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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mel'nikova S. V., Molokeev M. S., Laptash N. M., Misyul S. V.
Заглавие : A non-typical sequence of phase transitions in (NH4)3GeF7: optical and structural characterization
Коллективы : RFBR [15-02-02009 a]
Место публикации : Dalton Trans.: Royal Society of Chemistry, 2016. - Vol. 45, Is. 12. - P.5321-5327. - ISSN 1477-9226, DOI 10.1039/c5dt04907e. - ISSN 1477-9234(eISSN)
Примечания : Cited References:25. - The reported study was partially supported by RFBR, research project no. 15-02-02009 a
Предметные рубрики: Crystal-structure
Powder diffraction
NH4F
Fluorination
Аннотация: Single crystals of germanium double salt (NH4)3GeF7 = (NH4)2GeF6·NH4F = (NH4)3[GeF6]F were grown and studied by the methods of polarization optics and X-ray diffraction. The birefringence Δn = (no − ne), the rotation angle of the optical indicatrix ϕ(T) and unit cell parameters were measured in the temperature range 100–400 K. Three structural phase transitions were found at the temperatures: T1↓ = 279.2 K (T1↑ = 279.4 K), T2↑ = 270 K (T2↓ = 268.9 K), T3↓ = 218 K (T3↑ = 227 K). An unusual sequence of symmetry transformations with temperature change was established: P4/mbm (Z = 2) (G1) ↔ Pbam (Z = 4) (G2) ↔ P21/c (Z = 4) (G3) ↔ Pa (Z = 8) (G4). The crystal structures of different phases were determined. The experimental data were additionally interpreted by a group-theoretical analysis of the complete condensate of order parameters taking into account the critical and noncritical atomic displacements. Strengthening of the N–H⋯F hydrogen bonds can be a driving force of the observed phase transitions.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Aleksandrov K. S., Mel'nikova S. V., Kruglik A. I.
Заглавие : X-ray and optic investigations of phase-transition in cslicro4 crystal
Место публикации : Ferroelectrics: Gordon Breach SCI Publ LTD, 1988. - Vol. 81, Is. 1. - P.153-156. - ISSN 0015-0193, DOI 10.1080/00150198808008833
Примечания : Cited References: 2
Аннотация: The study of optical properties and X-ray investigations were carried out in CsLiCrO4crystal. It was found (is discussed) an unusual 4 temperature dependence of optical indicatrix rotation and monoclinic angles.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mel'nikova S. V., Aleksandrov K. S., Anistratov A. T., Beznosikov B. V.
Заглавие : Birefringence and structural phase transitions in ABCl//3-type crystals
Место публикации : Sov. Phys. Solid State. - 1977. - Vol. 19, Is. 1. - P.18-20; Phys. Solid State
Ключевые слова (''Своб.индексиров.''): electrooptical effects--crystals
Аннотация: The refractive indices and birefringence of CsPbCl//3, TlMnCl//3, and CsSrCl//3 were determined a wide temperature range, which included phase transition points. Relatively high values of the photoelastic and acoustooptic characteristics were obtained: the th acoustooptic figure of merit M//2 was 12 multiplied by (times) 10** minus **1**8 cgs units for TlMnCl//3 and 98 multiplied by (times) 10** minus **1**8 cgs units for CsPbCl//3. A strong influence of partial Sr for Ca substitution on the properties and transition temperatures was observed. A phenomenological theory was used to analyze the relationship between the birefringence anomalies and the theromodynamic parameters of the transitions. A comparison was made with KMnF//3 and SrTiO//3.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Aleksandrov K. S., Anistratov A. T., Mel'nikova S. V., Zinenko V. I., Shabanova L. A., Beznosikov B. V.
Заглавие : Birefringence, twinning and structural phase transitions in ABCl3 single crystals
Коллективы : International meeting on ferroelectricity
Место публикации : Ferroelectrics. - 1978. - Vol. 20, Spesial issue. - P.305-307. - DOI 10.1080/00150197808237245
Аннотация: The temperature investigations of birefringence, twinning and elasticity of CsPbCl3, CsSrCl3, TlMnCl3, RbCdCl3, CsCaCl3 and RbMnCl3, were carried out. A group-theoretical analysis is made and the description of phase transitions is given.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Chekanova L. A., Denisova E. A., Mel'nikova S. V., Iskhakov R. S.
Заглавие : Composite magnetic materials based on porous templates with different pores morphology: synthesis and magnetic properties
Коллективы : Euro-Asian Symposium "Trends in MAGnetism": Nanomagnetism
Место публикации : V Euro-Asian simposium "Trend in MAGnetism": Nanomagnetism: abstracts. - Vladivostok: FEFU, 2013. - С. 169. - ISBN 978-5-7444-3124-2
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Bogdanov E. V., Pogoreltsev E. I., Gorev M. V., Mel'nikova S. V., Molokeev M. S., Laptash N. M., Flerov I. N.
Заглавие : Effect of the size of the central atom on the stability of crystalline phases in solid solutions (NH4)3TixSn1-xF7
Колич.характеристики :8 с
Место публикации : J. Solid State Chem. - 2023. - Vol. 328. - Ст.124373. - ISSN 00224596 (ISSN), DOI 10.1016/j.jssc.2023.124373. - ISSN 1095726X (eISSN)
Примечания : Cited References: 20. - The study was supported by a grant from the Russian Science Foundation № 23-22-00115, https://rscf.ru/project/23-22-00115/X-ray and dilatometric data and SEM images were obtained using the equipment of the Krasnoyarsk Regional Center for Collective Use of the Federal Research Center — Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of Sciences. We are grateful to Dr. A.V. Shabanov for examination of the SEM images
Аннотация: The effect of a change in internal pressure as a result of partial substitution of the central atom on the realization and stability of the initial and distorted crystalline phases in (NH4)3TixSn1-xF7 solid solutions has been studied. It was found that at a Ti concentration in the range of x = 0.15–0.40, the reconstructive transition Pm-3m ↔ Pa-3 is transformed into a sequence of phase transitions Pm-3m ↔ P4/mbm ↔ P4/mnc ↔ Pa-3. In the (NH4)3Ti0.15Sn0.85F7 solid solution, the first-order phase transition between two cubic phases at T0 = 352 K is characterized by a significant volume jump δ(ΔV/V0) ≈ 1 %, comparable with that in (NH4)3SnF7. An increase of the Ti concentration leads to a strong decrease in the stability of the Pm-3m cubic phase: the first tetragonal P4/mbm phase appears in (NH4)3Ti0.4Sn0.6F7 at T0 = 400 K, which proves the existence of the predicted high-temperature cubic phase in (NH4)3TiF7. In solid solutions, a decrease in birefringence and entropy of phase transitions was observed in comparison with the initial compounds with Sn and Ti as central atoms. The role of critical parameters (unit cell volume, temperature, external pressure) in the formation of cubic and distorted phases is discussed.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Pogoreltsev E. I., Mel'nikova S. V., Kartashev A. V., Molokeev M. S., Gorev M. V., Flerov I. N., Laptash N. M.
Заглавие : Ferroelastic phase transitions in (NH4)2TaF7
Место публикации : Phys. Sol. St.: Pleiades Publishing, 2013. - Vol. 55, Is. 3. - P.611-618. - DOI 10.1134/S1063783413030232
Аннотация: The heat capacity, unit cell parameters, permittivity, optical properties, and thermal expansion of the (NH4)2TaF7 compound with a seven coordinated anion polyhedron have been measured. It has been found that the compound undergoes two successive phase transitions with the symmetry change: tetragonal (T1 = 174 K) orthorhombic (T2 = 156 K) tetragonal. The ferroelastic nature of structural transformations has been established, and their entropy and susceptibility to hydrostatic pressure have been determined.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Flerov I. N., Kartashev A. V., Mel'nikova S. V.
Заглавие : Calorimetric and optical studies of orthorhombic and cubic CsLiCrO4 crystals
Разночтения заглавия :авие SCOPUS: Calorimetric and optical studies of orthorhombic and cubic CsLiCrO 4 crystals
Место публикации : Phys. Solid State: MAIK NAUKA/INTERPERIODICA/SPRINGER, 2006. - Vol. 48, Is. 11. - P2171-2176. - ISSN 1063-7834, DOI 10.1134/S1063783406110242
Примечания : Cited References: 23
Предметные рубрики: PHASE-TRANSITIONS
X-RAY
NH4LISO4
ALPHA
Аннотация: Careful calorimetric and polarization optical studies of a metastable cubic modification of a CsLiCrO4 crystal (space group (F43m)) are performed. Anomalies of the heat capacity indicative of structural distortions at 92.4 and 69.1 K were revealed, and the values of the thermodynamic parameters of the phase transitions were determined. The crystal twinning in the intermediate phase was studied. A comparative analysis of the phase transitions occurring in a series of ALiMO(4) crystals (A=NH4, Cs; M=S, Cr, Mo, W) was performed. First studies of the monotropic structural transformation F43m - Pmcn and the enantiotropic phase transition Pmcn reversible arrow P112(1)/n were carried out using scanning calorimetry, and the thermodynamic parameters of these transitions were determined.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Krylov A. S., Goryainov S. V., Laptash N. M., Vtyurin A. N., Mel'nikova S. V., Krylova S. N.
Заглавие : Influence of the molecular groups ordering on structural phase transitions in (NH4)2WO2F4 crystal
Место публикации : Cryst. Growth Des.: American Chemical Society, 2014. - Vol. 14, Is. 1. - P.374-380. - ISSN 1528-7483, DOI 10.1021/cg400899m. - ISSN 1528-7505
Примечания : Cited References: 27. - This work was partly supported by the Russian Foundation for the Basic Research project no. 12-02-00056, no. 13-02-00825, and integration project SB RAS no. 28, SS-4828.2012.2.Published as part of the Crystal Growth & Design virtual special issue Anion-controlled New Inorganic Materials.
Предметные рубрики: RAMAN-SCATTERING
NEUTRON-SCATTERING
SOLID-STATE
OXYFLUORIDES
DISORDER
POLAR
ANION
Аннотация: Phase transitions of the (NH4)2WO2F 4 crystal were studied by Raman spectroscopy in the range from 10 to 350 K. The mechanism of two phase transitions at T1 = 201 and T 2 = 160 K was proposed. The significant spectra changes occur in the range corresponding to the W-O vibrations. The first temperature phase transition is due to the ordering of the quasi-octahedral groups [WO 2F4]2- and partial ordering of ammonium groups. Experimental data allow for attributing the first (T1 = 201 K) phase transition to the first order close to the tricritical point. The noticeable changes of the Raman spectrum have been found in the range corresponding to the ammonium vibrations below the temperature T2. The second phase transition is associated with the further ordering of ammonium groups. Room temperature (296 K) experiments have been carried out under high hydrostatic pressure up to 10 GPa. Above 2 GPa, new spectral features appear, allowing for the assumption of the existence of a new high-pressure phase of (NH 4)2WO2F4, which is mainly connected with ordering of the [WO2F4]2- quasi-octahedral groups.
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Bogdanov E. V., Pogoreltsev E. I., Mel'nikova S. V., Gorev M. V., Flerov I. N., Molokeev M. S., Kartashev A. V., Kocharova A. G., Laptash N. M.
Заглавие : Investigation into phase diagrams of the fluorine–oxygen system: ferroelastic–antiferroelectric (NH4)2WO2F4–(NH4)2MoO2F4
Место публикации : Phys. Sol. St.: Pleiades Publishing, 2013. - Vol. 55, Is. 2. - P.409-418. - DOI 10.1134/S1063783413020042
Аннотация: Thermal, physical, structural, optical, and dielectric investigations have been performed for oxy- fluoride solid solutions (NH4)2W1–xMoxO2F4 (x = 0, 0.1, 0.2, 0.3, 0.4, 0.6, 0.8, 1). The character of the influence of the chemical and hydrostatic pressures on the stability of the parent (space group Cmcm) and dis& torted ferroelastic and antiferroelectric phases has been determined by analyzing the temperature–pressure, unit cell volume–composition, and temperature–composition phase diagrams. The specific features of the nature and mechanism of the phase transitions have been discussed using the available data on the structural, entropy, and dielectric parameters.
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11.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mel'nikova S. V., Isaenko L. I., Goloshumova A. A., Lobanov S. I.
Заглавие : Investigation of the ferroelastic phase transition in the SrMgF4 pyroelectric crystal
Коллективы : Council on Grants from the Russian Federation for Support of Leading Scientific Schools [NSh-4828.2012.2]; Siberian Branch of the Russian Academy of Sciences within the Interdisciplinary Integration Project of Basic Research [28]
Место публикации : Phys. Solid State: MAIK Nauka-Interperiodica / Springer, 2014. - Vol. 56, Is. 4. - P.757-760. - ISSN 1063-7834, DOI 10.1134/S1063783414040192. - ISSN 1090-6460
Примечания : Cited References: 8. - This study was supported by the Council on Grants from the President of the Russian Federation for Support of Leading Scientific Schools (project no. NSh-4828.2012.2) and the Siberian Branch of the Russian Academy of Sciences within the Interdisciplinary Integration Project of Basic Research no. 28.
Предметные рубрики: BaMnF4
Аннотация: A SrMgF4 compound has been synthesized and a high optical-quality crystal has been grown. Optical-polarization observations, X-ray diffraction analysis, and the measurement of the birefringence Delta n (i) (t) in the SrMgF4 crystal have been carried out in the temperature range of 90-1200 K. A second-order improper ferroelastic phase transition accompanied by birefringence anomalies and the symmetry change P112(1) (Z = 12) a dagger" Cmc2(1) (Z = 4) has been discovered at T (0) = 478 +/- 1 K. The crystal remains pyroelectric in both phases. Considerable contributions of the fluctuations of the order parameter have been observed in the temperature ranges of (T (0) - T) 15 K and (T - T (0)) 60 K.
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12.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Isaenko L. I., Mel'nikova S. V., Merkulov A. A., Pashkov V. M., Tarasova A. Y.
Заглавие : Investigation of the influence of gradual substitution K a dagger" Rb on the structure and phase transition in K (x) Rb1-x Pb2Br5 solid solutions
Коллективы : President of the Russian Federation [NSh-1011.2008.2]
Разночтения заглавия :авие SCOPUS: Investigation of the influence of gradual substitution K - Rb on the structure and phase transition in K x Rb1 - X Pb 2Br5 solid solutions
Место публикации : Phys. Solid State: MAIK NAUKA/INTERPERIODICA/SPRINGER, 2009. - Vol. 51, Is. 3. - P589-592. - ISSN 1063-7834, DOI 10.1134/S1063783409030251
Примечания : Cited References: 5. - This study was supported by the Council on Grants from the President of the Russian Federation for the Support of Leading Scientific Schools ( grant no. NSh-1011.2008.2).
Предметные рубрики: CRYSTAL
Аннотация: Single crystals of K (x) Rb1 - x Pb2Br5 solid solutions have been grown and investigated using X-ray diffraction and polarized light microscopy in the temperature range 270-640 K. The regions of existence of the tetragonal (I4/mcm) and monoclinic (P2(1)/c) phases have been determined. It has been demonstrated that the partial introduction of rubidium into KPb2Br5 leads to an increase in the temperature of the ferroelastic phase transition (P2(1)/ca dagger"mmm), so that it approaches the melting temperature. In the solid solutions with x a parts per thousand 0.4-0.5, the temperature region of existence of the orthorhombic phase is narrowed to a parts per thousand 1-2 K. It has been revealed that an increase in the potassium content in the material results in a considerable increase in the incorporation coefficient of Er3+ ions.
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13.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mel'nikova S. V., Kartashev A. V., Grankina V. A., Flerov I. N.
Заглавие : Investigation of the reconstructive phase transition between metastable (alpha) and stable (beta) modifications of the NH4LiSO4 crystal
Разночтения заглавия :авие SCOPUS: Investigation of the Reconstructive Phase Transition between Metastable (α) and Stable (β) Modifications of the NH4LiSO 4 Crystal
Место публикации : Phys. Solid State: AMER INST PHYSICS, 2003. - Vol. 45, Is. 8. - P1572-1578. - ISSN 1063-7834, DOI 10.1134/1.1602898
Примечания : Cited References: 13
Предметные рубрики: AMMONIUM LITHIUM-SULFATE
LINH4SO4
TEMPERATURE
Аннотация: Crystals of ammonium lithium sulfate NH4LiSO4 in alpha and beta modifications are studied, and conditions of their nucleation and growth are determined. The alpha modification of NH4LiSO4 and alpha--beta phase transitions are investigated using polarized light microscopy, x-ray diffraction, and differential scanning calorimetry in the temperature range 80-530 K. It is found that, depending on the conditions of growth and storage, there exist two temperature ranges (T(alpha--beta)approximate to340-350 and approximate to440-450 K) in which the crystals can undergo an alpha--beta reconstructive phase transition. The enthalpy of this transformation depends on the symmetry of the final phase. In the former case (340-350 K), the reconstructive phase transition leads to rapid destruction of the sample. In the latter case (440-450 K), the crystal structure undergoes a slow transformation (recrystallization) without noticeable distortions. The results obtained indicate that no structural phase transition occurs in the alpha modification of NH4LiSO4 at 250 K. (C) 2003 MAIK "Nauka/Interperiodica".
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14.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mel'nikova S. V., Isaenko L. I., Gorev M. V., Vasil'ev A. D., Lobanov S. I.
Заглавие : Investigation of the structure, physical properties, and phase transition in SrAlF5
Коллективы :
Место публикации : Phys. Solid State: MAIK NAUKA/INTERPERIODICA/SPRINGER, 2010. - Vol. 52, Is. 3. - P509-514. - ISSN 1063-7834, DOI 10.1134/S1063783410030108
Примечания : Cited References: 16. - This study was supported by the Russian Foundation for Basic Research (project no. 07-02-00442) and the Siberian Branch of the Russian Academy of Sciences within the framework of the Interdisciplinary Integration Project No. 34.
Предметные рубрики: CRYSTAL-STRUCTURE
BEHAVIOR
GROWTH
SRAIF5
Аннотация: Crystals of SrAlF5 have been grown by the Bridgman method from the melt and by sintering of the components. Optical polarization studies and measurements of the thermal expansion and birefringence coefficients have been carried out over a wide temperature range. The electromechanical coefficient d (33) has been measured, and the optical second harmonic, dielectric hysteresis loop, and optical quality of the crystal have been assessed. X-ray diffraction investigations have been performed to identify the revealed compounds. It has been demonstrated that the SrAlF5 crystals obtained under the growth conditions chosen have I4(1)/a symmetry and do not undergo structural phase transitions in the temperature range 100-800 K. Crystalline inclusions of the AlOF oxyfluoride have been revealed in crystals grown with an AlF3 excess. The birefringence of the AlOF crystal is an order of magnitude higher than that of SrAlF5, does not depend on temperature, and has no anomalies up to 800 K.
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15.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Gorev M. V., Molokeev M. S., Kartashev A. V., Pogoreltsev E. I., Mel'nikova S. V., Laptash N. M., Flerov I. N.
Заглавие : Investigation of thermal properties and structure of complex fluoride K3ZrF7
Место публикации : J. Fluor. Chem. - 2021. - Vol. 241. - Ст.109677. - ISSN 00221139 (ISSN), DOI 10.1016/j.jfluchem.2020.109677
Примечания : Cited References: 44. - The reported study was funded by RFBR according to the research project No. 18-02-00269 a. X-ray and dilatometric data were obtained using the equipment of Krasnoyarsk Regional Center of Research Equipment of Federal Research Center "Krasnoyarsk Science Center SB RAS"
Аннотация: X-ray, calorimetric and dilatometric studies of K3ZrF7 revealed the existence of the phase transition Fm-3m ↔ R-3m at T0 = 320 K. The structural model assumes a disorder of a pentagonal bipyramid ZrF7 with the following ratio of equivalent orientation positions in the initial and distorted phases: 12 to 6. A good agreement was found between the experimental and model-calculated changes in strain and entropy during the phase transition. A comparative analysis of entropy and structural parameters of related fluorides K3ZrF7 - (NH4)2KZrF7 - (NH4)3ZrF7 was performed. The anomalous behavior of thermodynamic properties in the range 140−230 K is not typical for phase transitions and is accompanied by a significant change in the entropy of the crystal lattice.
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16.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Komogortsev S. V., Chekanova L. A., Denisova E. A., Bukaemskiy A. A., Iskhakov R. S., Mel'nikova S. V.
Заглавие : Macro- and nanoscale magnetic anisotropy of FeNi(P) micropillars in polycarbonate membrane
Место публикации : J. Supercond. Novel Magn. - 2019. - Vol. 32, Is. 4. - P.911–916. - ISSN 15571939 (ISSN) , DOI 10.1007/s10948-018-4772-y
Примечания : Cited References: 56
Ключевые слова (''Своб.индексиров.''): magnetic nanowires--magnetic microwires--magnetic pillars--magnetic anisotropy
Аннотация: Macroscopic and local magnetic anisotropy of the FeNi(P) pillars deposited using electroless plating in the pores of the nuclear track-etched polycarbonate membrane has been studied. The alloy fills the pores and forms a nail-shaped pillar. The macroscopic easy magnetization axis was found to be perpendicular to the membrane plane due to magnetic shape anisotropy. The macroscopic magnetic anisotropy constant decreases with decreasing pillar diameter from 0.4 to 0.1 μm supposedly due to increase of the pillar cap contribution. Approach to magnetic saturation analysis indicates that the order in local easy magnetization axis is localized on a nanoscale. The correlation length of the local easy axis and the local magnetic anisotropy field in (Fe100−xNi x )98P2 pillars of different compositions with diameter of 0.4 μm are studied.
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17.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Komogortsev S. V., Denisova E. A., Chekanova L. A., Bukaemskiy A. A., Iskhakov R. S., Mel'nikova S. V., Chizhik M. V.
Заглавие : Magnetic anisotropy of nanocrystalline FeNi(P) columns electroless deposited in polycarbonate membranes
Коллективы : Annual conference on мagnetism and мagnetic мaterials
Место публикации : 58th Annual conference on мagnetism and мagnetic мaterials : abstacts. - 2013. - P.580
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18.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Denisova E. A., Chekanova L. A., Iskhakov R. S., Komogortsev S. V., Mel'nikova S. V.
Заглавие : Magnetic properties of composite materials: Co(P) particles in porous templates
Коллективы : IEEE International Magnetics Conference (2014 ; May ; 4-8; Dresden, Germany)
Место публикации : Digest book IEEE International Magnetics Conference. - 2014. - P.2569-2570
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19.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mel'nikova S. V., Grankina V. A., Kartashev A. V.
Заглавие : A study of the effect of gradual substitution NH4 - Cs on phase transitions in NH4LiSO4 crystals
Разночтения заглавия :авие SCOPUS: A study of the effect of gradual substitution NH4 Cs on phase transitions in NH4LiSO4 crystals
Место публикации : Phys. Solid State: AMER INST PHYSICS, 2002. - Vol. 44, Is. 2. - P379-385. - ISSN 1063-7834, DOI 10.1134/1.1451032
Примечания : Cited References: 22
Предметные рубрики: MIXED-CRYSTALS
TEMPERATURE PHASE
LINH4SO4
BIREFRINGENCE
SULFATE
RAMAN
Аннотация: Solid solutions in the Cs-x(NH4)(1 - x)LiSO4 (0 less than or equal to x less than or equal to 0.35) system are grown and investigated. The birefringence (n(a) - n(b)) and the heat capacity are measured in the temperature range 100-530 K. The (x-T) phase diagram is constructed. It is demonstrated that the substitution of cesium for ammonium in the NH4LiSO4 crystal affects the transition temperatures in such a way that the region of the ferroelectric phase increases and the ferroelastic phase disappears at x 0.22. The character of the high-temperature transition remains unchanged (2beta = 0.24 +/- 0.01 for all compositions), but the birefringence anomaly and enthalpy decrease. As the concentration x increases, the low-temperature transition becomes more similar to a first-order transition: the birefringence jump deltan and the temperature hysteresis DeltaT increase. (C) 2002 MAIK "Nauka/Interperiodica".
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20.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mel'nikova S. V., Laptash N. M.
Заглавие : Influence of atmospheric humidity on the symmetry and phase transitions of layered potassium oxyfluorides K2NbOF5 · H2O
Место публикации : Phys. solid state: Springer, 2013. - Vol. 55, Is. 6. - P.1231-1235
Аннотация: Crystals of K2NbOF5 · H2O have been grown, polarization optical investigations have been performed, and the birefringence and rotation angle of the optical indicatrix have been measured in the temperature range 100–400 K. It has been found that, depending on the degree of atmospheric humidity, the layered K2NbOF5 · H2O crystal at room temperature can be in three states, namely, A, B, and C, which differ in symmetry and properties of the crystal. The K2NbOF5 · H2O crystal in the A state exists at a relative humidity RH = 90–100% and undergoes a first-order improper ferroelastic phase transition P 1ˉ ↔ C2/m, which is accompanied by strong anomalies of the optical characteristics, twinning, and shear strain x 6 at temperatures T 2 ↓ = 308 K and T 2 ↑= 313 K. The most stable state of the K2NbOF5 sdH2O crystal is the B state (RH = 20–90%), which retains the monoclinic symmetry C2/m in the temperature range 100–370 K. In a dry atmosphere (RH = 0–20%) or at T 1 ≈ 370 K, the crystal becomes anhydrous (K2NbOF5) with the symmetry P4/nmm (the C state). The difference between the crystals in the states A and B is explained by the presence or absence of water molecules in interlayer spaces.
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