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1.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Korets A., Krylov A. S., Mironov E., Rabchevskii E.
Заглавие : Experimental study of the structure of milled diamond-containing particles obtained by the detonation method
Место публикации : EPJ Appl. Phys. - 2012. - Vol. 57, Is. 3. - Ст.30701. - ISSN 1286-0042, DOI 10.1051/epjap/2012110208
Примечания : Cited References: 15
Предметные рубрики: PURIFICATION
NANODIAMOND
Ключевые слова (''Своб.индексиров.''): chemical change--diamond grains--experimental spectra--experimental studies--ir spectrum--mechanical force--detonation--diamonds--x ray diffraction--agglomeration
Аннотация: A diamond-containing material (DCM) produced by detonation was mechanically milled using KM-1 and AGO-2S mills. Experimental spectra for infrared (IR) absorption, Raman scattering and X-ray diffraction patterns (XRD) were obtained for the treated DCM samples. We compared the Raman and IR spectra for the KM-1 milled samples and concluded that the surface of the DCM particles was not uniform. The mechanical force that resulted from milling with the AGO-2S destroyed the non-diamond part of the particles and initiated irreversible physical and chemical changes in them. The destruction of the diamond grains was the consequence of these irreversible changes. It follows from the experiments that the dipole momentum of the DCM particle was caused by the presence of polar fragments of molecules. The constant dipole momentum of the particles facilitated the aggregation. Based on this, we proposed a model of a structurally inhomogeneous DCM particle. В© 2012 EDP Sciences.
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2.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Korets A. Y., Krylov A. S., Mironov E. V.
Заглавие : Molecular structural nonuniformity of ultradispersed diamond-containing material and the reasons why it arises
Место публикации : Russ. J. Phys. Chem. B: MAIK NAUKA/INTERPERIODICA/SPRINGER, 2007. - Vol. 1, Is. 5. - P485-492. - ISSN 1990-7931, DOI 10.1134/S1990793107050077
Примечания : Cited References: 25. - В описании WOS - Vol. 2 (ошибочно), Is. 5. - P 485-492
Предметные рубрики: DETONATION
Аннотация: An analysis of IR spectra, Raman spectra, and X-ray diffraction intensity curves for diamond-containing materials obtained by the detonation method under different conditions and purified by different methods was used to examine the structural nonuniformity of diamond-containing particles and the reasons why it arises.
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3.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Korets A. Y., Krylov A. S., Mironov E. V.
Заглавие : Structural Nonuniformity of Detonation-Produced Diamond-Containing Material
Место публикации : Russ. J. Phys. Chem. B: MAIK NAUKA/INTERPERIODICA/SPRINGER, 2010. - Vol. 4, Is. 5. - P793-796. - ISSN 1990-7931, DOI 10.1134/S1990793110050155
Примечания : Cited References: 10
Ключевые слова (''Своб.индексиров.''): diamond-like material--structural nonuniformity--raman scattering spectroscopy
Аннотация: Raman backscattering spectra (RBS), infrared spectra, and X-ray diffraction intensity curves for various fractions of ultradispersed diamond-containing material (UDDCM) were recorded. The RBS and XRD curves obtained suggest that UDDCM is characterized by sharp variations in the ratio between the diamond and nondiamond components, a factor that makes it possible to consider this phase as an individual product and determines the scale of variations in the main characteristics. Fine UDDCM fractions contain only small amounts diamond-like (sp(3) carbon) grains, if any. One possible reason for changes in the ratio between the phases is density fluctuations under nonequilibrium conditions of synthesis.
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4.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Korets A., Krylov A. S., Mironov E.
Заглавие : Structural heterogeneity of diamond-containing detonation material
Место публикации : Eur. Phys. J. - Appl. Phys. - 2010. - Vol. 52, Is. 1. - P.10901-10905. - ISSN 1286-0042, DOI 10.1051/epjap/2010126
Примечания : Cited References: 17
Предметные рубрики: NANODIAMONDS
Ключевые слова (''Своб.индексиров.''): influence of density--raman and infrared spectra--structural heterogeneity--variable ratio--detonation--diamonds--diffraction--holographic interferometry--spectroscopy--x ray diffraction--synthetic diamonds
Аннотация: Diamond-containing material (DCM) synthesized by detonation was separated into fractions. Raman and infrared spectra and X-ray diffraction patterns of the individual fractions were measured. The particles of this material were characterized by the variable ratio of the diamond (sp(3)) and non-diamond components. The distribution of sp(3)-grains in the particles was of complicated character. The fine DCM particles contained an insignificant amount of diamond. The influence of density fluctuations on the DCM formation is discussed.
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5.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Isakov V. P., Isakova V. G., Lyamkin A. I., Solntsev A. V., Gasanov Z. D.
Заглавие : Modification of chromium electrochemical coatings by detonation nanodiamonds
Коллективы : Российский федеральный ядерный центр - Всероссийский научно-исследовательский институт экспериментальной физики, "Экстремальные состояния вещества. Детонация. Ударные волны", международная конференция (2013 ; 18-22 марта; Саров), International conference "Extreme states of substance. Detonation. Shock waves" (March 18 - 22, 2013; Sarov, Russia), Харитоновские тематические научные чтения (15; 2013 ; март ; 18-22; Саров)
Место публикации : Экстремальные состояния вещества. Детонация. Ударные волны, междунар. конф.: Сб. тез. докл. - Саров, 2013. - P.392-393
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6.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Churilov G. N., Osipova I. V., Vnukova N. G., Glushchenko G. A., Petrakovskaya E. A., Kolonenko A. L., Chiganov A. S., Tomashevich Y. V., Zhyzhaev A. M.
Заглавие : Processing of detonation diamonds with metal-containing high-frequency arc plasma and their properties
Место публикации : Fuller. Nanotub. Carbon Nanostruct.: Taylor & Francis, 2012. - Vol. 20, Is. 4/7 SI. - P.611-615. - ISSN 1536-383X, DOI 10.1080/1536383X.2012.657014
Примечания : Cited References: 5. - The work was partially supported by RFBR foundation (project 09-03-00383).
Ключевые слова (''Своб.индексиров.''): nanodiamond--nanoparticle--metal-containing plasma
Аннотация: This paper describes coating of diamond powder with metal by plasma. Arc plasma was generated in double jet high-frequency argon-operated plasmatron with atomized metal inserts. The diamond powder was added to the plasma in a flow of helium. Copper and nickel coated particles of detonation and industrial diamonds were studied by XRD, XPS, SEM methods and electron magnetic resonance. Results of these studies are presented.
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7.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Korets A.Ya., Krylov A.S., Mironov E.V.
Заглавие : Structural heterogeneity detonation diamond containing mate rial
Коллективы : International Shock Interaction Symposium
Место публикации : 19th International Shock Interaction Symposium/ International Shock Interaction Symposium (19 ; 2010 ; Moscow, Russia). - 2010. - С. 19
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8.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Korets A.Ya., Krylov A.S., Mironov E.V.
Заглавие : Structural heterogeneity detonation diamond-containing mate rial
Коллективы : Chaotic modeling and Simulation International Conference
Место публикации : 3rd Chaotic modeling and Simulation International Conference: CHAOS 2010. - 2010. - С. 34
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9.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Korets A.Ya., Krylov A. S., Mironov E. V.
Заглавие : Structural Inhomogeneity of Detonation Diamond Containing Materials
Коллективы : International Conference on Equations of State for Matter, Physics of Ex treme States of Matter
Место публикации : Physics of extreme states of matter - 2010/ International Conference on Equations of State for Matter, Physics of Ex treme States of Matter (25 ; 2010 ; MAR ; 1-6 ; Elbrus, Russia). - 2010. - С. 33-34. - ISBN 978-5-901675-96-0
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Isakova V. G., Isakov V. P., Lyamkin A. I., Zharikova N. V., Yunoshev A. S., Nemtsev I. V.
Заглавие : Surface modification of detonation nanodiamonds with platinum and palladium nanoparticles
Место публикации : Int. J. Chem. - 2015. - Vol. 7, No. 1. - P.1-9. - ISSN 1916-9698, DOI 10.5539/ijc.v7n1p1
Примечания : Cited References: 38
Ключевые слова (''Своб.индексиров.''): detonation-synthesized nanodiamond supports--platinum and palladium nanoparticles--combustion--chemical modific--dnd additional purification
Аннотация: Acetylacetonates of platinum group metals (M(acac)n, acac= CH3COCHCOCH3,n - oxidation state of metal) are the most suitable precursors for use in highly effective MOCVD (metal-organic chemical vapor deposition) processes because of their thermal properties, low price of initial ligand and accessible synthesis methods. In this study we have developed a simple, scalable inexpensive, MOCVD-like approach to the deposition of Pt and Pd nanoparticle dispersions on powder detonation nanodiamonds (DND) using combustion in air of powder mixtures of DND with Pt and Pd acetylacetonates. This one-step process requires no specialized apparatus, and is conducted at mild temperatures (180°C – 250°C). The substrate surface of DND initiates chemical thermal destruction of precursor and deposition of nanoparticle networks composed of constituent particles. DND-supported Pd and Pt nanoparticles with their loading being from 10 and 5wt. % were obtained the average of particle size 20-25 nm and 7-10nm decreases with decreasing the metal loading. For additional purification and disaggregation of the commercial detonation-synthesized nanodiamond (DNDcomm) the method of annealing of the powder mixtures DNDcomm with Na(acac) have been used. The purified diamond nanoparticulates (DND), as well as DNDcomm, Pt/DND and Pd/DND, were subjected to physicochemical characterizations, such as X-ray diffraction (XRD), scanning electron microscopy (SEM), and energy dispersive X-ray (EDX) analysis.
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