii M. S., Skorobogatov S. A., Pankrats A. I.
Заглавие : Features of the melt–solution synthesis of the TbCr3(BO3)4 single crystals
Колич.характеристики :6 с
Место публикации : J. Cryst. Growth. - 2024. - Vol. 637-638. - Ст.127716. - ISSN 00220248 (ISSN), DOI 10.1016/j.jcrysgro.2024.127716. - ISSN 18735002 (eISSN)
Примечания : Cited References: 22. - The authors thank A.V. Zamkov for assistance in preparing the samples for the conoscopic study. The characterization and examination of the samples were performed at the Center for Collective Use, Krasnoyarsk Scientific Center, Siberian Branch of the Russian Academy of SciencesThis study was supported in part by the Russian Science Foundation and the Krasnoyarsk Territorial Foundation for Support of Scientific and R&D Activity, project no. 22-12-20019
Аннотация: The phase formation of terbium chromoborate TbCr3(BO3)4 in the bismuth trimolybdate and lithium tungstate melt–solutions has been studied. The absence of the terbium chromoborate trigonal phase in the bismuth trimolybdate-based system at all component ratios has been shown. The component ratio in the lithium tungstate-based system has been found at which the TbCr3(BO3)4 trigonal crystals are formed at temperatures above 1100 °C; below this temperature, the monoclinic phase dominates. The structural and magnetic properties of the grown crystals have been studied. It has been established that the trigonal and monoclinic TbCr3(BO3)4 crystals synthesized from the lithium tungstate-based solvent exhibit identical magnetic properties. At the same time, a significant difference of the magnetic properties of the single crystals synthesized from the bismuth molybdate melt–solution has been observed. This difference has been attributed to the effect of Bi3+ ions that partially replace Tb3+ ions.
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14.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Melnikova S. V., Shabanova L. A., Zaitsev A. I., Parshikov S. A., Ageev O. A., Aleksandrov K. S.
Заглавие : Ferroelastic phase transition in Cs3Bi2I9 crystal
Место публикации : Ferroelectrics, Letters Section. - 1996. - Vol. 20, Is. 5-6. - P.163-167. - ISSN 0731-5171
Ключевые слова (''Своб.индексиров.''): birefringence--cesium compounds--crystal symmetry--crystals--differential scanning calorimetry--elasticity--ferroelectricity--permittivity--stiffness--twinning--cesium bismuth iodide--elastic constant--elastic stiffness--ferroelastic phase transition--phase transitions
Аннотация: Phase transition (PT) was found in Cs3Bi2I9 single crystal at T0=223 K. Optical birefringence, dielectric and elastic constants and differential scanning calorimetry have been studied. It was found that birefringence ?nc and twinning picture appeared on (001) - and (100) - plates below T0, as well as softening of elastic stiffness C44 above T0. It allows to classify the PT as proper ferroelastic one with symmetry change 6/mmm - 2/m. В© 1996 OPA (Overseas Publishers Association) Amsterdam B.V. Published in The Netherlands under license by Gordon and Breach Science Publishers SA.
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15.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Pogoreltsev E. I., Mel'nikova S. V., Kartashev A. V., Molokeev M. S., Gorev M. V., Flerov I. N., Laptash N. M.
Заглавие : Ferroelastic phase transitions in (NH4)2TaF7
Место публикации : Phys. Sol. St.: Pleiades Publishing, 2013. - Vol. 55, Is. 3. - P.611-618. - DOI 10.1134/S1063783413030232
Аннотация: The heat capacity, unit cell parameters, permittivity, optical properties, and thermal expansion of the (NH4)2TaF7 compound with a seven coordinated anion polyhedron have been measured. It has been found that the compound undergoes two successive phase transitions with the symmetry change: tetragonal (T1 = 174 K) orthorhombic (T2 = 156 K) tetragonal. The ferroelastic nature of structural transformations has been established, and their entropy and susceptibility to hydrostatic pressure have been determined.
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16.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Gorev M. V., Flerov I. N., Melnikova S.V., Misyul S. V., Bovina A. F., Afanasiev M. L., Tresso A.
Заглавие : Ferroelectric phase transitions in cryolite (NH4)(3)ScF6
Коллективы : Конференция по физике сегнетоэлектриков
Место публикации : Izv. Akad. Nauk Ser. Fiz. - 2000. - Vol. 64, Is. 6. - P.1104-1110. - ISSN 1026-3489
Примечания : Cited References: 9
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17.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Aleksandrov K. S., Anistratov A. T., Melnikova S. V., KLEVTSOV P. V., KRUGLIK A. I., VORONOV V. N.
Заглавие : Ferroelectric phase-transitions in CSLIMOO4 single-crystals
Место публикации : Phys. Status Solidi A. - 1981. - Vol. 67, Is. 2. - P.377-380. - ISSN 0031-8965, DOI 10.1002/pssa.2210670203
Примечания : Cited References: 3
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18.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Aleksandrov K. S., ANISTRATOV A. T., Melnikova S. V., Klevtsov P. V., Kruglik A. I., Voronov V. N.
Заглавие : Ferroelectricity in caesium lithium molybdate CsLiMoO4 and related crystals CsLiWO4 and RbLiMoO4
Коллективы : International meeting on ferroelectricity
Место публикации : International meeting on ferroelectricity (5 ; 1981 ; 17-21 Aug. ; Universal Park, USA). Ferroelectrics. - 1981. - Vol. 36, Is. 1. - P.399-402. - ISSN 0015-0193, DOI 10.1080/00150198108218138
Ключевые слова (''Своб.индексиров.''): cesium compounds--rubidium compounds--cesium lithium molybdate--cesium lithium tungstate--phase transitions--rubidium lithium molybdate--ferroelectric materials
Аннотация: Successive ferroelectric phase transitions were discovered in CsLiMoO//4, CsLiWO//4 and RbLiMoO//4 single crystals. Strong elastic and no dielectric anomalies were found with temperature lowering in the initial cubic phases. The phase transitions are qualitatively described as pseudoproper ferroelectric ones.
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19.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Aleksandrov K. S., Anistratov A. T., Melnikova S. V., Kruglik A. I., Zherebtsova L. I., Shabanova L. A.
Заглавие : Ferroelectricity in CS-Li molybdate crystals
Место публикации : Fiz. Tverd. Tela: Mezhdunarodnaya kniga, 1982. - Vol. 24, Is. 4. - P.1094-1101. - ISSN 0367-3294
Примечания : Cited References: 9
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20.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Flerov I. N., Kartashev A. V., Mel'nikova S. V.
Заглавие : Calorimetric and optical studies of orthorhombic and cubic CsLiCrO4 crystals
Разночтения заглавия :авие SCOPUS: Calorimetric and optical studies of orthorhombic and cubic CsLiCrO 4 crystals
Место публикации : Phys. Solid State: MAIK NAUKA/INTERPERIODICA/SPRINGER, 2006. - Vol. 48, Is. 11. - P2171-2176. - ISSN 1063-7834, DOI 10.1134/S1063783406110242
Примечания : Cited References: 23
Предметные рубрики: PHASE-TRANSITIONS
X-RAY
NH4LISO4
ALPHA
Аннотация: Careful calorimetric and polarization optical studies of a metastable cubic modification of a CsLiCrO4 crystal (space group (F43m)) are performed. Anomalies of the heat capacity indicative of structural distortions at 92.4 and 69.1 K were revealed, and the values of the thermodynamic parameters of the phase transitions were determined. The crystal twinning in the intermediate phase was studied. A comparative analysis of the phase transitions occurring in a series of ALiMO(4) crystals (A=NH4, Cs; M=S, Cr, Mo, W) was performed. First studies of the monotropic structural transformation F43m - Pmcn and the enantiotropic phase transition Pmcn reversible arrow P112(1)/n were carried out using scanning calorimetry, and the thermodynamic parameters of these transitions were determined.
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