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    A comparative study of γ-Fe2O3 and ε-Fe2O3 nanoparticles arising in borate glasses doped with Fe and Gd / O. S. Ivanova [et al.] // J. Sib. Fed. Univ. Math. Phys. - 2016. - Vol. 9, Is. 4. - P. 459–462 ; Журн. СФУ. Сер. "Математика и физика", DOI 10.17516/1997-1397-2016-9-4-459-462. - Cited References: 6. - The work was supported partly by the RFBR, 14-02-01211-a, and by the President of Russia Grant NSh-7559.2016.2. . - ISSN 1997-1397
   Перевод заглавия: Сравнительное изучение γ-Fe2O3 и ϵ-Fe2O3 наночастиц, формирующихся в стекле, допированном железом и гадолинием
Кл.слова (ненормированные):
magnetic nanoparticles -- magnetic circular dichroism -- magnetic measurements -- магнитные наночастицы -- магнитный круговой дихроизм -- магнитные измерения
Аннотация: Formation and properties of the iron oxides γ -Fe2O3 and ϵ-Fe2O3 nanoparticles arising in glasses of basic compositions Ge2O-K2O-Al2O3-B2O3 and K2O-Al2O3-B2O3 doped with different concentrations of Fe2O3 and Gd2O3 and subjected to the additional thermal treatment are studied. The X-ray diffraction, TEM microscopy, magnetooptical effects, and electron spin resonance study allow elucidating the matrix and Gd role in determining the nanoparticle properties.
Изучены свойства наночастиц γ-Fe2O3 и ϵ-Fe2O3, формирующихся в стеклах основного состава Ge2O-K2O-Al2O3-B2O3 и K2O-Al2O3-B2O3, допированных Fe2O3 и Gd2O3 и подвергнутых дополни- тельной термической обработке. Результаты исследования рентгеновской дифракции, электрон- ной микроскопии, магнитооптических эффектов и электронного спинового резонанса позволили объяснить роль матрицы и гадолиния в определении свойств наночастиц.

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Доп.точки доступа:
Ivanova, O. S.; Иванова, Оксана Станиславовна; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Edelman, I. S.; Эдельман, Ирина Самсоновна; Petrakovskaja, E. A.; Петраковская, Элеонора Анатольевна

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A comparative study of γ-Fe2O3 and ε-Fe2O3 nanoparticles arising in borate glasses doped with Fe and Gd / O. S. Ivanova [et al.] // VI Euro-Asian Symposium "Trends in MAGnetism" (EASTMAG-2016) : abstracts / ed.: O. A. Maksimova, R. D. Ivantsov. - Krasnoyarsk : KIP RAS SB, 2016. - Ст. P9.11. - P. 397. - References: 1. - The work was supported partly by the RFBR grant No. 14-02-01211 . - ISBN 978-5-904603-06-9
Кл.слова (ненормированные):
magnetic nanoparticles -- magnetic circular dichroism -- magnetic measurements

Доп.точки доступа:
Ivanova, O. S.; Иванова, Оксана Станиславовна; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Edelman, I. S.; Эдельман, Ирина Самсоновна; Petrakovskaja, E. A.; Петраковская, Элеонора Анатольевна; Euro-Asian Symposium "Trends in MAGnetism"(6 ; 2016 ; Aug. ; 15-19 ; Krasnoyarsk); "Trends in MAGnetism", Euro-Asian Symposium(6 ; 2016 ; Aug. ; 15-19 ; Krasnoyarsk); Институт физики им. Л.В. Киренского Сибирского отделения РАН

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A study of the synthesis products of fullerenes with nickel and cobalt / E. A. Petrakovskaya [et al.] // Tech. Phys. - 2001. - Vol. 46, Is. 1. - P. 42-46, DOI 10.1134/1.1340883. - Cited References: 15 . - ISSN 1063-7842

РУБ Physics, Applied
Рубрики:
COMPLEXES
SPECTRA
Аннотация: Qualitative analysis of the products of plasmochemical synthesis of fullerenes with metallic nickel and cobalt has been carried out using electron paramagnetic resonance (EPR) and electron microscopy. These studies show that the synthesis products are mainly fullerenes, metallic nanoparticles coated with an insulating layer, and isolated atomic clusters. (C) 2001 MAIK "Nauka/Interperiodica".

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Держатели документа:
Russian Acad Sci, LV Kirensky Phys Inst, Siberian Branch, Krasnoyarsk 660036, Russia
ИФ СО РАН
Kirenskii Inst. of Physics, Siberian Branch, RAS, Krasnoyarsk, 660036, Russian Federation

Доп.точки доступа:
Petrakovskaya, E. A.; Петраковская, Элеонора Анатольевна; Bulina, N. V.; Булина, Наталья Васильевна; Churilov, G. N.; Чурилов, Григорий Николаевич; Puzyr', A. P.
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Dissipative structures in thin films of cavitation-activated soot suspensions / O. P. Stebeleva [et al.] // J. Phys. Conf. Ser. - 2019. - Vol. 1399. - Ст. 044073, DOI 10.1088/1742-6596/1399/4/044073. - Cited References: 8 . - ISSN 1742-6588. - ISSN 1742-6596
Рубрики:
Engineering and Materials Science
Аннотация: This paper presents analysis of optical images of films obtained by evaporation (293 K) of a thin layer of low-concentrated (1% wt.) aqueous soot suspensions in a Petri dish. Suspensions of wood, fullerene and diamond-containing (after detonation synthesis) soot were prepared using hydrodynamic dispersion in a cavitation mixer with a wedge-shaped cavitator with the rotor's angular velocity of rotation being 10000 rpm. The components of the hydrodynamic dispersion process are turbulent micro-mixing and bubble cavitation. As a result of intense turbulence, carbon suspensions assumed properties of non-equilibrium systems. The images of an optical microscope revealed self-organized dissipative micron-sized structures in the dried films being present there in the form of chain, branched and ring-shaped cluster fractals of various dimensions that look very similar to nanotubes. The self-assembling effect was identified for all the types of suspensions under study. The EPR method was used to study the change in the electronic structure of soot resulting from the exposure to high temperatures and pressures that occur when the cavitation bubbles collapse (cavitational activation). The dynamics of changes in dissipative structures in the process of film drying was monitored.

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Держатели документа:
Siberian Federal University, Svobodnyy Ave, 79, Krasnoyarsk, 660049, Russia
L.V. Kirensky Institute of Physics SB RAS, Federal Research Center "Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of Sciences", Akademgorodok, 50, Krasnoyarsk, 660021, Russia
Federal Research Center "Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of Sciences", Akademgorodok, 50, Krasnoyarsk, 660021, Russia
Krasnoyarsk Institute of Railway Engineering Branch of Irkutsk State Transport University, Lado Kechoveli st, 89, Krasnoyarsk, 660028, Russia

Доп.точки доступа:
Stebeleva, O. P.; Kashkina, L. V.; Petrakovskaya, E. A.; Петраковская, Элеонора Анатольевна; Nikitin, S. L.; Dobrosmyslov, S. S.; Rublev, G. V.; "Conference on Applied Physics, Information Technologies and Engineering"(2019 ; Sept. ; 25-27 ; Krasnoyarsk, Russian Federation); "Прикладная физика, информационные технологии и инжиниринг", международная конференция(2019 ; сент. ; 25-27 ; Красноярск)
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Effect of gadolinium on magnetic circular dichroism and electron magnetic resonance of ε-Fe2O3 nanoparticles formed in borate glasses / I. Edelman [et al.] // J. Non-Cryst. Solids. - 2019. - Vol. 506. - P. 68-79, DOI 10.1016/j.jnoncrysol.2018.12.006. - Cited References: 81. - The work is supported by Russian Academy of Sciences in the frame of the Project № 0356-2017-0030. . - ISSN 0022-3093
Кл.слова (ненормированные):
Iron oxides -- ε-Fe2O3 -- Borate glasses -- Nanoparticles -- Magnetic circular dichroism -- Electron magnetic resonance
Аннотация: A remarkable characteristic of borate glasses is the ability of forming magnetic nanoparticles at low doping with transition element oxides. We have studied structure and magnetic properties of iron oxide nanoparticles formed in borate glasses, in particular, concentration and temperature dependences of magnetic circular dichroism (MCD) and electron magnetic resonance (EMR) spectra. A series of glasses of molar composition 22.5K2O-22.5Al2O3–55B2O3 doped with 1.5 mass % of Fe2O3 and different contents of Gd2O3 from 0.1 to 1.0 mass % was prepared using a conventional melt quenching technique and subjected to an additional thermal treatment. The whole set of results allows to identify the predominant magnetic phase in these glasses as ε-Fe2O3 nanoparticles, with a considerable part of iron ions substituted by gadolinium. Analysis and computer simulations of the EMR spectra allow separating the contribution of electron paramagnetic resonance of diluted iron ions and together with the temperature dependences of magnetization demonstrate a superparamagnetic character of the nanoparticle magnetism.

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Держатели документа:
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
LOMA, UMR 5798 Universite de Bordeaux-CNRS, Talence cedex, 33405, France
Siberian Federal University, Krasnoyarsk, 660041, Russian Federation
Boreskov Institute of Catalysis, Siberian Branch of RAS, Novosibirsk, 630090, Russian Federation
NRC “Kurchatov Institute”, Moscow, 123182, Russian Federation
Vavilov State Optical Institute, St.-Petersburg, 199053, Russian Federation

Доп.точки доступа:
Edelman, I. S.; Эдельман, Ирина Самсоновна; Kliava, J.; Ivanova, O. S.; Иванова, Оксана Станиславовна; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Zaikovskii, V.; Petrakovskaja, E. A.; Петраковская, Элеонора Анатольевна; Zubavichus, Y.; Stepanov, S.
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Efficiency of high energy impact in synthesis of coal-water suspensions / L. V. Kashkina [et al.] // Mater. Today: Proc. - 2018. - Vol. 5, Is. 12, Pt. 3. - P. 26033-26037, DOI 10.1016/j.matpr.2018.08.024. - Cited References: 18 . - ISSN 2214-7853
Кл.слова (ненормированные):
Coal-water slurry -- Cavitation -- Nanocarbon -- Man-made gas emission
Аннотация: A study of thermophysical and ecological properties of highly loaded (50% mass.) coal-water slurry based on Kansk-Achinsk brown coal and distilled water (coal-water slurry fuel – CWSF) with exposure of used water to cavitation-treatment, microwave processing of coal powder, T-900 nanocarbon additions is presented. The study shows that under the conditions of this experiment the thermal physical properties of CWSF are most affected by the use of cavitation-activated water.

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Держатели документа:
Siberian Federal University, Svobodnyy Ave 79, Krasnoyarsk 660049, Russia
Federal Research Center «Krasnoyarsk Research Center (Russian Academy of Sciences, Siberian Branch») L.V. Kirensky Institute of Physics, SB RAS, Akademgorodok 50 bld. 38, Krasnoyarsk 660036, Russia

Доп.точки доступа:
Kashkina, L. V.; Stebeleva, O. P.; Petrakovskaya, E. A.; Петраковская, Элеонора Анатольевна; Cherepakhin, A. V.; Черепахин, Александр Владимирович; Carbon: Fundamental Problem, Material Science, Technology - International Conference(11th ; 29 May - 1 June 2018 ; Troitsk, Moscow)
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Electrical and magnetic properties of nanodiamond and pyrocarbon composites / N. I. Kiselev [et al.] // Russ. J. Gen. Chem. - 2013. - Vol. 83, Is. 11. - P. 2173-2181, DOI 10.1134/S1070363213110376 . - ISSN 1070-3632
Аннотация: The electrical and magnetic properties of the nanodiamond composites comprising nanodiamond, pyrolytic carbon, and nanosized pores were studied. The composites are p-type semiconductors and their resistance decreases by 12 orders of magnitude as the pyrocarbon-to-diamond ratio γ increases from 0 to 80 wt %. Evidence for paramagnetic properties of the nanodiamond composites was obtained. The observed properties are explained by increased concentration of surface Tamm states. The paramagnetic properties are explained in terms of the electron spins localized on the nanodiamond surface in the composite.

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Держатели документа:
Russian Acad Sci, Siberian Branch, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
Cent Res Inst Mat Fed Unitary Enterprise, St Petersburg, Russia
Russian Acad Sci, Siberian Branch, Inst Chem & Chem Technol, Krasnoyarsk 660036, Russia
Inst Biophys, Siberian Branch,Russian Acad Sci, Krasnoyarsk, Russia;
Siberian Fed Univ, Youth Open Lab Perspect Res & Technol, Russia

Доп.точки доступа:
Kiselev, N. I.; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Korchagina, S. B.; Petrakovskaya, E. A.; Петраковская, Элеонора Анатольевна; Vasil'ev, A. D.; Васильев, Александр Дмитриевич; Solov'ev, L. A.; Соловьев, Леонид Александрович; Balaev, D. A.; Балаев, Дмитрий Александрович; Bayukov, O. A.; Баюков, Олег Артемьевич; Denisov, I. A.; Денисов, И. А.; Tsegel'Nik, S. S.; Eremin, E. V.; Еремин, Евгений Владимирович; Znak, D. A.; Shaikhutdinov, K. A.; Шайхутдинов, Кирилл Александрович; Shubin, A. A.; Shestakov, N. P.; Шестаков, Николай Петрович; Volkov, N. V.; Волков, Никита Валентинович; Gordeev, S. K.; Belobrov, P. I.; Белобров, Петр Иванович
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Electron Magnetic Resonance in nanoparticles of 3-d and 5-d metals formation in nanocarbon powders [Text] / Petrakovskaya E., Isakova V., Velikanov D., Isakov V. // EUROMAR 2008 Conference : St.Peterbsburg, 2008, [6-11 July]. - 2008. - p. 224

Доп.точки доступа:
Petrakovskaya, E. A.; Петраковская, Элеонора Анатольевна; Isakova, V. G.; Исакова, Виктория Гавриловна; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Isakov, V.; "Магнитный резонанс для будущего", Международный конгресс(2008 ; июль ; Санкт-Петербург); "Euromar", International Conference(2008 ; Jul. ; St.-Peterburg)
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Electron Paramagnetic Resonance and Gd3+ Clustering in the{xGd203-(1-x)(La203-Al203-B203-SiO2-GeO2)} Glasses [Text] / J. Kliava, R. Berger, A. A. Potseluyko [et al.] // The Physics of Metals and Metallography. - 2006. - Vol. 102, Suppl. 1. - P. S39-S41DOI 10.1134/S0031918X06140092. - Библиогр.: 6. - Krasnoyarsk Regional Science Foundation (grant no. 12F0045C).
Аннотация: A multicomponent glass system 20La2O3–22Al2O3–23B23–35(SiO2+ GeO2) in which part of La2O3is substituted by Gd2O3 in different concentrations has been studied by EPR. The EPR spectra show the presence of clustering at higher Gd contents. At low temperatures, the cluster-related resonance signal is altered in shape, indicating the appearance of a magnetic anisotropy field.

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Держатели документа:
CPMOH, Üniversite Bordeaux–I, 33405 Talence Cedex, France
Kirensky Institute of Physics, Siberian Division, Russian Academy of Sciences, Krasnoyarsk 660036, Russia
Vavilov State Optical Institute, St. Petersburg, 199034 Russia

Доп.точки доступа:
Kliava, J.; Berger, R.; Potseluyko, A. A.; Поцелуйко, Анатолий Артёмович; Edelman, I. S.; Petrakovskaya, E. A.; Петраковская, Элеонора Анатольевна; Zarubina, T.
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10.

EMR spectra of borat glasses containing two types of transition ion simultaneously [Text] / Kliava J., Marbeuf A., Edelman I., Ivanova O., Petrakovskaja E., Ivantsov R. // EUROMAR 2008 Conference : St.Peterbsburg, 2008, [6-11 July]. - 2008. - p. 221

Доп.точки доступа:
Kliava, J.; Marbeuf, A.; Edelman, I. S.; Эдельман, Ирина Самсоновна; Ivanova, O. S.; Иванова, Оксана Станиславовна; Petrakovskaja, E. A.; Петраковская, Элеонора Анатольевна; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; "Магнитный резонанс для будущего", Международный конгресс(2008 ; июль ; Санкт-Петербург); "Euromar", International Conference(2008 ; Jul. ; St.-Peterburg)
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11.

Ensembles of γ-Fe2O3 nanoparticles formed during devitrification of borate glasses / O. S. Ivanova [et al.] // Solid State Phenom. : Selected, peer reviewed papers. - 2014. - Vol. 215: Trends in Magnetism: Nanomagnetism (EASTMAG-2013). - P. 173-178, DOI 10.4028/www.scientific.net/SSP.215.173. - Cited References: 16 . - ISSN 978-30383. - ISSN 1662-9779
Кл.слова (ненормированные):
Magnetic nanoparticles -- Magneto-optical properties
Аннотация: Structural, magnetic and magneto-optical properties of borate glasses co-doped with Fe and the lager radius ions are presented. Maghemite, ?-Fe2O3, nanoparticles arise in the glasses as a result of their thermal treatment in different regimes. Magnetization FC and ZFC temperature dependences demonstrate the superparamagnetic behavior of the particles with the blocking temperature below the room temperature. The EMR spectra measurements revealed a significant anisotropy with a large contribution of the nanoparticles' surface anisotropy. The FR maximum centered near 700 nm is a characteristic feature of the investigated glasses. © (2014) Trans Tech Publications, Switzerland.

Доп.точки доступа:
Ovchinnikov, S. G. \ed.\; Овчинников, Сергей Геннадьевич; Samardak, A. \ed.\; Ivanova, O. S.; Иванова, Оксана Станиславовна; Edelman, I. S.; Эдельман, Ирина Самсоновна; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Petrakovskaja, E. A.; Петраковская, Элеонора Анатольевна; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Trofimova, N. N.; Zubavichus, Y. V.; Euro-Asian Symposium "Trends in MAGnetism": Nanomagnetism(5 ; 2013 ; sept. ; 15-21 ; Vladivostok)
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12.

Ensembles OF[[d]]γ[[/d]]-Fe[[d]]2[[/d]]O[[d]]3[[/d]] nanoparticles formed during devitrification of borate glasses [Текст] / O. S. Ivanova [и др.] // V Euro-Asian simposium "Trend in MAGnetism": Nanomagnetism : abstracts. - Vladivostok : FEFU, 2013. - P138 . - ISBN 978-5-7444-3124-2

Доп.точки доступа:
Ivanova, O. S.; Иванова, Оксана Станиславовна; Edelman, I. S.; Эдельман, Ирина Самсоновна; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Petrakovskaya, E. A.; Петраковская, Элеонора Анатольевна; Великанов, Дмитрий Анатольевич; Velikanov, D. A.; Trofimova, N. N.; Трофимова, Н. Н.; Zubavichus, Y. V.; Зубавичус, Я. В.; Euro-Asian Symposium "Trends in MAGnetism": Nanomagnetism(5 ; 2013 ; Sept. ; 15-21 ; Vladivostok)
}
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13.

EPR Study of Solid Solutions Based on the Compound ScF3 [Text] / Voronov V.N., Petrakovskaya E.A., Alexandrovskaya A.V. // Functional Materials. - 2010. - Vol. 17, Is. 3. - P324-328

Доп.точки доступа:
Voronov, V. N.; Воронов Владимир Николаевич; Petrakovskaya, E. A.; Петраковская Элеонора Анатольевна; Alexandrovskaya, A. V.
}
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14.

Ferrite nanoparticles in borate glass matrix: structure and magnetic properties / N. N. Trofimova [et al.] // Moscow Int. Symp. on Magnet. (MISM-2014) : Book of abstracts. - 2014. - Ст. 2PO-I1-2. - P. 745 . - ISBN 978-5-91978-025-0

Book of abstracts

Доп.точки доступа:
Trofimova, N. N.; Zubavichus, Y. V.; Edelman, I. S.; Эдельман, Ирина Самсоновна; Ivanova, O. S.; Иванова, Оксана Станиславовна; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Petrakovskaya, E. A.; Петраковская, Элеонора Анатольевна; Zaikovskii, V. I.; Московский государственный университет им. М.В. Ломоносова; Moscow International Symposium on Magnetism(6 ; 2014 ; 29 June-3 July ; Moscow)
}
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15.

Ferritization of industrial waste water and microbial synthesis of iron-based magnetic nanomaterials from sediments / M. I. Teremova [et al.] // Environ. Prog. Sustain. Energy. - 2016. - Vol. 35, Is. 5. - P. 1407-1414, DOI 10.1002/ep.12368. - Cited References:26. - The work has been carried out with support of grant of RFFI No 10-08-01278 and DST-ILTP-A.2.61 under DST-RFBR Indo-Russian Long term Collaborative Project. Authors are grateful to P.P. Pustoshilov, N.M. Kuchin, O.A. Bayukov, A.P. Puzyr and Lobova T.I. for assistance in experiment performance and valuable remarks. . - ISSN 1944-7442. - ISSN 1944-7450

РУБ Green & Sustainable science & Technology + Engineering, Environmental + Engineering, Chemical + Engineering, Industrial + Environmental Sciences
Рубрики:
ACIDITHIOBACILLUS FERROOXIDANS CELLS
POT MULTICOMPONENT SYNTHESIS
Кл.слова (ненормированные):
industrial wastes -- ferritization -- bacteria -- magnetic -- ferrihydrite -- nanoparticles
Аннотация: The precipitation of iron and associated heavy metals in industrial waste water and in model solution using ferritization and aerobic bacterial culture was investigated. Magnetic sediments extractable by magnetic separation (specific saturation magnetization of 16–36.8 G cm3/g) were produced by precipitation of iron by ferritization method at рН (8–10) and 60–80°С for 15–30 min. Nanoparticles of ferrihydrite or ferric hydroxide doped with associated metals (Co, Ni) were produced under precipitation of ferric iron in model solution with bacteria at the temperature 26–34°С. The radii of synthesized particles are 1–5 nm and nanoparticles of ferrihydrite are superparamagnetic in both un-doped and doped (Co, Ni, Zn) sets. Dispersed structure of biogenic nanoparticle sols, their magnetic and other properties were studied by atomic force microscopy, X-ray small-angle scattering, X-ray diffraction, electron magnetic resonance, Mössbauer and X-ray photoelectron spectroscopy.

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Держатели документа:
Russian Acad Sci, Siberian Branch, Krasnoyarsk Sci Ctr, Krasnoyarsk, Russia.
Russian Acad Sci, Inst Phys, Siberian Branch, Krasnoyarsk, Russia.
Russian Acad Sci, Boreskov Inst Catalysis & Chem Technol, Siberian Branch, Novosibirsk, Russia.
Russian Acad Sci, Inst Catalysis, Siberian Branch, Novosibirsk, Russia.
Siberian Fed Univ, Krasnoyarsk, Russia.
Natl Met Lab, CSIR, Jamshedpur, Bihar, India.

Доп.точки доступа:
Teremova, M. I.; Petrakovskaya, E. A.; Петраковская, Элеонора Анатольевна; Romanchenko, A. S.; Tuzikov, F. V.; Gurevich, Y. L.; Tsibina, O. V.; Yakubailik, E. K.; Якубайлик, Эдуард Константинович; Abhilash; RFFI [10-08-01278]; DST-RFBR Indo-Russian Long term Collaborative Project [DST-ILTP-A.2.61]
}
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16.

    FMR and TEM Studies of Co and Ni Nanoparticles Implanted in the SiO2 Matrix / I. S. Edelman [et al.] // Appl. Magn. Reson. - 2011. - Vol. 40, Is. 3. - P363-375, DOI 10.1007/s00723-011-0218-4. - Cited Reference Count: 51. - Гранты: The work was supported in part by the Russian Foundation for Basic Research, grant no. 11-02-00972-a, Ministry of Education and Science of the Russian Federation, Federal Target Program "Scientific and scientific-pedagogical personnel of innovative Russia'', contract no. 02.740.11.0797, and State Program "Development of the Scientific Potential of the Higher Education School'', project no. 2.1.1/6038. S.M. Zharkov acknowledges the financial support of the Russian government contract no. 02.740.11.0568. The electron microscopy investigations were carried out at the Joint Center of the Siberian Federal University. - Финансирующая организация: Russian Foundation for Basic Research [11-02-00972-a]; Ministry of Education and Science of the Russian Federation [02.740.11.0797]; State Program "Development of the Scientific Potential of the Higher Education School'' [2.1.1/6038]; Russian government [02.740.11.0568] . - MAY. - ISSN 0937-9347. - ISSN 1613-7507
Рубрики:
FERROMAGNETIC-RESONANCE
   MAGNETIC-PROPERTIES
   THIN-FILMS
   COBALT NANOPARTICLES
   ION-IMPLANTATION
   FINE PARTICLES
   GRANULAR FILMS
   ANISOTROPY
   POLYIMIDES
   RUTILE
Кл.слова (ненормированные):
energy dispersive x ray spectroscopy -- face-centered cubic structure -- fused silica plates -- g factors -- hexagonal close packing -- high dose -- high-dose implantation -- implantation dose -- implanted samples -- line shape -- magnetic parameters -- matrix -- metal nanoparticles -- ni nanoparticles -- nonsymmetric -- out-of-plane -- room temperature -- spherical shape -- subsurface layer -- tem -- temperature dependence -- thin magnetic films -- uniaxial magnetic anisotropy -- cobalt -- fused silica -- magnetic anisotropy -- nanoparticles -- silica -- silicon compounds -- transmission electron microscopy -- x ray spectroscopy -- ferromagnetic resonance
Аннотация: Fused silica plates have been implanted with 40 keV Co+ or Ni+ ions to high doses in the range of (0.25-1.0) x 10(17) ions/cm(2), and magnetic properties of the implanted samples have been studied with ferromagnetic resonance (FMR) technique supplemented by transmission electron microscopy, electron diffraction and energy dispersive X-ray spectroscopy. The high-dose implantation with 3d-ions results in the formation of cobalt and nickel metal nanoparticles in the irradiated subsurface layer of the SiO2 matrix. Co and Ni nanocrystals with hexagonal close packing and face-centered cubic structures have a spherical shape and the sizes of 4-5 nm (for cobalt) and 6-14 nm (for nickel) in diameter. Room-temperature FMR signals from ensembles of Co and Ni nanoparticles implanted in the SiO2 matrix exhibit an out-of-plane uniaxial magnetic anisotropy that is typical for thin magnetic films. The dose and temperature dependences of FMR spectra have been analyzed using the Kittel formalism, and the effective magnetization and g-factor values have been obtained for Co- and Ni-implanted samples. Nonsymmetric FMR line shapes have been fitted by a sum of two symmetrical curves. The dependences of the magnetic parameters of each curve on the implantation dose and temperature are presented.

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Держатели документа:
Siberian Fed Univ, Krasnoyarsk 660041, Russia
Russian Acad Sci, Siberian Branch, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
Zavoisky Physical-Technical Institute,Russian Academy of Sciences

Доп.точки доступа:
Edelman, I. S.; Эдельман, Ирина Самсоновна; Petrakovskaja, E. A.; Петраковская, Элеонора Анатольевна; Petrov, D. A.; Петров, Дмитрий Анатольевич; Zharkov, S. M.; Жарков, Сергей Михайлович; Khaibullin, R. I.; Nuzhdin, V. I.; Stepanov, A. L.
}
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17.

Formation and evolution of magnetic nanoparticles in borate glass simultaneously doped with Fe and Mn oxides / J. . Kliava [et al.] // J. Appl. Phys. - 2008. - Vol. 104, Is. 10. - Ст. 103917, DOI 10.1063/1.3021289. - Cited References: 37. - A financial support from the Russian Foundation for Basic Research (RFBR)-CNRS (Grant No. 07-02-92174) is highly appreciated. R. Ivantsov is grateful to the Russian Science Support Foundation. Y. Yeshurun acknowledges the support of the Israel Scienc Foundation (ISF). . - ISSN 0021-8979

РУБ Physics, Applied
Рубрики:
COBALT FERRITE PARTICLES
   SUPERPARAMAGNETIC RESONANCE
   GAMMA-FE2O3 NANOPARTICLES
   MATRIX
   SIZE
   SYSTEMS
Кл.слова (ненормированные):
aluminium compounds -- borate glasses -- coercive force -- Faraday effect -- heat treatment -- iron compounds -- magnetic hysteresis -- magnetic particles -- magnetic susceptibility -- manganese compounds -- Mossbauer effect -- nanoparticles -- paramagnetic materials -- potassium compounds -- remanence -- superparamagnetism -- transmission electron microscopy -- X-ray chemical analysis -- Atomic spectroscopy -- Auger electron spectroscopy -- Crystal structure -- Electric relays -- Electronic medical equipment -- Ferrite -- Ferrites -- Glass -- Heat treatment -- Hysteresis -- Hysteresis loops -- Magnetic properties -- Magnetic resonance measurement -- Magnetic susceptibility -- Magnetism -- Manganese -- Manganese compounds -- Molybdenum -- Nanoparticles -- Optical properties -- Ozone water treatment -- Polydispersity -- Superparamagnetism -- Borate glasses -- Concentration ratios -- Electron magnetic resonances -- Emr spectrums -- Experimental techniques -- Faraday rotations -- Glass compositions -- Glass matrixes -- Glass preparations -- Magnetic measurements -- Magnetic nano particles -- Magnetic orders -- Magnetically ordered systems -- Magneto-optical properties -- Manganese ferrites -- Mean diameters -- Mn oxides -- Phase states -- Polydisperse nanoparticles -- Remnant magnetizations -- Ssbauer spectroscopies -- Superparamagnetic -- Superparamagnetic states -- Thermal treatments -- Variable temperatures -- Magnetic materials
Аннотация: Evolution of the phase state of paramagnetic additions at various stages of synthesis and subsequent thermal treatment of glasses of the system Al(2)O(3)-K(2)O-B(2)O(3) simultaneously doped with Fe(2)O(3) and MnO is studied by means of a combination of experimental techniques: Faraday rotation (FR), electron magnetic resonance (EMR), transmission electron microscopy (TEM), Mossbauer spectroscopy, and magnetic measurements. Both FR and EMR show that magnetically ordered clusters occur already at the first stage of the glass preparation. In particular, for the ratio of the Fe and Mn oxides in the charge close to 3:2, fine magnetic nanoparticles are formed with characteristics similar to those of manganese ferrite. By computer simulating the EMR spectra at variable temperatures, a superparamagnetic nature of these nanoparticles is confirmed and their mean diameter is estimated as approximately 3.2 nm. In the thermally treated glasses larger magnetic nanoparticles are formed, giving rise to FR spectra, characteristic of magnetically ordered systems, and the EMR spectra different from those in as-prepared glasses but also showing superparamagnetic narrowing. The Mossbauer spectroscopy corroborates the manganese ferrite structure of the nanoparticles and indicates their coexistence in the ferrimagnetic and superparamagnetic states. The TEM shows the presence of polydisperse nanoparticles on the background of the glass matrix, and electron diffraction of a selected region containing larger particles indicates a crystal structure close to that of MnFe(2)O(4). Energy-dispersive atomic x-ray spectra confirm that the major part of Fe and Mn introduced to the glass composition is gathered in the particles, with the concentration ratio close to 2:1, characteristic of bulk MnFe(2)O(4). Magnetic hysteresis loops of samples subjected to an additional thermal treatment demonstrate a strong increase in the coercive force, remnant magnetization, and high-field magnetic susceptibility with temperature decrease. The consistent results obtained using various techniques demonstrate that the formation of nanoparticles with characteristics close to those of MnFe(2)O(4) confers to these glasses magnetic and magneto-optical properties typical of substances possessing magnetic order.

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Держатели документа:
[Kliava, J.] Univ Bordeaux 1, CNRS, UMR 5798, CPMOH, F-33405 Talence, France
[Edelman, I.
Ivanova, O.
Ivantsov, R.
Bayukov, O.
Petrakovskaja, E.
Stepanov, S.] RAS, Siberian Branch, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
[Zaikovskiy, V.] RAS, Siberian Branch, Boreskov Inst Catalysis, Novosibirsk 630090, Russia
[Bruckental, I.
Yeshurun, Y.] Bar Ilan Univ, Dept Phys, IL-52900 Ramat Gan, Israel
[Stepanov, S.] SI Vavilov State Opt Inst, St Petersburg 199034, Russia
ИФ СО РАН
CPMOH, Universit? Bordeaux, 1-CNRS UMR 5798, 33405 Talence Cedex, France
Kirensky Institute of Physics, Siberian Branch of RAS, 660036 Krasnoyarsk, Russian Federation
Boreskov Institute of Catalysis, Siberian Branch, RAS, 630090 Novosibirsk, Russian Federation
Department of Physics, Bar-Ilan University, Ramat-Gan 52900, Israel
S. I. Vavilov State Optical Institute, St. Petersburg 199034, Russian Federation

Доп.точки доступа:
Kliava, J.; Edelman, I. S.; Эдельман, Ирина Самсоновна; Ivanova, O. S.; Иванова, Оксана Станиславовна; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Bayukov, O. A.; Баюков, Олег Артемьевич; Petrakovskaja, E. A.; Петраковская, Элеонора Анатольевна; Zaikovskiy, V.; Bruckental, I.; Yeshurun, Y.; Stepanov, S.
}
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18.

Formation, characterization and magnetic properties of maghemite γ-Fe2O3 nanoparticles in borate glasses / I. S. Edelman [et al.] // J. Alloys Compd. - 2015. - Vol. 624. - P. 60-67, DOI 10.1016/j.jallcom.2014.11.059. - Cited References: 25. - This work was supported partly by the Russian Foundation for Basic Research - Russia, Grant No. 14-02-01211-a and by the President of Russia Grant No. NSh-2886.2014.2. This work was performed using the equipment of Unique Scientific Facility "Kurchatov Synchrotron Radiation Source'' supported by the Russian Ministry of Science and Education (project code RFMEFI61914X0002). . - ISSN 0925-8388

РУБ Chemistry, Physical + Materials Science, Multidisciplinary + Metallurgy & Metallurgical Engineering
Рубрики:
SUPERPARAMAGNETIC RESONANCE
   HYSTERESIS LOOPS
   EXCHANGE BIAS
   IONS
   MATRIX
Кл.слова (ненормированные):
Nanostructures -- Crystal structure and symmetry -- Magnetic measurements
Аннотация: A new type of nanocomposite materials based on maghemite, γ-Fe2O3, nanoparticles dispersed in borate glasses co-doped with low contents of iron together with the larger radius element combinations: Y and Bi, or Sm and Pb, or Y and Pb is studied. Nanoparticles arise as a result of heat treatment of the glasses which gives them properties characteristic of magnetically ordered substances. Transmission electron microscopy and XRD show that only one magnetic phase, namely γ-Fe2O3 nanoparticles, occurs in glasses subjected to the thermal treatment at 540 °C during 24 h independently on the doping element nature. At the same time doping element and their concentrations ratio in every combination affect the particles average size and glass magnetic properties, such as magnetization temperature dependences, Faraday rotation value and electron magnetic resonance spectrum characteristics.

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Держатели документа:
RAS, Siberian Branch, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
Siberian Fed Univ, Krasnoyarsk 660036, Russia
NRC Kurchatov Inst, Moscow 123182, Russia
RAS, Siberian Branch, Boreskov Inst Catalysis, Novosibirsk 630090, Russia
Novosibirsk State Univ, Novosibirsk 630090, Russia

Доп.точки доступа:
Edelman, I. S.; Эдельман, Ирина Самсоновна; Ivanova, O. S.; Иванова, Оксана Станиславовна; Petrakovskaja, E. A.; Петраковская, Элеонора Анатольевна; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Tarasov, I. A.; Тарасов, Иван Анатольевич; Zubavichus, Y. V.; Trofimova, N. N.; Zaikovskii, V. I.; Russian Foundation for Basic Research - Russia [14-02-01211-a]; President of Russia [NSh-2886.2014.2]; Russian Ministry of Science and Education [RFMEFI61914X0002]
}
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19.

    Hydrodynamic dispersion of calcium aluminosilicate from technogenic and nonmetallic material / L. V. Kashkina [et al.] // J. Sib. Fed. Univ. Eng. Technol. - 2014. - Vol. 7, Is. 1. - P. 3-12 ; Журн. СФУ. Сер. "Техника и технологии"
   Перевод заглавия: Гидродинамическое диспергирование кальций-алюмосиликатных материалов из техногенного и нерудного сырья
Кл.слова (ненормированные):
hydrodynamic dispersion -- cavitation -- crystal ceramic foam -- porous glass material -- гидродинамическое диспергирование -- кавитация -- зола -- пеноматериал -- пористая стеклокерамика
Аннотация: Physicochemical properties of two calcium aluminosilicate materials after reducing in the hydrodynamic rotary generator in supercavitation mode were studied. The samples are the crystal ceramic foam based on Kansko-Achinsk lignite-ash and the porous glass material obtained from low-manganese nonmetallic feed. X-ray phase analysis, EPR-method, NPR-method (the Mossbauer Effect) and optical microscopy were used. It was found that the material is changing its stucrure in a hydrodynamic dispersion process caused by high-cavitation. The nature of the changes depends on its initial state.
Изучены физико-химические свойства двух кальций-алюмосиликатных материалов после измельчения в гидродинамическом генераторе роторного типа в режиме суперкавитации. Исследованы образцы – кристаллическая пенокерамика на основе зол бурых Канско-Ачинских углей и пористый стекломатериал, полученный из нерудного сырья с низким содержанием марганца. Для анализа были использованы методы РФА, ЭМР, ЯГР (эффект Мёссбауэра), оптическая микроскопия. Показано, что в процессе гидродинамического диспергирования за счет высокоэнергетического кавитационного воздействия в материалах происходят глубокие структурные изменения. Получено, что характер изменений зависит от исходного состояния исследуемого материала.

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Держатели документа:
Siberian Federal University, 79 Svobodny, Krasnoyarsk, 660041, Russia
L.V. Kirensky Institute of Physics SB RAS, 50/38 Akademgorodok, Krasnoyarsk, 660036, Russia

Доп.точки доступа:
Kashkina, L. V.; Stebeleva, O. P.; Emelyanova, T. Y.; Petrakovskaya, E. A.; Петраковская, Элеонора Анатольевна; Bayukov, O. A.; Баюков, Олег Артемьевич

}
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20.

Identification of ε-Fe2O3 nano-phase in borate glasses doped with Fe and Gd / O. S. Ivanova [et al.] // J. Magn. Magn. Mater. - 2016. - Vol. 401. - P. 880-889, DOI 10.1016/j.jmmm.2015.10.126. - Cited References: 40. - This work was supported partly by the Russian Foundation for Basic Research, Grants No 14-02-01211-a and by the President of Russia Grant No. NSh-2886.2014.2. Authors are grateful to G.A. Bukhtiyarova and U.N. Martyanov for the assistance in the ε-Fe2O3 nanoparticles prepared by a wet chemical pore filling impregnation method and for the discussion of the obtained results . - ISSN 0304-8853

РУБ Materials Science, Multidisciplinary + Physics, Condensed Matter
Рубрики:
MAGNETIC-PROPERTIES
   IRON-OXIDE
   NANOPARTICLES
   CERAMICS
   CRYSTAL
   PARTICLES
   SURFACE
Кл.слова (ненормированные):
Magnetic nanoparticles -- ε-Fe2O3 -- Magnetic circular dichroism -- Electron magnetic resonance
Аннотация: A new type of magnetic nanoparticles was revealed in borate glasses co-doped with low contents of iron and gadolinium. Structure and magnetic properties of the particles differ essentially from that of the α-Fe2O3, γ-Fe2O3, or Fe3O4 nanoparticles which were detected earlier in similar glass matrices. Transmission electron microscopy including STEM-HAADF and EDX, synchrotron radiation-based XRD, static magnetic measurements, magnetic circular dichroism, and electron magnetic resonance studies allow referring the nanoparticles to the iron oxide phase-ε-Fe2O3. Analysis of the data set has shown that it is Gd atoms that govern the process of nanoparticles' nucleation and its incorporation into the particles in different proportions can be used to adjust their magnetic and magneto-optical characteristics. © 2015 Elsevier B.V.

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Держатели документа:
L.V. Kirensky Institute of Physics, Siberian Branch of RAS, Krasnoyarsk, Russian Federation
Siberian Federal University, Krasnoyarsk, Russian Federation
NRC Kurchatov Institute, Moscow, Russian Federation
Boreskov Institute of Catalysis, Siberian Branch of RAS, Novosibirsk, Russian Federation
Novosibirsk State University, Novosibirsk, Russian Federation
Vavilov State Optical Institute, All-Russia Research Center, Petersburg, Russian Federation

Доп.точки доступа:
Ivanova, O. S.; Иванова, Оксана Станиславовна; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Edelman, I. S.; Эдельман, Ирина Самсоновна; Petrakovskaja, E. A.; Петраковская, Элеонора Анатольевна; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Zubavichus, Y. V.; Zaikovskii, V .I.; Stepanov, S. A.
}
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