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    2-Thiobarbiturate complexes of Ca(II): synthesis, crystal structure and thermal properties / N. N. Golovnev [et al.] // 3 Int. Conf. on the Advancement of Mater. and Nanotechn. (ICAMN 2013) : Programme and abstracts book. - 2013. - P. 157
   Перевод заглавия: 2-тиобарбитуровые комплексы Ca(II): синтез, кристаллическая структура и термические свойства
Кл.слова (ненормированные):
calcium -- 2-thiobarbituric acid -- crystal structure -- thermal decomposition -- IR spectroscopy

Доп.точки доступа:
Golovnev, N. N.; Головнёв, Николай Николаевич; Molokeev, M. S.; Молокеев, Максим Сергеевич; Vereschagin, S. N.; Верещагин, С. Н.; Atuchin, V. V.; Атучин, Виктор Валерьевич; International Conference on the Advancement of Materials and Nanotechnology (3 ; 2013 ; Nov. ; 19-22 ; Penang, Malaysia)
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A quantum chemical study of the formation of 2-hydroperoxy-coelenterazine in the Сa2+-regulated photoprotein obelin / L. Y. Antipina [et al.] // J. Struct. Chem. - 2011. - Vol. 52, Is. 5. - P. 870-875. - Cited References: 19. - The work was supported by RFBR (07-04-00930-a), the "Molecular and Cell Biology" Program of the Presidium of the Russian Academy of Sciences, and the Program of the Siberian Division of the Russian Academy of Sciences (project No. 2) within the implementation of the Federal Targeted Program "Scientific and Scientific Pedagogical Personnel of Innovative Russia, 2010" (P333 and P213). . - ISSN 0022-4766

РУБ Chemistry, Inorganic & Nuclear + Chemistry, Physical
Рубрики:
CALCIUM-DISCHARGED OBELIN
   SEMIEMPIRICAL METHODS
   1.7 ANGSTROM
   OPTIMIZATION
   PARAMETERS
   MECHANISM
   FLUORESCENCE
   ELEMENTS
   PROTEIN
   EMITTER
Кл.слова (ненормированные):
coelenterazine -- 2-hydroperoxy-coelenterazine -- Obelia longissima -- Renilla muelleri
Аннотация: The Ca2+-regulated photoprotein obelin determines the luminescence of the marine hydroid Obelia longissima. Bioluminescence is initiated by calcium and appears as a result of the oxidative decarboxylation related to the coelenterazine substrate. The luciferase of the luminescent marine coral Renilla muelleri (RM) also uses coelenterazine as a substrate. However, three proteins are involved in the in vivo bioluminescence of these animals: luciferase, green fluorescent protein, and Ca2+-regulated coelenterazine-binding protein (CBP). In fact, CBP that contains one strongly bound coelenterazine molecule is the RM luciferase substrate in the in vivo bioluminescent reaction. Coelenterazine becomes available for oxygen and the reaction with luciferase only after binding CBP with calcium ions. Unlike Ca2+-regulated photoproteins, the coelenterazine molecule is not activated by oxygen in the CBP molecule. In this work, by means of quantum chemical methods the behavior of substrates in these proteins is analyzed. It is shown that coelenterazine can form different tautomers: CLZ(2H) and CLZ(7H). The formation of 2-hydroperoxy-coelenterazine is studied. According to the obtained data, these proteins use different forms of the substrates for the reaction. In obelin, the substrate is in the CLZ(2H) form that affords hydrogen peroxide. In RM, coelenterazine is in the CLZ(7H) form, and therefore, CBP is not activated by oxygen.

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Держатели документа:
Russian Acad Sci, LV Kirensky Phys Inst, Siberian Div, Krasnoyarsk, Russia
Russian Acad Sci, Inst Biophys, Siberian Div, Krasnoyarsk, Russia
MF Reshetnev Siberian State Aerosp Univ, Krasnoyarsk, Russia

Доп.точки доступа:
Antipina, L. Yu.; Tomilin, F. N.; Томилин, Феликс Николаевич; Vysotski, E. S.; Высоцкий, Евгений Степанович; Ovchinnikov, S. G.; Овчинников, Сергей Геннадьевич
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    Calcium and strontium thiobarbiturates with discrete and polymeric structures / N. N. Golovnev [et al.] // J. Coordinat. Chem. - 2013. - Vol. 66. No. 23. - P. 4119–4130, DOI 10.1080/00958972.2013.860450 . - ISSN 4119-4130
   Перевод заглавия: Кальциевый и стронциевый тиобарбитураты с дискретной и полимерной структурами
Кл.слова (ненормированные):
Calcium -- 2-Thiobarbituric acid IR -- Crystal structure -- Thermal decomposition -- Strontium -- IR spectroscopy
Аннотация: Three new alkaline earth metal complexes, [Ca2(H2O)8(μ2-HTBA-O,O′)2(HTBA-O)2] (1), [Ca(H2O)5(HTBA-O)2]·2H2O (2), and [Sr(H2O)4(μ2-HTBA-O,S)2]n (3) (H2TBA = 2-thiobarbituric acid, C4H4N2O2S), were synthesized and characterized by FT-IR spectroscopy, TG-DSC, and single-crystal and powder X-ray diffraction analysis. The single-crystal X-ray diffraction data revealed that 1 and 2 are discrete structures, whereas 3 is a polymer. In 1 and 2, Ca2+ is seven-coordinate and forms a monocapped trigonal prism. In 1, the prisms are pairwise connected with the assistance of two [μ2-HTBA-O,O′]− ligands. In 3, Sr2+ is coordinated by four monodentate HTBA− via S or O donors and four waters, with the formation of a distorted square antiprism. The antiprisms are connected by μ2-O,S bridging HTBA−. Hydrogen bonding involving coordinated water and π–π interactions plays an important role in construction of the supramolecular 3-D structures in 1–3. Infrared spectroscopic data supported the structural data. The thermal stability of 1–3 decreases in the order 1 > 2 > 3. Dehydration of 1–3 was a multi-step process, followed by exothermic oxidative degradation of the 2-thiobarbiturate moiety between 290 and 800 °C.

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Держатели документа:
Siberian Fed Univ, Dept Chem, Krasnoyarsk, Russia
LV Kirenskii Inst Phys, Lab Crystal Phys, Krasnoyarsk 660036, Russia
Inst Chem & Chem Technol, Lab Catalyt Convers Small Mol, Krasnoyarsk, Russia
Russian Acad Sci, Inst Semicond Phys, Lab Opt Mat & Struct, Novosibirsk 630090, Russia;

Доп.точки доступа:
Golovnev, N. N.; Головнёв, Николай Николаевич; Molokeev, M. S.; Молокеев, Максим Сергеевич; Vereshchagin, S. N.; Atuchin, V. V.
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    Complex of Ca(II) with ceftriaxone: Synthesis, structure, spectral and antibacterial properties / G. V. Novikova, D. I. Tsyplenkova, A. A. Kuzubov [и др.] // J. Sib. Fed. Univ. Chem. - 2021. - Vol. 14, Is. 3. - P. 290-301 ; Журн. СФУ. Химия, DOI 10.17516/1998-2836-0238. - Cited References: 39. - The research was funded by RFBR, Krasnoyarsk Territory and Krasnoyarsk Regional Fund of Science, project number 20-43-240007 . - ISSN 1998-2836. - ISSN 2313-6049
   Перевод заглавия: Комплекс Ca(II) с цефтриаксоном: синтез, структура, спектральные и антибактериальные свойства

РУБ Chemistry, Multidisciplinary
Рубрики:
BASIS-SETS
   ALGORITHM
   1ST-ROW
   CALCIUM
Кл.слова (ненормированные):
ceftriaxone -- calcium -- DFT -- IR spectroscopy -- luminescence properties -- antibacterial screening -- цефтриаксон -- кальций -- теория функционала плотности -- ИК-спектроскопия -- люминесцентные свойства -- антибактериальный скрининг
Аннотация: The calcium complex of ceftriaxone was synthesized and characterized by elemental, atomic-emission analysis, TGA, IR spectroscopy and density functional theory calculations. The luminescence and antibacterial properties of the ceftriaxone disodium and calcium complex wcrc investigated. Ca(II) complex was obtained in a crystalline form, cell parameters of the compound were determined. Ceftriaxone was coordinated to the calcium ion by the oxygen of the triazine cycle in the 6th position, the nitrogen of the amine group of the thiazole ring, and the oxygens of the lactam carbonyl and carboxylate groups. The complex of Ca(II) with ceftriaxone was screened for antibacterial activity against Staphylococcus aureus, Escherichia coli and Pseudomonas aeruginosa, and the results were compared with the activity of ceftriaxone disodium salt.
Кальциевый комплекс цефтриаксона был синтезирован и охарактеризован с помощью элементного, атомно-эмиссионного анализа, ТГА, ИК‑спектроскопии и расчетов теории функционала плотности. Исследованы люминесцентные и антибактериальные свойства динатриевой соли цефтриаксона и комплекса цефтриаксона с кальцием. Комплекс Ca(II) получен в кристаллическом виде, определены параметры кристаллической решетки соединения. Цефтриаксон координировался к иону кальция через атом кислорода триазинового цикла в 6-м положении, атом азота аминогруппы тиазольного кольца и атомами кислорода карбонильной и карбоксилатной групп. Комплекс Са(II) с цефтриаксоном обладает антибактериальной активностью против Staphylococcus aureus, Escherichia coli и Pseudomonas aeruginosa, полученные результаты сравнивали с активностью динатриевой соли цефтриаксона.

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Держатели документа:
Siberian Fed Univ, Sch Nonferrous Met & Mat Sci, Krasnoyarsk, Russia.
FRC Krasnoyarsk Sci Ctr SB RAS, LV Kirensky Inst Phys SB RAS, Krasnoyarsk, Russia.
FRC Krasnoyarsk Sci Ctr SB RAS, Sci Res Inst Med Problems North, Krasnoyarsk, Russia.
FRC Krasnoyarsk Sci Ctr SB RAS, Inst Chem & Chem Technol SB RAS, Krasnoyarsk, Russia.

Доп.точки доступа:
Novikova, Galina, V; Tsyplenkova, Darya, I; Kuzubov, A. A.; Кузубов, Александр Александрович; Kolenchukova, Oksana A.; Samoilo, Alexander S.; Vorobyev, Sergey A.; RFBR, Krasnoyarsk Territory; Krasnoyarsk Regional Fund of Science [20-43-240007]

}
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Heat capacity and thermodynamic properties of germanates CaR2Ge3O10 (R = Pr, Nd) in the region of 320–1000 K / L. T. Denisova, M. S. Molokeev, N. A. Galiakhmetova [et al.] // Russ. J. Phys. Chem. A. - 2022. - Vol. 96, Is. 5. - P. 913-917, DOI 10.1134/S0036024422050077. - Cited References: 30. - The authors are grateful to the Krasnoyarsk Regional Shared Resource Center of the Krasnoyarsk Science Center. This work was performed as part of a State Task for Siberian Federal University, project no. FSRZ-2020-0013 . - ISSN 0036-0244
Кл.слова (ненормированные):
neodymium and praseodymium calcium germanates -- differential scanning calorimetry -- high-temperature heat capacity
Аннотация: Sequential annealing of stoichiometric mixtures of CaCO3, Pr6O11(Nd2O3), and GeO2 in air at 1423–1473 K yields germanates CaPr2Ge3O10 and CaNd2Ge3O10. Their crystal structure is refined via X-ray diffraction. The high-temperature heat capacity (320–1000 K) is measured by means of differential scanning calorimetry. The thermodynamic properties of germanates are calculated using experimental dependences Cp = f(T).

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Публикация на русском языке Теплоемкость и термодинамические свойства германатов CaR2Ge3O10 (R = Pr, Nd) в области 320–1000 K [Текст] / Л. Т. Денисова, М. С. Молокеев, Н. А. Галиахметова [и др.] // Журн. физ. химии. - 2022. - Т. 96 № 5. - С. 615-620

Держатели документа:
Siberian Federal University, Krasnoyarsk, 660041, Russian Federation
Krasnoyarsk Science Center, Siberian Branch, Russian Academy of Sciences, Krasnoyarsk, 660036, Russian Federation

Доп.точки доступа:
Denisova, L. T.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Galiakhmetova, N. A.; Denisov, V. M.; Belousova, N. V.
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High-temperature heat capacity and thermodynamic properties of the CaY2Ge3O10 and CaY2Ge4O12 germanates / L. T. Denisova, M. S. Molokeev, Y. F. Kargin [et al.] // Inorg. Mater. - 2022. - Vol. 58, Is. 4. - P. 414-419, DOI 10.1134/S0020168522040033. - Cited References: 31. - This work was supported in part by the Russian Federation Ministry of Science and Higher Education as part of the state research target for the Siberian Federal University federal state autonomous educational institution of higher education, project no. FSRZ-2020-0013 . - ISSN 0020-1685
Кл.слова (ненормированные):
calcium yttrium germanates -- solid-state synthesis -- X-ray diffraction -- crystal structure -- high-temperature heat capacity -- thermodynamic properties
Аннотация: The CaY2Ge3O10 and CaY2Ge4O12 germanates have been synthesized by a standard ceramic processing route using CaCO3, Y2O3, and GeO2 as starting materials, and their crystal structure has been refined by X-ray diffraction. The high-temperature (350–1000 K) experimental heat capacity data obtained for the germanates by differential scanning calorimetry have been used to calculate their principal thermodynamic functions.

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Публикация на русском языке Высокотемпературная теплоемкость и термодинамические свойства германатов CaY2Ge3O10 и CaY2Ge4O12 [Текст] / Л. Т. Денисова, М. С. Молокеев, Ю. Ф. Каргин [и др.] // Неорган. матер. - 2022. - Т. 58. № 4. - С. 432-436

Держатели документа:
Siberian Federal University, Krasnoyarsk, 660041, Russian Federation
Kirensky Institute of Physics, Krasnoyarsk Scientific Center (Federal Research Center), Siberian Branch, Russian Academy of Sciences, Akademgorodok, Krasnoyarsk, 660036, Russian Federation
Baikov Institute of Metallurgy and Materials Science, Russian Academy of Sciences, Moscow, 119991, Russian Federation

Доп.точки доступа:
Denisova, L. T.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Kargin, Y. F.; Galiakhmetova, N. A.; Beletskii, V. V.; Denisov, V. M.
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    Hydrodynamic dispersion of calcium aluminosilicate from technogenic and nonmetallic material / L. V. Kashkina [et al.] // J. Sib. Fed. Univ. Eng. Technol. - 2014. - Vol. 7, Is. 1. - P. 3-12 ; Журн. СФУ. Сер. "Техника и технологии"
   Перевод заглавия: Гидродинамическое диспергирование кальций-алюмосиликатных материалов из техногенного и нерудного сырья
Кл.слова (ненормированные):
hydrodynamic dispersion -- cavitation -- crystal ceramic foam -- porous glass material -- гидродинамическое диспергирование -- кавитация -- зола -- пеноматериал -- пористая стеклокерамика
Аннотация: Physicochemical properties of two calcium aluminosilicate materials after reducing in the hydrodynamic rotary generator in supercavitation mode were studied. The samples are the crystal ceramic foam based on Kansko-Achinsk lignite-ash and the porous glass material obtained from low-manganese nonmetallic feed. X-ray phase analysis, EPR-method, NPR-method (the Mossbauer Effect) and optical microscopy were used. It was found that the material is changing its stucrure in a hydrodynamic dispersion process caused by high-cavitation. The nature of the changes depends on its initial state.
Изучены физико-химические свойства двух кальций-алюмосиликатных материалов после измельчения в гидродинамическом генераторе роторного типа в режиме суперкавитации. Исследованы образцы – кристаллическая пенокерамика на основе зол бурых Канско-Ачинских углей и пористый стекломатериал, полученный из нерудного сырья с низким содержанием марганца. Для анализа были использованы методы РФА, ЭМР, ЯГР (эффект Мёссбауэра), оптическая микроскопия. Показано, что в процессе гидродинамического диспергирования за счет высокоэнергетического кавитационного воздействия в материалах происходят глубокие структурные изменения. Получено, что характер изменений зависит от исходного состояния исследуемого материала.

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Держатели документа:
Siberian Federal University, 79 Svobodny, Krasnoyarsk, 660041, Russia
L.V. Kirensky Institute of Physics SB RAS, 50/38 Akademgorodok, Krasnoyarsk, 660036, Russia

Доп.точки доступа:
Kashkina, L. V.; Stebeleva, O. P.; Emelyanova, T. Y.; Petrakovskaya, E. A.; Петраковская, Элеонора Анатольевна; Bayukov, O. A.; Баюков, Олег Артемьевич

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Magnetoresistance hysteresis of bulk textured Bi1.8Pb0.3Sr1.9Ca2Cu3Ox + Ag ceramics and its anisotropy / D. A. Balaev [et al.] // Physica C. - 2010. - Vol. 470, Is. 1. - P. 61-67, DOI 10.1016/j.physc.2009.10.007. - Cited References: 24. - Authors thanks to I.L. Belozerova for help in preparation of textured ceramics. This work was supported by program N5 of RAS, project N7, and in part in frames of young scientist projects of Siberian Federal University, project N6. . - ISSN 0921-4534

РУБ Physics, Applied
Рубрики:
CRITICAL-CURRENT ANISOTROPY
   HIGH-TEMPERATURE SUPERCONDUCTOR
   CRITICAL-CURRENT DENSITY
   MAGNETIC HYSTERESIS
   TAPES
   FLUX
   YBA2CU3O7-DELTA
   FIELD
Кл.слова (ненормированные):
Magnetoresistance -- Anisotropy -- Scaling -- Magnetization -- Bi2223 -- BSCCO -- Anisotropy -- Bi2223 -- BSCCO -- Magnetization -- Magnetoresistance -- Scaling -- Bi-2223 -- BSCCO -- External fields -- Granular superconductors -- Magnetic induction -- Parameters characterizing -- Anisotropy -- Calcium -- Ceramic materials -- Crystallites -- Electric resistance -- Hysteresis -- Lead -- Magnetic moments -- Magnetoelectronics -- Magnetoresistance -- Nanocrystalline alloys -- Silver -- Superconducting materials -- Superconductivity -- Magnetic field effects
Аннотация: Magnetoresistance of bulk textured Bi1.8Pb0.3Sr1.9Ca2Cu3Ox + Ag ceramics has been studied in the magnetic fields applied parallel and perpendicular to a-b planes of Bi2223 crystallites. Besides well known anisotropy of magnetoresistance of textured superconductors (R-H parallel to c > RH parallel to a-b), anisotropic hysteresis of R(H) dependences was investigated. Parameters characterizing hysteretic R(H) curves differ for the cases H parallel to c and H parallel to a-b. This behavior is explained within the model of a granular superconductor where the total magnetic induction in the intercrystallite boundaries is superposition of the external field and the magnetic field induced by dipole magnetic moments of neighbor crystallites. (C) 2009 Elsevier B.V. All rights reserved.

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Держатели документа:
[Gokhfeld, D. M.] RAS, SD, LV Kirensky Phys Inst, High Magnet Fields Lab, Krasnoyarsk 660036, Russia
[Balaev, D. A.
Semenov, S. V.
Shaykhutdinov, K. A.] Siberian Fed Univ, Krasnoyarsk 660041, Russia
ИФ СО РАН
L.V. Kirensky Institute of Physics, Krasnoyarsk, 660036, Russian Federation
Siberian Federal University, Krasnoyarsk, 660041, Russian Federation

Доп.точки доступа:
Balaev, D. A.; Балаев, Дмитрий Александрович; Popkov, S. I.; Попков, Сергей Иванович; Semenov, S. V.; Семенов, Сергей Васильевич; Bykov, A. A.; Быков, Алексей Анатольевич; Shaykhutdinov, K. A.; Шайхутдинов, Кирилл Александрович; Gokhfeld, D. M.; Гохфельд, Денис Михайлович; Petrov, M. I.; Петров, Михаил Иванович
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Mechanism of the hysteretic behavior of the magnetoresistance of granular HTSCs: The universal nature of the width of the magnetoresistance hysteresis loop / D. A. Balaev [et al.] // J. Exp. Theor. Phys. - 2009. - Vol. 108, Is. 2. - P. 241-248, DOI 10.1134/S106377610902006X. - Cited References: 32. - This study was carried out under the program "Quantum Macrophysics" of the Russian Academy of Sciences and complex integration project no. 3.4 of the Siberian Branch of the Russian Academy of Sciences, and was partly supported by the Krasnoyarsk Regional Science Foundation (grant no. 18G011). D. A. B. and A. A. D. are grateful to the Foundation for Supporting National Science Projects. . - ISSN 1063-7761

РУБ Physics, Multidisciplinary
Рубрики:
CRITICAL-CURRENT-DENSITY
   HIGH-TEMPERATURE SUPERCONDUCTOR
   CURRENT-VOLTAGE CHARACTERISTICS
   EXTERNAL MAGNETIC-FIELD
   BA-CU-O
   JOSEPHSON MEDIUM
   CRITICAL-STATE
   FLUX
   COMPOSITES
   YBA2CU3O7-DELTA
Кл.слова (ненормированные):
Barium -- Calcium -- Damping -- Electric resistance -- High temperature superconductors -- Magnetic field effects -- Magnetic materials -- Magnetoelectronics -- Magnetoresistance -- Stiffness -- Classical systems -- Critical densities -- Experimental datum -- External conditions -- Flux trapping -- Hysteretic behaviors -- Josephson vortices -- Residual resistances -- Transport currents -- Universal behaviors -- Y-ba-cu-o -- Hysteresis
Аннотация: The hysteretic behavior of the magnetoresistance R(H) of granular high-temperature superconductors (HTSCs) of the Y-Ba-Cu-O, Bi-Ca-Sr-Cu-O, and La-Sr-Cu-O classical systems is investigated for transport current densities lower and higher than the critical density (at H = 0). All systems exhibit universal behavior of the width of the magnetoresistance hysteresis loop: independence of transport current under identical external conditions. This means that flux trapping in HTSC grains is the main mechanism controlling the hysteretic behavior of the magnetoresistance of granular HTSCs, while pinning of Josephson vortices in the intragranular medium makes no appreciable contribution to the formation of magnetoresistance hysteresis (when transport current flows through the sample). Experimental data on relaxation of residual resistance after the action of a magnetic field also confirm this conclusion.

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Держатели документа:
[Balaev, D. A.
Dubrovskii, A. A.
Shaikhutdinov, K. A.
Popkov, S. I.
Gokhfeld, D. M.
Gokhfeld, Yu. S.
Petrov, M. I.] Russian Acad Sci, Siberian Branch, Kirenskii Inst Phys, Krasnoyarsk 660036, Russia
ИФ СО РАН
Kirenskii Institute of Physics, Siberian Branch, Russian Academy of Sciences, Krasnoyarsk, 660036, Russian Federation

Доп.точки доступа:
Balaev, D. A.; Балаев, Дмитрий Александрович; Dubrovskii, A. A.; Дубровский, Андрей Александрович; Shaikhutdinov, K. A.; Шайхутдинов, Кирилл Александрович; Popkov, S. I.; Попков, Сергей Иванович; Gokhfeld, D. M.; Гохфельд, Денис Михайлович; Gokhfeld, Yu. S.; Гохфельд, Юлия Сергеевна; Petrov, M. I.; Петров, Михаил Иванович; Quantum Macrophysics of the Russian Academy of Sciences [3.4]; Krasnoyarsk Regional Science Foundation [18G011]; Foundation for Supporting National Science Projects
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10.

    New insight into the crystal structure of Sr4Ca(PO4)2SiO4 and the photoluminescence tuning of Sr4Ca(PO4)2SiO4:Ce3+,Na+,Eu2+ phosphors / M. Zhang [et al.] // J. Mater. Chem. C. - 2016. - Vol. 4, Is. 38. - P. 9078-9084, DOI 10.1039/c6tc03373c. - Cited References: 31 . - ISSN 2050-7534
   Перевод заглавия: Новый взгляд на кристаллическую структуру Sr4Ca(PO4)2SiO4 и управление люминесценцией в Sr4Ca(PO4)2SiO4:Ce3+,Na+,Eu2+
Кл.слова (ненормированные):
Calcium -- Energy transfer -- Europium -- Light emission -- Light emitting diodes -- Luminescence -- Phosphate minerals -- Phosphors -- Photoluminescence -- Positive ions -- Rietveld refinement -- Tuning -- Chemical compositions -- Energy transfer mechanisms -- Green component -- Hexagonal cells -- Luminescence properties -- Single phase -- Solid state method -- White lightemitting diodes (WLEDs) -- Crystal structure
Аннотация: A new single phase based on the substitution of a Sr cation by a Ca cation in the apatite-type Sr5(PO4)2(SiO4) has been fabricated with the nominal chemical composition of Sr4Ca(PO4)2(SiO4), which appears as a definite compound rather than a solid solution between (Sr,Ca)3(PO4)2 and (Sr,Ca)2SiO4. The crystal structure of Sr4Ca(PO4)2(SiO4) has been firstly analysed by the difference electron map, and further resolved by the Rietveld refinement, and the final composition has been determined as Sr4Ca(PO4)(2+x)(SiO4)(1-x)(OH)x (x = 0.64) with a hexagonal cell (P63/m). The Ce3+/Eu2+ codoped Sr4Ca(PO4)2SiO4 phosphors have been designed and prepared by the solid state method, and the photoluminescence tuning from blue to green upon 365 nm ultraviolet (UV) radiation can be realized, which is ascribed to the energy transfer from Ce3+ to Eu2+ ions. The luminescence properties and the energy transfer mechanism in Ce3+/Eu2+ codoped Sr4Ca(PO4)2SiO4 phosphors have been discussed, which might act as potential candidates for blue-green components in UV-pumped white light emitting diodes (WLEDs). © 2016 The Royal Society of Chemistry.

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Держатели документа:
School of Materials Sciences and Engineering, University of Science and Technology Beijing, Beijing, China
Laboratory of Crystal Physics, Kirensky Institute of Physics, SB RAS, Krasnoyarsk, Russian Federation
Department of Physics, Far Eastern State Transport University, Khabarovsk, Russian Federation

Доп.точки доступа:
Zhang, M.; Xia, Z.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Shi, L.; Liu, Q.
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