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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mikhlin Y. L., Vishnyakova E. A., Romanchenko A. S., Saikova S. V., Likhatski M. N., Larichev Y. V., Tuzikov F. V., Zaikovskii V. I., Zharkov S. M.
Заглавие : Oxidation of Ag nanoparticles in aqueous media: Effect of particle size and capping
Место публикации : Appl. Surf. Sci.: Elsevier Science, 2014. - Vol. 297. - P.75-83. - ISSN 0169-4332, DOI 10.1016/j.apsusc.2014.01.081. - ISSN 1873-5584
Примечания : Cited References: 58. - This work was partially financially supported by the Ministry of Education and Science of RF (Grant 8580) and RFBR (12-03-31178).
Предметные рубрики: EX-SITU XPS
POLYCRYSTALLINE SILVER ELECTRODES
RAY PHOTOELECTRON-SPECTROSCOPY
METAL NANOPARTICLES
ELECTROCHEMICAL OXIDATION
ABSORPTION SPECTROSCOPY
PYROLYTIC-GRAPHITE
OXYGEN-ADSORPTION
TRANSFORMATIONS
DISSOLUTION
Ключевые слова (''Своб.индексиров.''): silver nanoparticles--oxidation--resistive switching effect--x-ray photoelectron spectroscopy
Аннотация: Many applications and environmental impact of silver-bearing nanomaterials critically depend upon their specific reactivity, which is still poorly understood. Here, silver nanoparticles (Ag NPs) of about 3-5 nm and 10-12 nm in diameter, uncapped and capped with l-glucose or citrate, were prepared, characterized using UV-vis absorption spectroscopy, SAXS, TEM, and their (electro) chemical oxidation was examined in comparison with each other and bulk metal applying scanning tunneling microscopy and spectroscopy, cyclic voltammetry, and XPS. A resistive switching effect was found in the tunneling spectra measured in air at the smaller uncapped Ag NPs deposited on HOPG and was interpreted in terms of Ag transfer between the particle and the probe. The anodic oxidation of these Ag NPs in 1 M NaOH yielded 3D Ag2O, while only a layer of "primary"Ag(I) oxide emerged on larger uncapped nanoparticles during the potential sweep. The formation of AgO at higher potentials proceeded readily at the "primary"oxide but was retarded at the smaller NPs. The citrate- and glucose-capping substantially impeded the formation both of Ag2O and AgO. The findings highlighted, particularly, a non-trivial effect of particle size and transient mobilization of Ag species on the reactions of silver nanoparticles. (c) 2014 Elsevier B.V. All rights reserved.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Voronin A. S., Ivanchenko F. S., Simunin M. M., Shiverskiy A. V., Aleksandrovsky A. S., Nemtsev I. V., Fadeev Y. V., Karpova D. V., Khartov S. V.
Заглавие : High performance hybrid rGO/ Ag quasi-periodic mesh transparent electrodes for flexible electrochromic devices
Место публикации : Appl. Surf. Sci.: Elsevier Science, 2016. - Vol. 364. - P.931–937. - ISSN 0169-4332, DOI 10.1016/j.apsusc.2015.12.182. - ISSN 1873-5584
Примечания : Cited References: 31
Предметные рубрики: NANOWIRE NETWORKS
GRAPHENE FILMS
OXIDE
OXIDATION
HEATERS
Ключевые слова (''Своб.индексиров.''): quasi-periodic mesh transparent electrode self-organized template--reduced graphene oxide (rgo)--flexible electrochromic device
Аннотация: A possibility of creating a stable hybrid coating based on the hybrid of a reduced graphene oxide (rGO)/ Ag quasi-periodic mesh (q-mesh) coating has been demonstrated. The main advantages of the suggested method are the low cost of the processes and the technology scalability. The Ag q-mesh coating is formed by means of the magnetron sputtering of silver on the original template obtained as a result of quasi-periodic cracking of a silica film. The protective rGO film is formed by low temperature reduction of a graphene oxide (GO) film, applied by the spray-deposition in the solution of NaBH4. The coatings have low sheet resistance (12.3 Ω/sq) and high optical transparency (82.2%). The hybrid coating are characterized by high chemical stability, as well as they show high stability to deformation impacts. High performance of the hybrid coatings as electrodes in the sandwich-system «electrode – electrochromic composition – electrode» has been demonstrated. The hybrid electrodes allow the electrochromic sandwich to function without any visible degradation for a long time, while an unprotected mesh electrode does not allow performing even a single switching cycle.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Vasil'ev E. N., Nesterov D. A.
Заглавие : Numerical simulation of the spatial structure of a moving arc discharge
Место публикации : High Temp.: SPRINGER, 2008. - Vol. 46, Is. 6. - P746-751. - ISSN 0018-151X, DOI 10.1134/S0018151X08060023
Примечания : Cited References: 9
Ключевые слова (''Своб.индексиров.''): 52--80--mg--cavity resonators--computer simulation--discharge (fluid mechanics)--magnetic fields--three dimensional--arc discharges--current strengths--experimental datums--gas flows--magnetogasdynamics--numerical simulations--parallel electrodes--physical parameters--spatial shapes--spatial structures--state processes--transverse magnetic fields--electric discharges
Аннотация: Results are given of the calculation of the structure of an arc discharge moving on parallel electrodes in air under the effect of a transverse magnetic field (0.086 T) at a current strength of 320 A. The numerical simulation is performed within an unsteady-state three-dimensional mathematical model of radiation magnetogasdynamics. The calculations reveal that fluctuations of values of physical parameters and of spatial shape of arc arise in the arc, which are caused by the gas flow past the discharge column and by unsteady-state processes in the electrode regions. Comparison is made with the available experimental data.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Voronin A. S., Simunin M. M., Ivanchenko F. S., Shiverskii A. V., Fadeev, Yu. V., Tambasov I. A., Nemtsev I. V., Matsynin A. A., Khartov S. V.
Заглавие : Preparation and investigation of composite transparent electrodes of poly(3, 4-ethylenedioxythiophene) polystyrene sulfonate/single-wall carbon nanotubes
Коллективы : Russian Foundation for Basic Research [16-32-00302 mol_a]; RFBR; Government of Krasnoyarsk Krai; Krasnoyarsk Krai Foundation [16-42-243059 r_mol_a, 16-42-243006 r_mol_a, 16-48-242092 r_ofi_m]
Место публикации : Tech. Phys. Lett.: MAIK Nauka-Interperiodica / Springer, 2017. - Vol. 43, Is. 9. - P.783-786. - ISSN 1063-7850, DOI 10.1134/S1063785017090127. - ISSN 1090-6533(eISSN)
Примечания : Cited References:7. - This study was supported by the Russian Foundation for Basic Research (RFBR project no. 16-32-00302 mol_a) and jointly by the RFBR, Government of Krasnoyarsk Krai, and the Krasnoyarsk Krai Foundation for the Support of Scientific and Technological Work within scientific projects nos. 16-42-243059 r_mol_a, 16-42-243006 r_mol_a, and 16-48-242092 r_ofi_m.
Предметные рубрики: SOLAR-CELLS
Аннотация: The preparation of composite transparent electrodes of poly(3, 4-ethylenedioxythiophene) polystyrene sulfonate/single-wall carbon nanotubes by the spray method is described. The influence of the successive treatment of each functional layer in acid media with different activities on the optical and electric film characteristics is considered. The composite with the surface resistance of 89 Ω/sq at the transparency of 85.3% (550 nm) on a polymer substrate is obtained.
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Вид документа : Статья из сборника (выпуск продолж. издания)
Шифр издания :
Автор(ы) : Karpov I. V., Ushakov A. V., Lepeshev A. A., Fedorov L. Y., Dorozhkina E. A., Karpova O. N., Shaikhadinov A. A., Demin V. G., Bachurina E. P., Lichargin D. V., Abkaryan A. K., Zeer G. M., Zharkov S. M.
Заглавие : The influence of magnetic field on the rate of cathode erosion at vacuum arc spraying
Коллективы : International Scientific Conference Reshetnev Readings
Место публикации : IOP Conf. Ser.: Mater. Sci. Eng. - 2017. - Vol. 255, Is. 1. - Ст.012007. - , DOI 10.1088/1757-899X/255/1/012007
Примечания : Cited References: 27
Ключевые слова (''Своб.индексиров.''): cathodes--copper compounds--electrodes--magnetic fields--magnetism--metals--vacuum applications--vacuum technology--cathode erosion--influence of magnetic field--metal oxides--nano powders--particular condition--vacuum arcs--magnetoplasma
Аннотация: The influence of the magnetic field in the cathode space on the synthesis of metal oxide nanopowders by vacuum-arc spraying was studied. It was found that, depending on the geometry of the magnetic field and the pressure of gaseous medium in plasma-chemical reactor, particular conditions which enhance the efficiency of CuO synthesis, appear.
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Вид документа : Статья из сборника (выпуск продолж. издания)
Шифр издания :
Автор(ы) : Karpov I. V., Ushakov A. V., Lepeshev A. A., Fedorov L. Y., Dorozhkina E. A., Karpova O. N., Shaikhadinov A. A., Demin V. G., Bachurina E. P., Lichargin D. V., Abkaryan A. K., Zeer G. M., Zharkov S. M.
Заглавие : The investigation of the influence of oxygen concentration in the gas mixture on nanodispersed oxides synthesis
Коллективы : International Scientific Conference Reshetnev Readings
Место публикации : IOP Conf. Ser.: Mater. Sci. Eng. - 2017. - Vol. 255, Is. 1. - Ст.012008. - , DOI 10.1088/1757-899X/255/1/012008
Примечания : Cited References: 25
Ключевые слова (''Своб.индексиров.''): cathodes--electrodes--particle size--vacuum applications--average particle size--cathode process--discharge gaps--energy of ions--influence of oxygen--low pressure arc--oxides synthesis--superheated gas--gases
Аннотация: Thermal effects in cathode space of low-pressure arc discharge, which contribute to the synthesis of nanopowders with an average particle size of less than 10 nm, are considered. One of the most important parameters, characterizing the cathode processes of vacuum arc, is a voltage drop across the discharge gap. All the gases demonstrate a decrease of a voltage drop across the discharge gap under the condition ofincreasing the gas pressure in the range of p = 10-3 - 1 Pa. Dissipation of energy of ions and electrons on gas molecules causes abrupt heating of the gas. Heat, coming from gas plasma, has a significant impact on evaporating material of a cathode. It can be assumed that a microdrop fraction, formed as a result of a cathode spraying in a liquid phase, will further evaporate in a superheated gas.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Lepeshev A. A., Drokin N. A., Ushakov A. V., Karpov I. V., Fedorov L. Y., Bachurina E. P.
Заглавие : Localization and transfer of charge carriers in CuO nanopowder by impedance spectroscopy
Место публикации : J. Mater. Sci.: Mater. Electron. - 2018. - Vol. 29, Is. 14. - P.12118–12125. - ISSN 09574522 (ISSN), DOI 10.1007/s10854-018-9319-2
Примечания : Cited References: 26. - The work was performed with a support of the Grant of the Russian Science Foundation (Project No. 16-19-10054).
Ключевые слова (''Своб.индексиров.''): copper oxides--electric charge--electric fields--electrodes--metal nanoparticles--permittivity--spectroscopy
Аннотация: Particular electro-physical characteristics of CuO nanopowder were investigated by impedance spectroscopy using a sensor based on interdigitated structure in the frequency range from 1 Hz to 100 MHz. The results of investigation were considered. Simulation of impedance spectra by equivalent electric circuits was carried out for numerical approximations of the frequency dependences of the dielectrical permittivity and conductivity. Electric charge accumulation of on the boundaries of nanoparticles and near the metal electrodes of the sensor was revealed. It was shown that a double electric layer is formed near the electrodes, which leads to the appearance of anomalously large values of dielectrical permittivity and an increase in the conductivity in the low-frequency region. The obtained results can be explained by proton conductivity in the nanopowder caused by moisture which is adsorbed on the surface of the nanoparticles. It was shown that after high-temperature annealing of CuO nanopowders, accumulation of electric charges was not observed. It was established that hopping or polaron conductivity occurs in the annealed CuO samples, which increases with increasing electric field frequency according to the power law with a fractional exponent.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Voronin A. S., Simunin M. M., Fadeev, Yu. V., Ivanchenko F. S., Karpova D. V., Tambasov I. A., Khartov S. V.
Заглавие : Technological Basis of the Formation of Micromesh Transparent Electrodes by Means of a Self-Organized Template and the Study of Their Properties
Коллективы : Russian Foundation for Basic Research [18-38-00852_mol-a]
Место публикации : Tech. Phys. Lett. - 2019. - Vol. 45, Is. 4. - P.366-369. - ISSN 1063-7850, DOI 10.1134/S1063785019040187. - ISSN 1090-6533(eISSN)
Примечания : Cited References: 15. - This work was supported by the Russian Foundation for Basic Research, project no. 18-38-00852_mol-a.
Предметные рубрики: UNIFORM
Аннотация: This Letter presents the results of a study of the physical properties of micromesh transparent electrodes on a flexible substrate, obtained using a template in the form of silica layers subjected to controlled cracking. For the first time, a combined approach to the control of parameters of a micromesh structure (crack width and cell size) by varying the pH and the thickness of the sol layer is proposed. Using this approach, transparent electrodes with a surface resistance of 4.1 Ω/sq with a transparency of 85.7% were obtained. Micromesh electrodes are characterized by linear optical transmission in the visible and IR ranges, which opens up prospects for their use in optoelectronics.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Voronin A. S., Fadeev Y. V., Govorun I. V., Podshivalov I. V., Simunin M. M., Tambasov I. A., Karpova D. V., Smolyarova T. E., Lukyanenko A. V., Karacharov A. A., Nemtsev I. V., Khartov S. V.
Заглавие : Cu-Ag and Ni-Ag meshes based on cracked template as efficient transparent electromagnetic shielding coating with excellent mechanical performance
Коллективы : Russian Foundation for Basic Research projectRussian Foundation for Basic Research (RFBR) [18-38-00852]; Russian FederationRussian Federation [SP-2235.2019.1]
Место публикации : J. Mater. Sci. - 2021. - Vol. 56. Is. 26. - P.14741-14762. - ISSN 0022-2461, DOI 10.1007/s10853-021-06206-4. - ISSN 1573-4803(eISSN)
Примечания : Cited References: 79. - This work was supported by Russian Foundation for Basic Research project «mol_a» № 18-38-00852 and a scholarship from the President of the Russian Federation SP-2235.2019.1. The sputtering Ag seed mesh and physicochemical analysis of materials was carried out on the equipment of Krasnoyarsk Regional Center of Research Equipment of Federal Research Center «Krasnoyarsk Science Center SB RAS»
Предметные рубрики: COPPER NANOWIRES
METALLIC MESH
PLASTIC SUBSTRATE
ELECTRODES
FILMS
Аннотация: Nowadays, the technical advances call for efficient electromagnetic interference (EMI) shielding of transparent devices which may be subject to data theft. We developed Cu–Ag and Ni–Ag meshes on flexible PET substrate for highly efficiency transparent EMI shielding coating. Cu–Ag and Ni–Ag meshes obtained with galvanic deposition of copper and nickel on thin Ag seed mesh which was made by cracked template method. Coefficients S11, S21 and shielding efficiency (SE) were measured for Cu–Ag and Ni–Ag meshes in X-band (8–12 GHz) and K-band (18–26.5 GHz). 90 s copper deposition increase SE from 23.2 to 43.7 dB at 8 GHz with a transparency of 82.2% and a sheet resistance of 0.25 Ω/sq. The achieved maximum SE was 47.6 dB for Cu–Ag mesh with 67.8% transparency and 41.1 dB for Ni–Ag mesh with 77.8% transparency. Cu–Ag and Ni–Ag meshes have high bending and long-term stability. Minimum bend radius is lower than 100 µm. This effect allows to produce different forms of transparent shielding objects, for example, origami method. Our coatings are the leading among all literary solutions in three-dimensional coordinates: of sheet resistance–optical transmittance–cost of produced.
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Krinitsyn D. O., Romanchenko A. S., Vorob'ev S. A., Likhatskii M. N., Karacharov A. A., Krylov A. S., Volochaev M. N., Mikhlin, Yu L.
Заглавие : Synthesizing zinc sulfide films on the gold surface as the sensor for electrochemical quartz crystal microbalance
Коллективы : Russian Scientific FoundationRussian Science Foundation (RSF) [18-17-00135]
Место публикации : Russ. J. Electrochem. - 2021. - Vol. 57, Is. 12. - P.1157-1163. - ISSN 1023-1935, DOI 10.1134/S1023193521120041. - ISSN 1608-3342(eISSN)
Примечания : Cited References: 23. - The study was supported by the Russian Scientific Foundation (grant no. 18-17-00135)
Предметные рубрики: CHEMICAL BATH DEPOSITION
ZNS
SPHALERITE
ELECTRODES
ACTIVATION
Аннотация: A zinc sulfate film is deposited from aqueous solutions of zinc sulfate onto the gold surface with the aim of preparation of a sensor for electrochemical quartz crystal microbalance (EQCM). The kinetics of this process, the particles formed in solution, and the film itself are studied by the methods of electrochemical quartz crystal microbalance, X-ray photoelectron spectroscopy, transmission electron microscopy, atomic force microscopy, optical and Raman spectroscopies, and dynamic light scattering. The effect of the procedure of gold surface preparation, the reagent concentration, and the temperature on the film adhesion, the length of induction period, the kinetics of film growth, and its structure and thickness are studied. It is shown that the film formation proceeds as a result of deposition of sufficiently coarse 200-700 nm colloid particles of sphalerite. It is demonstrated that this sensor can be used in studying the electrochemical reactions of ZnS and the interface phenomena by the methods of EQCM and cyclic voltammetry.
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