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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Vasil'ev E. N., Nesterov D. A.
Заглавие : Numerical simulation of the spatial structure of a moving arc discharge
Место публикации : High Temp.: SPRINGER, 2008. - Vol. 46, Is. 6. - P746-751. - ISSN 0018-151X, DOI 10.1134/S0018151X08060023
Примечания : Cited References: 9
Ключевые слова (''Своб.индексиров.''): 52--80--mg--cavity resonators--computer simulation--discharge (fluid mechanics)--magnetic fields--three dimensional--arc discharges--current strengths--experimental datums--gas flows--magnetogasdynamics--numerical simulations--parallel electrodes--physical parameters--spatial shapes--spatial structures--state processes--transverse magnetic fields--electric discharges
Аннотация: Results are given of the calculation of the structure of an arc discharge moving on parallel electrodes in air under the effect of a transverse magnetic field (0.086 T) at a current strength of 320 A. The numerical simulation is performed within an unsteady-state three-dimensional mathematical model of radiation magnetogasdynamics. The calculations reveal that fluctuations of values of physical parameters and of spatial shape of arc arise in the arc, which are caused by the gas flow past the discharge column and by unsteady-state processes in the electrode regions. Comparison is made with the available experimental data.
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Вид документа : Статья из сборника (выпуск продолж. издания)
Шифр издания :
Автор(ы) : Karpov I. V., Ushakov A. V., Lepeshev A. A., Fedorov L. Y., Dorozhkina E. A., Karpova O. N., Shaikhadinov A. A., Demin V. G., Bachurina E. P., Lichargin D. V., Abkaryan A. K., Zeer G. M., Zharkov S. M.
Заглавие : The investigation of the influence of oxygen concentration in the gas mixture on nanodispersed oxides synthesis
Коллективы : International Scientific Conference Reshetnev Readings
Место публикации : IOP Conf. Ser.: Mater. Sci. Eng. - 2017. - Vol. 255, Is. 1. - Ст.012008. - , DOI 10.1088/1757-899X/255/1/012008
Примечания : Cited References: 25
Ключевые слова (''Своб.индексиров.''): cathodes--electrodes--particle size--vacuum applications--average particle size--cathode process--discharge gaps--energy of ions--influence of oxygen--low pressure arc--oxides synthesis--superheated gas--gases
Аннотация: Thermal effects in cathode space of low-pressure arc discharge, which contribute to the synthesis of nanopowders with an average particle size of less than 10 nm, are considered. One of the most important parameters, characterizing the cathode processes of vacuum arc, is a voltage drop across the discharge gap. All the gases demonstrate a decrease of a voltage drop across the discharge gap under the condition ofincreasing the gas pressure in the range of p = 10-3 - 1 Pa. Dissipation of energy of ions and electrons on gas molecules causes abrupt heating of the gas. Heat, coming from gas plasma, has a significant impact on evaporating material of a cathode. It can be assumed that a microdrop fraction, formed as a result of a cathode spraying in a liquid phase, will further evaporate in a superheated gas.
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Вид документа : Статья из сборника (выпуск продолж. издания)
Шифр издания :
Автор(ы) : Karpov I. V., Ushakov A. V., Lepeshev A. A., Fedorov L. Y., Dorozhkina E. A., Karpova O. N., Shaikhadinov A. A., Demin V. G., Bachurina E. P., Lichargin D. V., Abkaryan A. K., Zeer G. M., Zharkov S. M.
Заглавие : The influence of magnetic field on the rate of cathode erosion at vacuum arc spraying
Коллективы : International Scientific Conference Reshetnev Readings
Место публикации : IOP Conf. Ser.: Mater. Sci. Eng. - 2017. - Vol. 255, Is. 1. - Ст.012007. - , DOI 10.1088/1757-899X/255/1/012007
Примечания : Cited References: 27
Ключевые слова (''Своб.индексиров.''): cathodes--copper compounds--electrodes--magnetic fields--magnetism--metals--vacuum applications--vacuum technology--cathode erosion--influence of magnetic field--metal oxides--nano powders--particular condition--vacuum arcs--magnetoplasma
Аннотация: The influence of the magnetic field in the cathode space on the synthesis of metal oxide nanopowders by vacuum-arc spraying was studied. It was found that, depending on the geometry of the magnetic field and the pressure of gaseous medium in plasma-chemical reactor, particular conditions which enhance the efficiency of CuO synthesis, appear.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Voronin A. S., Simunin M. M., Fadeev, Yu. V., Ivanchenko F. S., Karpova D. V., Tambasov I. A., Khartov S. V.
Заглавие : Technological Basis of the Formation of Micromesh Transparent Electrodes by Means of a Self-Organized Template and the Study of Their Properties
Коллективы : Russian Foundation for Basic Research [18-38-00852_mol-a]
Место публикации : Tech. Phys. Lett. - 2019. - Vol. 45, Is. 4. - P.366-369. - ISSN 1063-7850, DOI 10.1134/S1063785019040187. - ISSN 1090-6533(eISSN)
Примечания : Cited References: 15. - This work was supported by the Russian Foundation for Basic Research, project no. 18-38-00852_mol-a.
Предметные рубрики: UNIFORM
Аннотация: This Letter presents the results of a study of the physical properties of micromesh transparent electrodes on a flexible substrate, obtained using a template in the form of silica layers subjected to controlled cracking. For the first time, a combined approach to the control of parameters of a micromesh structure (crack width and cell size) by varying the pH and the thickness of the sol layer is proposed. Using this approach, transparent electrodes with a surface resistance of 4.1 Ω/sq with a transparency of 85.7% were obtained. Micromesh electrodes are characterized by linear optical transmission in the visible and IR ranges, which opens up prospects for their use in optoelectronics.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Krinitsyn D. O., Romanchenko A. S., Vorob'ev S. A., Likhatskii M. N., Karacharov A. A., Krylov A. S., Volochaev M. N., Mikhlin, Yu L.
Заглавие : Synthesizing zinc sulfide films on the gold surface as the sensor for electrochemical quartz crystal microbalance
Коллективы : Russian Scientific FoundationRussian Science Foundation (RSF) [18-17-00135]
Место публикации : Russ. J. Electrochem. - 2021. - Vol. 57, Is. 12. - P.1157-1163. - ISSN 1023-1935, DOI 10.1134/S1023193521120041. - ISSN 1608-3342(eISSN)
Примечания : Cited References: 23. - The study was supported by the Russian Scientific Foundation (grant no. 18-17-00135)
Предметные рубрики: CHEMICAL BATH DEPOSITION
ZNS
SPHALERITE
ELECTRODES
ACTIVATION
Аннотация: A zinc sulfate film is deposited from aqueous solutions of zinc sulfate onto the gold surface with the aim of preparation of a sensor for electrochemical quartz crystal microbalance (EQCM). The kinetics of this process, the particles formed in solution, and the film itself are studied by the methods of electrochemical quartz crystal microbalance, X-ray photoelectron spectroscopy, transmission electron microscopy, atomic force microscopy, optical and Raman spectroscopies, and dynamic light scattering. The effect of the procedure of gold surface preparation, the reagent concentration, and the temperature on the film adhesion, the length of induction period, the kinetics of film growth, and its structure and thickness are studied. It is shown that the film formation proceeds as a result of deposition of sufficiently coarse 200-700 nm colloid particles of sphalerite. It is demonstrated that this sensor can be used in studying the electrochemical reactions of ZnS and the interface phenomena by the methods of EQCM and cyclic voltammetry.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Voronin A. S., Simunin M. M., Ivanchenko F. S., Shiverskii A. V., Fadeev, Yu. V., Tambasov I. A., Nemtsev I. V., Matsynin A. A., Khartov S. V.
Заглавие : Preparation and investigation of composite transparent electrodes of poly(3, 4-ethylenedioxythiophene) polystyrene sulfonate/single-wall carbon nanotubes
Коллективы : Russian Foundation for Basic Research [16-32-00302 mol_a]; RFBR; Government of Krasnoyarsk Krai; Krasnoyarsk Krai Foundation [16-42-243059 r_mol_a, 16-42-243006 r_mol_a, 16-48-242092 r_ofi_m]
Место публикации : Tech. Phys. Lett.: MAIK Nauka-Interperiodica / Springer, 2017. - Vol. 43, Is. 9. - P.783-786. - ISSN 1063-7850, DOI 10.1134/S1063785017090127. - ISSN 1090-6533(eISSN)
Примечания : Cited References:7. - This study was supported by the Russian Foundation for Basic Research (RFBR project no. 16-32-00302 mol_a) and jointly by the RFBR, Government of Krasnoyarsk Krai, and the Krasnoyarsk Krai Foundation for the Support of Scientific and Technological Work within scientific projects nos. 16-42-243059 r_mol_a, 16-42-243006 r_mol_a, and 16-48-242092 r_ofi_m.
Предметные рубрики: SOLAR-CELLS
Аннотация: The preparation of composite transparent electrodes of poly(3, 4-ethylenedioxythiophene) polystyrene sulfonate/single-wall carbon nanotubes by the spray method is described. The influence of the successive treatment of each functional layer in acid media with different activities on the optical and electric film characteristics is considered. The composite with the surface resistance of 89 Ω/sq at the transparency of 85.3% (550 nm) on a polymer substrate is obtained.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mikhlin Y. L., Vishnyakova E. A., Romanchenko A. S., Saikova S. V., Likhatski M. N., Larichev Y. V., Tuzikov F. V., Zaikovskii V. I., Zharkov S. M.
Заглавие : Oxidation of Ag nanoparticles in aqueous media: Effect of particle size and capping
Место публикации : Appl. Surf. Sci.: Elsevier Science, 2014. - Vol. 297. - P.75-83. - ISSN 0169-4332, DOI 10.1016/j.apsusc.2014.01.081. - ISSN 1873-5584
Примечания : Cited References: 58. - This work was partially financially supported by the Ministry of Education and Science of RF (Grant 8580) and RFBR (12-03-31178).
Предметные рубрики: EX-SITU XPS
POLYCRYSTALLINE SILVER ELECTRODES
RAY PHOTOELECTRON-SPECTROSCOPY
METAL NANOPARTICLES
ELECTROCHEMICAL OXIDATION
ABSORPTION SPECTROSCOPY
PYROLYTIC-GRAPHITE
OXYGEN-ADSORPTION
TRANSFORMATIONS
DISSOLUTION
Ключевые слова (''Своб.индексиров.''): silver nanoparticles--oxidation--resistive switching effect--x-ray photoelectron spectroscopy
Аннотация: Many applications and environmental impact of silver-bearing nanomaterials critically depend upon their specific reactivity, which is still poorly understood. Here, silver nanoparticles (Ag NPs) of about 3-5 nm and 10-12 nm in diameter, uncapped and capped with l-glucose or citrate, were prepared, characterized using UV-vis absorption spectroscopy, SAXS, TEM, and their (electro) chemical oxidation was examined in comparison with each other and bulk metal applying scanning tunneling microscopy and spectroscopy, cyclic voltammetry, and XPS. A resistive switching effect was found in the tunneling spectra measured in air at the smaller uncapped Ag NPs deposited on HOPG and was interpreted in terms of Ag transfer between the particle and the probe. The anodic oxidation of these Ag NPs in 1 M NaOH yielded 3D Ag2O, while only a layer of "primary"Ag(I) oxide emerged on larger uncapped nanoparticles during the potential sweep. The formation of AgO at higher potentials proceeded readily at the "primary"oxide but was retarded at the smaller NPs. The citrate- and glucose-capping substantially impeded the formation both of Ag2O and AgO. The findings highlighted, particularly, a non-trivial effect of particle size and transient mobilization of Ag species on the reactions of silver nanoparticles. (c) 2014 Elsevier B.V. All rights reserved.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Lepeshev A. A., Drokin N. A., Ushakov A. V., Karpov I. V., Fedorov L. Y., Bachurina E. P.
Заглавие : Localization and transfer of charge carriers in CuO nanopowder by impedance spectroscopy
Место публикации : J. Mater. Sci.: Mater. Electron. - 2018. - Vol. 29, Is. 14. - P.12118–12125. - ISSN 09574522 (ISSN), DOI 10.1007/s10854-018-9319-2
Примечания : Cited References: 26. - The work was performed with a support of the Grant of the Russian Science Foundation (Project No. 16-19-10054).
Ключевые слова (''Своб.индексиров.''): copper oxides--electric charge--electric fields--electrodes--metal nanoparticles--permittivity--spectroscopy
Аннотация: Particular electro-physical characteristics of CuO nanopowder were investigated by impedance spectroscopy using a sensor based on interdigitated structure in the frequency range from 1 Hz to 100 MHz. The results of investigation were considered. Simulation of impedance spectra by equivalent electric circuits was carried out for numerical approximations of the frequency dependences of the dielectrical permittivity and conductivity. Electric charge accumulation of on the boundaries of nanoparticles and near the metal electrodes of the sensor was revealed. It was shown that a double electric layer is formed near the electrodes, which leads to the appearance of anomalously large values of dielectrical permittivity and an increase in the conductivity in the low-frequency region. The obtained results can be explained by proton conductivity in the nanopowder caused by moisture which is adsorbed on the surface of the nanoparticles. It was shown that after high-temperature annealing of CuO nanopowders, accumulation of electric charges was not observed. It was established that hopping or polaron conductivity occurs in the annealed CuO samples, which increases with increasing electric field frequency according to the power law with a fractional exponent.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Voronin, Anton S., Nemtsev I. V., Molokeev M. S., Simunin, Mikhail M., Kozlova, Ekaterina A., Markovskaya, Dina V., Lebedev, Denis V., Lopatin, Dmitry S., Khartov, Stanislav V.
Заглавие : Laser-induced chemical liquid-phase deposition plasmonic gold nanoparticles on porous TiO2 fIlm with great photoelectrochemical performance
Место публикации : Appl. Sci. - 2022. - Vol. 12, Is. 1. - Ст.30. - ISSN 2076-3417(eISSN), DOI 10.3390/app12010030
Примечания : Cited References: 35
Предметные рубрики: AU NANOPARTICLES
ELECTRODES
Аннотация: This paper considers the photoelectrochemical characteristics of a composite porous TiO2 thin film with deposited plasmonic gold nanoparticles. The deposition of gold nanoparticles was carried out by the laser-induced chemical liquid-phase deposition (LCLD) method. The structural characteristics of the composite have been studied; it has been shown that the porous TiO2 film has a lattice related to the tetragonal system and is in the anatase phase. Gold nanoparticles form on the surface of a porous TiO2 film. A complex of photoelectrochemical measurements was carried out. It was shown that the deposition of plasmonic gold nanoparticles led to a significant increase in the photocurrent density by ~820%. The proposed concept is aimed at testing the method of forming a uniform layer of plasmonic gold nanoparticles on a porous TiO2 film, studying their photocatalytic properties for further scaling, and obtaining large area Au/TiO2/FTO photoelectrodes, including in the roll-to-roll process.
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Padamata, Sai Krishna, Yasinskiy, Andrey, Shabanov A. V., Bermeshev, Timofey, Yang, You-jian, Wang, Zhao-wen, Cao, Dao, Polyakov, Peter
Заглавие : Improving corrosion resistance of Cu-Al-based anodes in KF-AlF3-Al2O3 melts
Коллективы : State Assignment for the Science of Siberian Federal University, Russia [FSRZ-2020-0013]
Место публикации : Trans. Nonferrous Met. Soc. China. - 2022. - Vol. 32, Is. 1. - P.354-363. - ISSN 1003-6326, DOI 10.1016/S1003-6326(22)65800-X. - ISSN 2210-3384(eISSN)
Примечания : Cited References: 24. - The work is performed as a part of the State Assignment for the Science of Siberian Federal University, Russia (No. FSRZ-2020-0013) . Use of Krasnoyarsk Regional Center of Research Equipment of Federal Research Center "Krasnoyarsk Science Center SB RAS" is acknowledged
Предметные рубрики: NI-FE
ALUMINUM ELECTROLYSIS
INERT ANODES
NICKEL FERRITE
BEHAVIOR
Аннотация: The anodic behaviour of pre-oxidised and non-oxidised Cu−Al-based anodes (Cu−10Al and Cu−9.8Al−2Mn) in KF−AlF3−Al2O3 melts was studied through galvanostatic and potentiodynamic polarization techniques. The alloy compositions were oxidised for a short-term (8 h) at 700 °C, followed by galvanostatic polarization for 1 h at 800 °C with an applied current density of 0.4 A/cm2. The potentiodynamic curves were recorded with a sweep rate of 0.01 V/s. XRD analysis was conducted on frozen melt samples collected on the surface of the anode, and SEM observation was performed on the anode after the experiment to study the phases of the scales formed on the alloys. All the anode materials had a steady potential between 2.30 and 2.50 V(vs Al/AlF3). The corrosion rates of the anodes were calculated from the data acquired through potentiodynamic polarization. It was seen that pre-oxidised anodes possess a low corrosion rate compared to those without pre-oxidation treatment.
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