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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Golovnev N. N., Molokeev M. S., Vereschagin S. N., Atuchin V. V.
Заглавие : 2-Thiobarbiturate complexes of Ca(II): synthesis, crystal structure and thermal properties
Коллективы : International Conference on the Advancement of Materials and Nanotechnology (3; 2013 ; Nov. ; 19-22; Penang, Malaysia)
Место публикации : 3 Int. Conf. on the Advancement of Mater. and Nanotechn. (ICAMN 2013): Programme and abstracts book. - 2013. - P.157
Ключевые слова (''Своб.индексиров.''): calcium--2-thiobarbituric acid--crystal structure--thermal decomposition--ir spectroscopy
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Antipina L. Yu., Tomilin F. N., Vysotski E. S., Ovchinnikov S. G.
Заглавие : A quantum chemical study of the formation of 2-hydroperoxy-coelenterazine in the Сa2+-regulated photoprotein obelin
Место публикации : J. Struct. Chem.: Springer, 2011. - Vol. 52, Is. 5. - P.870-875. - ISSN 0022-4766
Примечания : Cited References: 19. - The work was supported by RFBR (07-04-00930-a), the "Molecular and Cell Biology" Program of the Presidium of the Russian Academy of Sciences, and the Program of the Siberian Division of the Russian Academy of Sciences (project No. 2) within the implementation of the Federal Targeted Program "Scientific and Scientific Pedagogical Personnel of Innovative Russia, 2010" (P333 and P213).
Предметные рубрики: CALCIUM-DISCHARGED OBELIN
SEMIEMPIRICAL METHODS
1.7 ANGSTROM
OPTIMIZATION
PARAMETERS
MECHANISM
FLUORESCENCE
ELEMENTS
PROTEIN
EMITTER
Ключевые слова (''Своб.индексиров.''): coelenterazine--2-hydroperoxy-coelenterazine--obelia longissima--renilla muelleri
Аннотация: The Ca2+-regulated photoprotein obelin determines the luminescence of the marine hydroid Obelia longissima. Bioluminescence is initiated by calcium and appears as a result of the oxidative decarboxylation related to the coelenterazine substrate. The luciferase of the luminescent marine coral Renilla muelleri (RM) also uses coelenterazine as a substrate. However, three proteins are involved in the in vivo bioluminescence of these animals: luciferase, green fluorescent protein, and Ca2+-regulated coelenterazine-binding protein (CBP). In fact, CBP that contains one strongly bound coelenterazine molecule is the RM luciferase substrate in the in vivo bioluminescent reaction. Coelenterazine becomes available for oxygen and the reaction with luciferase only after binding CBP with calcium ions. Unlike Ca2+-regulated photoproteins, the coelenterazine molecule is not activated by oxygen in the CBP molecule. In this work, by means of quantum chemical methods the behavior of substrates in these proteins is analyzed. It is shown that coelenterazine can form different tautomers: CLZ(2H) and CLZ(7H). The formation of 2-hydroperoxy-coelenterazine is studied. According to the obtained data, these proteins use different forms of the substrates for the reaction. In obelin, the substrate is in the CLZ(2H) form that affords hydrogen peroxide. In RM, coelenterazine is in the CLZ(7H) form, and therefore, CBP is not activated by oxygen.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Golovnev N. N., Molokeev M. S., Vereshchagin S. N., Atuchin V. V.
Заглавие : Calcium and strontium thiobarbiturates with discrete and polymeric structures
Место публикации : J. Coordinat. Chem.: Taylor & Francis, 2013. - Vol. 66. No. 23. - P.4119–4130. - ISSN 4119-4130, DOI 10.1080/00958972.2013.860450
Ключевые слова (''Своб.индексиров.''): calcium--2-thiobarbituric acid ir--crystal structure--thermal decomposition--strontium--ir spectroscopy
Аннотация: Three new alkaline earth metal complexes, [Ca2(H2O)8(μ2-HTBA-O,O′)2(HTBA-O)2] (1), [Ca(H2O)5(HTBA-O)2]·2H2O (2), and [Sr(H2O)4(μ2-HTBA-O,S)2]n (3) (H2TBA = 2-thiobarbituric acid, C4H4N2O2S), were synthesized and characterized by FT-IR spectroscopy, TG-DSC, and single-crystal and powder X-ray diffraction analysis. The single-crystal X-ray diffraction data revealed that 1 and 2 are discrete structures, whereas 3 is a polymer. In 1 and 2, Ca2+ is seven-coordinate and forms a monocapped trigonal prism. In 1, the prisms are pairwise connected with the assistance of two [μ2-HTBA-O,O′]− ligands. In 3, Sr2+ is coordinated by four monodentate HTBA− via S or O donors and four waters, with the formation of a distorted square antiprism. The antiprisms are connected by μ2-O,S bridging HTBA−. Hydrogen bonding involving coordinated water and π–π interactions plays an important role in construction of the supramolecular 3-D structures in 1–3. Infrared spectroscopic data supported the structural data. The thermal stability of 1–3 decreases in the order 1 2 3. Dehydration of 1–3 was a multi-step process, followed by exothermic oxidative degradation of the 2-thiobarbiturate moiety between 290 and 800 °C.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Novikova, Galina, V, Tsyplenkova, Darya, I, Kuzubov A. A., Kolenchukova, Oksana A., Samoilo, Alexander S., Vorobyev, Sergey A.
Заглавие : Complex of Ca(II) with ceftriaxone: Synthesis, structure, spectral and antibacterial properties
Коллективы : RFBR, Krasnoyarsk Territory; Krasnoyarsk Regional Fund of Science [20-43-240007]
Место публикации : J. Sib. Fed. Univ. Chem. - 2021. - Vol. 14, Is. 3. - P.290-301. - ISSN 1998-2836, DOI 10.17516/1998-2836-0238; Журн. СФУ. Химия. - ISSN 2313-6049(eISSN)
Примечания : Cited References: 39. - The research was funded by RFBR, Krasnoyarsk Territory and Krasnoyarsk Regional Fund of Science, project number 20-43-240007
Предметные рубрики: BASIS-SETS
ALGORITHM
1ST-ROW
CALCIUM
Аннотация: The calcium complex of ceftriaxone was synthesized and characterized by elemental, atomic-emission analysis, TGA, IR spectroscopy and density functional theory calculations. The luminescence and antibacterial properties of the ceftriaxone disodium and calcium complex wcrc investigated. Ca(II) complex was obtained in a crystalline form, cell parameters of the compound were determined. Ceftriaxone was coordinated to the calcium ion by the oxygen of the triazine cycle in the 6th position, the nitrogen of the amine group of the thiazole ring, and the oxygens of the lactam carbonyl and carboxylate groups. The complex of Ca(II) with ceftriaxone was screened for antibacterial activity against Staphylococcus aureus, Escherichia coli and Pseudomonas aeruginosa, and the results were compared with the activity of ceftriaxone disodium salt.Кальциевый комплекс цефтриаксона был синтезирован и охарактеризован с помощью элементного, атомно-эмиссионного анализа, ТГА, ИК‑спектроскопии и расчетов теории функционала плотности. Исследованы люминесцентные и антибактериальные свойства динатриевой соли цефтриаксона и комплекса цефтриаксона с кальцием. Комплекс Ca(II) получен в кристаллическом виде, определены параметры кристаллической решетки соединения. Цефтриаксон координировался к иону кальция через атом кислорода триазинового цикла в 6-м положении, атом азота аминогруппы тиазольного кольца и атомами кислорода карбонильной и карбоксилатной групп. Комплекс Са(II) с цефтриаксоном обладает антибактериальной активностью против Staphylococcus aureus, Escherichia coli и Pseudomonas aeruginosa, полученные результаты сравнивали с активностью динатриевой соли цефтриаксона.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Denisova L. T., Molokeev M. S., Galiakhmetova N. A., Denisov V. M., Belousova N. V.
Заглавие : Heat capacity and thermodynamic properties of germanates CaR2Ge3O10 (R = Pr, Nd) in the region of 320–1000 K
Место публикации : Russ. J. Phys. Chem. A. - 2022. - Vol. 96, Is. 5. - P.913-917. - ISSN 00360244 (ISSN), DOI 10.1134/S0036024422050077
Примечания : Cited References: 30. - The authors are grateful to the Krasnoyarsk Regional Shared Resource Center of the Krasnoyarsk Science Center. This work was performed as part of a State Task for Siberian Federal University, project no. FSRZ-2020-0013
Аннотация: Sequential annealing of stoichiometric mixtures of CaCO3, Pr6O11(Nd2O3), and GeO2 in air at 1423–1473 K yields germanates CaPr2Ge3O10 and CaNd2Ge3O10. Their crystal structure is refined via X-ray diffraction. The high-temperature heat capacity (320–1000 K) is measured by means of differential scanning calorimetry. The thermodynamic properties of germanates are calculated using experimental dependences Cp = f(T).
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Denisova L. T., Molokeev M. S., Kargin Y. F., Galiakhmetova N. A., Beletskii V. V., Denisov V. M.
Заглавие : High-temperature heat capacity and thermodynamic properties of the CaY2Ge3O10 and CaY2Ge4O12 germanates
Место публикации : Inorg. Mater. - 2022. - Vol. 58, Is. 4. - P.414-419. - ISSN 00201685 (ISSN), DOI 10.1134/S0020168522040033
Примечания : Cited References: 31. - This work was supported in part by the Russian Federation Ministry of Science and Higher Education as part of the state research target for the Siberian Federal University federal state autonomous educational institution of higher education, project no. FSRZ-2020-0013
Аннотация: The CaY2Ge3O10 and CaY2Ge4O12 germanates have been synthesized by a standard ceramic processing route using CaCO3, Y2O3, and GeO2 as starting materials, and their crystal structure has been refined by X-ray diffraction. The high-temperature (350–1000 K) experimental heat capacity data obtained for the germanates by differential scanning calorimetry have been used to calculate their principal thermodynamic functions.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Kashkina L. V., Stebeleva O. P., Emelyanova T. Y., Petrakovskaya E. A., Bayukov O. A.
Заглавие : Hydrodynamic dispersion of calcium aluminosilicate from technogenic and nonmetallic material
Место публикации : J. Sib. Fed. Univ. Eng. Technol. - 2014. - Vol. 7, Is. 1. - P.3-12; Журн. СФУ. Сер. "Техника и технологии"
Ключевые слова (''Своб.индексиров.''): hydrodynamic dispersion--cavitation--crystal ceramic foam--porous glass material--гидродинамическое диспергирование--кавитация--зола--пеноматериал--пористая стеклокерамика
Аннотация: Physicochemical properties of two calcium aluminosilicate materials after reducing in the hydrodynamic rotary generator in supercavitation mode were studied. The samples are the crystal ceramic foam based on Kansko-Achinsk lignite-ash and the porous glass material obtained from low-manganese nonmetallic feed. X-ray phase analysis, EPR-method, NPR-method (the Mossbauer Effect) and optical microscopy were used. It was found that the material is changing its stucrure in a hydrodynamic dispersion process caused by high-cavitation. The nature of the changes depends on its initial state.Изучены физико-химические свойства двух кальций-алюмосиликатных материалов после измельчения в гидродинамическом генераторе роторного типа в режиме суперкавитации. Исследованы образцы – кристаллическая пенокерамика на основе зол бурых Канско-Ачинских углей и пористый стекломатериал, полученный из нерудного сырья с низким содержанием марганца. Для анализа были использованы методы РФА, ЭМР, ЯГР (эффект Мёссбауэра), оптическая микроскопия. Показано, что в процессе гидродинамического диспергирования за счет высокоэнергетического кавитационного воздействия в материалах происходят глубокие структурные изменения. Получено, что характер изменений зависит от исходного состояния исследуемого материала.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Balaev D. A., Popkov S. I., Semenov S. V., Bykov A. A., Shaykhutdinov K. A., Gokhfeld D. M., Petrov M. I.
Заглавие : Magnetoresistance hysteresis of bulk textured Bi1.8Pb0.3Sr1.9Ca2Cu3Ox + Ag ceramics and its anisotropy
Коллективы :
Место публикации : Physica C. - 2010. - Vol. 470, Is. 1. - P.61-67. - ISSN 0921-4534, DOI 10.1016/j.physc.2009.10.007
Примечания : Cited References: 24. - Authors thanks to I.L. Belozerova for help in preparation of textured ceramics. This work was supported by program N5 of RAS, project N7, and in part in frames of young scientist projects of Siberian Federal University, project N6.
Предметные рубрики: CRITICAL-CURRENT ANISOTROPY
HIGH-TEMPERATURE SUPERCONDUCTOR
CRITICAL-CURRENT DENSITY
MAGNETIC HYSTERESIS
TAPES
FLUX
YBA2CU3O7-DELTA
FIELD
Ключевые слова (''Своб.индексиров.''): magnetoresistance--anisotropy--scaling--magnetization--bi2223--bscco--anisotropy--bi2223--bscco--magnetization--magnetoresistance--scaling--bi-2223--bscco--external fields--granular superconductors--magnetic induction--parameters characterizing--anisotropy--calcium--ceramic materials--crystallites--electric resistance--hysteresis--lead--magnetic moments--magnetoelectronics--magnetoresistance--nanocrystalline alloys--silver--superconducting materials--superconductivity--magnetic field effects
Аннотация: Magnetoresistance of bulk textured Bi1.8Pb0.3Sr1.9Ca2Cu3Ox + Ag ceramics has been studied in the magnetic fields applied parallel and perpendicular to a-b planes of Bi2223 crystallites. Besides well known anisotropy of magnetoresistance of textured superconductors (R-H parallel to c RH parallel to a-b), anisotropic hysteresis of R(H) dependences was investigated. Parameters characterizing hysteretic R(H) curves differ for the cases H parallel to c and H parallel to a-b. This behavior is explained within the model of a granular superconductor where the total magnetic induction in the intercrystallite boundaries is superposition of the external field and the magnetic field induced by dipole magnetic moments of neighbor crystallites. (C) 2009 Elsevier B.V. All rights reserved.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Balaev D. A., Dubrovskii A. A., Shaikhutdinov K. A., Popkov S. I., Gokhfeld D. M., Gokhfeld Yu. S., Petrov M. I.
Заглавие : Mechanism of the hysteretic behavior of the magnetoresistance of granular HTSCs: The universal nature of the width of the magnetoresistance hysteresis loop
Коллективы : Quantum Macrophysics of the Russian Academy of Sciences [3.4]; Krasnoyarsk Regional Science Foundation [18G011]; Foundation for Supporting National Science Projects
Место публикации : J. Exp. Theor. Phys.: MAIK NAUKA/INTERPERIODICA/SPRINGER, 2009. - Vol. 108, Is. 2. - P241-248. - ISSN 1063-7761, DOI 10.1134/S106377610902006X
Примечания : Cited References: 32. - This study was carried out under the program "Quantum Macrophysics" of the Russian Academy of Sciences and complex integration project no. 3.4 of the Siberian Branch of the Russian Academy of Sciences, and was partly supported by the Krasnoyarsk Regional Science Foundation (grant no. 18G011). D. A. B. and A. A. D. are grateful to the Foundation for Supporting National Science Projects.
Предметные рубрики: CRITICAL-CURRENT-DENSITY
HIGH-TEMPERATURE SUPERCONDUCTOR
CURRENT-VOLTAGE CHARACTERISTICS
EXTERNAL MAGNETIC-FIELD
BA-CU-O
JOSEPHSON MEDIUM
CRITICAL-STATE
FLUX
COMPOSITES
YBA2CU3O7-DELTA
Ключевые слова (''Своб.индексиров.''): barium--calcium--damping--electric resistance--high temperature superconductors--magnetic field effects--magnetic materials--magnetoelectronics--magnetoresistance--stiffness--classical systems--critical densities--experimental datum--external conditions--flux trapping--hysteretic behaviors--josephson vortices--residual resistances--transport currents--universal behaviors--y-ba-cu-o--hysteresis
Аннотация: The hysteretic behavior of the magnetoresistance R(H) of granular high-temperature superconductors (HTSCs) of the Y-Ba-Cu-O, Bi-Ca-Sr-Cu-O, and La-Sr-Cu-O classical systems is investigated for transport current densities lower and higher than the critical density (at H = 0). All systems exhibit universal behavior of the width of the magnetoresistance hysteresis loop: independence of transport current under identical external conditions. This means that flux trapping in HTSC grains is the main mechanism controlling the hysteretic behavior of the magnetoresistance of granular HTSCs, while pinning of Josephson vortices in the intragranular medium makes no appreciable contribution to the formation of magnetoresistance hysteresis (when transport current flows through the sample). Experimental data on relaxation of residual resistance after the action of a magnetic field also confirm this conclusion.
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Zhang M., Xia Z., Molokeev M. S., Shi L., Liu Q.
Заглавие : New insight into the crystal structure of Sr4Ca(PO4)2SiO4 and the photoluminescence tuning of Sr4Ca(PO4)2SiO4:Ce3+,Na+,Eu2+ phosphors
Место публикации : J. Mater. Chem. C: Royal Society of Chemistry, 2016. - Vol. 4, Is. 38. - P.9078-9084. - ISSN 20507534 (ISSN), DOI 10.1039/c6tc03373c
Примечания : Cited References: 31
Ключевые слова (''Своб.индексиров.''): calcium--energy transfer--europium--light emission--light emitting diodes--luminescence--phosphate minerals--phosphors--photoluminescence--positive ions--rietveld refinement--tuning--chemical compositions--energy transfer mechanisms--green component--hexagonal cells--luminescence properties--single phase--solid state method--white lightemitting diodes (wleds)--crystal structure
Аннотация: A new single phase based on the substitution of a Sr cation by a Ca cation in the apatite-type Sr5(PO4)2(SiO4) has been fabricated with the nominal chemical composition of Sr4Ca(PO4)2(SiO4), which appears as a definite compound rather than a solid solution between (Sr,Ca)3(PO4)2 and (Sr,Ca)2SiO4. The crystal structure of Sr4Ca(PO4)2(SiO4) has been firstly analysed by the difference electron map, and further resolved by the Rietveld refinement, and the final composition has been determined as Sr4Ca(PO4)(2+x)(SiO4)(1-x)(OH)x (x = 0.64) with a hexagonal cell (P63/m). The Ce3+/Eu2+ codoped Sr4Ca(PO4)2SiO4 phosphors have been designed and prepared by the solid state method, and the photoluminescence tuning from blue to green upon 365 nm ultraviolet (UV) radiation can be realized, which is ascribed to the energy transfer from Ce3+ to Eu2+ ions. The luminescence properties and the energy transfer mechanism in Ce3+/Eu2+ codoped Sr4Ca(PO4)2SiO4 phosphors have been discussed, which might act as potential candidates for blue-green components in UV-pumped white light emitting diodes (WLEDs). © 2016 The Royal Society of Chemistry.
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