Библиотека института физики им. Л.В. Киренского СО РАН

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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Krylova S. N., Chernyshev V. А., Ruseikina A. V., Grigoriev M. V., Aleksandrovskiy A. S., Krylov A. S.
Заглавие : Raman spectroscopy of SrLnCuS3 (Ln = La, Nd, Tm): experiment and ab initio calculation
Коллективы : International Feofilov symposium on spectroscopy of crystals doped with rare earth and transition metal ions, Физический институт им. П.Н. Лебедева РАН, Институт спектроскопии РАН
Место публикации : XVIII International Feofilov symposium on spectroscopy of crystals doped with rare earth and transition metal ions (IFS-2022): book of abstracts : Aug. 22-27, 2022, Moscow, Russia. - 2022. - P.71-72. - ISBN 978-5-89513-513-6
Примечания : Библиогр.: 8. - The work of Krylova S. was financially supported by the Russian Foundation for Basic Research and DFG project number No 21-52-12018. The research of Ruseikina A. was supported by the Tyumen region within the framework of the grant agreement in the form of a grant to non-profit organizations no. 89-don dated 07.12.2020. Chernyshev V. thanks the Ministry of Science and Higher Education of the Russian Federation (project no. FEUZ-2020-0054) for financial support.
Аннотация: The Raman spectra of SrLaCuS3, SrNdCuS3, SrTmCuS3 compounds have been investigated. Ab initio calculations of the crystal structure and phonon spectrum of the compounds have been carried out. The types and wave numbers of the fundamental modes have been determined. The experimental Raman spectra have been interpreted.
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Вид документа : Статья из сборника (выпуск продолж. издания)
Шифр издания :
Автор(ы) : Muzalevskiy K. V., Mikhaylov M. I., Ruzicka Z.
Заглавие : Synthesizing of ultra-wide band impulse by means of a log-periodic dipole antenna. Case study for a radar stand experiment
Коллективы : IEEE International Multi-Conference on Engineering, Computer and Information Sciences 2022
Место публикации : 2022 IEEE International Multi-Conference on Engineering, Computer and Information Sciences, SIBIRCON 2022: IEEE, 2022. - P.1140-1143. - , DOI 10.1109/SIBIRCON56155.2022.10017008
Примечания : Cited References: 20. - The investigation supported by the Russian Science Foundation and the Krasnoyarsk Regional Science Foundation, project № 22-17-20042
Аннотация: In this work, the approach of ultra-wide band pulses synthesizing is proposed using a broadband low-cost log-periodic dipole antenna and a vector network analyzer. Synthesis of UWB pulse (duration of 2.2ns) became possible due to minimization of antenna dispersion by compensation of amplitude and phase-frequency distortions introduced by the antenna into radiated and received pulse. The method had been developed for a down-looking antenna in a monostatic radar configuration. The antenna return loss was calculated using the model of two-port linear network with S-parameters. To calibrate the model, an original amplitude-phase method was proposed that requires measuring the antenna's return loss when the antenna is located only at several heights above the reflecting surface (metal sheet). In this case, the antenna return loss in an empty room does not need to be measured. The proposed method for synthesizing UWB pulses does not require changes in the design of the antenna and can be implemented as an additional software calibration of the antenna-feeder path. The proposed method of UWB pulses synthesizing can be implemented using miniature, low-cost vector network analyzers for environment remote sensing from unmanned aerial vehicle using the UWB impulses.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Korzhneva K. E., Bekenev V. L., Khyzhun O. Y., Goloshumova A. A., Tarasova A. Y., Molokeev M. S., Isaenko L. I., Kurus A. F.
Заглавие : Single crystal growth and the electronic structure of Rb2Na(NO3)3: Experiment and theory
Место публикации : J. Solid State Chem. - 2021. - Vol. 294. - Ст.121910. - ISSN 00224596 (ISSN), DOI 10.1016/j.jssc.2020.121910
Примечания : Cited References: 54. - This work was done on state assignment of IGM SB RAS, Ministry of Science and Higher Education of the Russian Federation; NSU BCH-2020-0036-4 (10988) (XRD analysis), and was supported by Russian Foundation for Basic Research (grants Nos. 18-32-00359 , 19-42-540012)
Аннотация: Rb2Na(NO3)3 crystals demonstrate nonlinear optical properties and can be used as a converter of laser radiation in the shortwave region. The crystals were grown in the present work by the Bridgman–Stockbarger method in a ratio of 75 wt%(RbNO3) and 25 wt%(NaNO3). After the growth, a transparent centimeter size single crystal (6 cm long) was obtained for the first time that is very important for its practical application. The unit cell volume of double Rb2Na(NO3)3 nitrate is intermediate between the cell volumes of simple rubidium and sodium nitrates, RbNO3 and NaNO3. Electronic structure of Rb2Na(NO3)3 was studied in the present work from both experimental and theoretical viewpoints. In particular, employing X-ray photoelectron spectroscopy, we have measured binding energies of core electrons and energy distribution of the electronic states within the valence band region of the Rb2Na(NO3)3 crystal and established rather big binding energies for N 1s and O 1s core-level electrons. The bombardment of middle-energy Ar+ ions induces transformation of some nitrogen atoms of the analyzing topmost layers of the Rb2Na(NO3)3 crystal surface from the NO3– group to the NO2– group. To explore in detail the filling of the valence band of Rb2Na(NO3)3 by electronic states associated with constituting atoms, we use first-principles calculations within a density functional theory (DFT) framework. The DFT calculations reveal that O 2p states are the principal contributors to the valence band bringing the main input in its upper portion. The theoretical finding is supported experimentally by fitting the X-ray photoelectron valence band spectrum and the X-ray emission O Kα band on the total energy scale. The conduction band bottom of Rb2Na(NO3)3 is composed by unoccupied O 2p and N 2p states in almost equal proportion.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Ryzhkov I. I., Kharchenko I. A., Mikhlina E. V., Minakov A. V., Guzei D. V., Nemtsev I. V., Volochaev M. N., Korobko A. V., Simunin M. M.
Заглавие : Growth of carbon nanotubes inside porous anodic alumina membranes: Simulation and experiment
Место публикации : Int. J. Heat Mass Transf. - 2021. - Vol. 176. - Ст.121414. - ISSN 00179310 (ISSN), DOI 10.1016/j.ijheatmasstransfer.2021.121414
Примечания : Cited References: 57. - This work is supported by the Russian Foundation for Basic Research, Project 18-29-19078
Аннотация: Porous anodic alumina (PAA) membranes represent a widely used and extensively studied template for production of carbon nanotubes (CNT). The PAA–CNT membranes possess a number of unique properties, such as controllable nanotube geometry, size– and chemically–based selectivity as well as high water permeability. In this work, we first propose a combination of gas phase and surface reaction models to quantitatively describe the growth of carbon nanotubes in PAA membranes in a commercial CVD reactor. A complimentary experimental study of CNT formation from ethanol precursor with argon as a carrier gas is performed. A new method for characterizing carbon nanotubes geometry by SEM and TEM image processing of membrane cross–sections is proposed. The simulations show that the carbon growth rate (in nm/min) averaged over the membrane remains constant during the deposition process until the pore diameter becomes relatively small, and rapidly falls to zero after that. The carbon nanotube thickness near the membrane surface is slightly higher than that in the membrane center. The carbon growth rate increases with synthesis temperature and pressure, while it decreases with the argon flow rate. The dependence of carbon growth rate on the ethanol/water flow rate reaches maximum at some intermediate value. These results are supported by the experimental data obtained from SEM/TEM image processing. It is found that the SEM data provide overestimated values of nanotube diameter and thickness in comparison with the TEM data. The obtained results provide new insights into the CNT growth kinetics in nanoporous media, and develop quantitative guidelines for synthesis of CNT–PAA membranes with precisely controlled nanopore geometry. It also validates the combined homogenous / heterogeneous reaction model by comparison with carbon deposition kinetics on a nanometer scale.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Ryzhkov, Ilya I., Shchurkina, Margarita A., Mikhlina, Elena, V, Simunin, Mikhail M., Nemtsev I. V.
Заглавие : Switchable ionic selectivity of membranes with electrically conductive surface: Theory and experiment
Коллективы : Russian Foundation for Basic ResearchRussian Foundation for Basic Research (RFBR) [18-38-20046]
Место публикации : Electrochim. Acta. - 2021. - Vol. 375. - Ст.137970. - ISSN 0013-4686, DOI 10.1016/j.electacta.2021.137970. - ISSN 1873-3859(eISSN)
Примечания : Cited References: 67. - This work is supported by the Russian Foundation for Basic Research , Project 18-38-20046 . The physicochemical analysis of materials was carried out in Krasnoyarsk Regional Center of Research Equipment of Federal Research Center 'Krasnoyarsk Science Center SB RAS'
Аннотация: Nanoporous membranes with electrically conductive surface represent an important class of stimuli–responsive materials. The variation of surface potential provides a powerful tool for adjusting ionic selectivity, conductivity, and rejection. This work is devoted to the theoretical and experimental study of switchable ionic selectivity. The one–dimensional Space charge (SC) and two–dimensional Uniform potential (UP) models are first generalized to constant surface potential case taking into account the Stern layer with inner (iHp) and outer (oHp) Helmholtz planes. The ionic selectivity is investigated experimentally by measuring the membrane potential at zero current for C–Nafen membranes prepared from alumina nanofibers with conductive carbon coating. The evolution of charging current is used to determine the dependence of surface charge density and differential capacitance on the applied potential. These data are fitted by the UP and SC models to find the Stern layer capacitance. It is shown that the variation of surface potential results in a continuous change of ionic selectivity from anion to cation. The membrane potential data are fitted by the UP and SC models using the chemical charge density and concentration boundary layer thickness as fitting parameters. It allows to determine the potential, at which the membrane becomes non–selective. The SC and UP models provide close results for membrane potential and surface charge density and demonstrate a good agreement with the experimental data. The UP model overestimates the solution velocity and ion concentrations at the membrane surface, while it underestimates the ion fluxes and iHp/oHp potentials. This work essentially extends our understanding of ion transport in stimuli–responsive membranes operated by the electric field. The results can be applied in the area of nanofiltration, (reverse) electrodialysis, electrochemical sensors, and nanofluidic devices.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Krylova S. N., Aleksandrovsky A. S., Roginskii E. M., Krylov A. A., Gudim I. A., Vtyurin A. N.
Заглавие : Optical properties of the HoGa3(BO3)4 crystal: experiment and ab initio calculation
Место публикации : Ferroelectrics. - 2020. - Vol. 559, Is. 1. - P.135-140. - ISSN 00150193 (ISSN), DOI 10.1080/00150193.2020.1722015
Примечания : Cited References: 22. - This work was supported by the Russian Foundation for Basic Research (grant No 18-02-00754)
Аннотация: Single crystal of HoGa3(BO3)4 has been grown using solution-melt synthesis. The optical band gap determined from the measured absorption spectrum is due to direct allowed transition and equals to 4.14 eV. The optical properties of this crystal are calculated by the plane-wave pseudo-potential method based on density functional theory. The structure of the crystal has been optimized. The electronic structure of HoGa3(BO3)4 is calculated. The experimental and theoretical fundamental absorption spectra are compared. The calculated bandgap is in good agreement with the experimental data.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Музалевский, Константин Викторович
Заглавие : Дистанционное измерение профилей влажности в пахотном слое почвы на основе поляриметрических наблюдений коэффициента отражения в P- и C-диапазонах частот. Эксперимент
Место публикации : Соврем. проблемы дистанц. зондир. Земли из космоса. - 2020. - Т. 17, № 3. - С. 145-148. - ISSN 2070-7401 (ISSN), DOI 10.21046/2070-7401-2020-17-3-145-148. - ISSN 2411-0280 (eISSN)
Примечания : Библиогр.: 5. - Работа выполнена в рамках проекта Российского фонда фундаментальных исследований № 18-05-00405, методика измерения коэффициентов отражения была развита при поддержке проекта государственного задания № 0356-2019-0004
Аннотация: В данном сообщении экспериментально подтверждена принципиальная возможность дистанционного измерения профилей влажности в пахотном слое почвы с пригодной для практического применения точностью на основе поляриметрических измерений коэффициента отражения на двух частотах 630 МГц и 5,4 ГГц. Коэффициенты отражения измерялись под углом 35° импульсным методом в ходе естественных циклов испарения и увлажнения пахотного слоя почвы на участке сельскохозяйственного поля, находящегося под паром в районе пос. Минино, Красноярский край. Профили влажности почвы восстанавливались в ходе решения обратной задачи, информативным признаком в которой выступало отношение коэффициентов обратного радарного рассеяния на согласованных линейных поляризациях. Отношение коэффициентов обратного радарного рассеяния было оценено в скалярном приближении метода Кирхгофа в виде отношения коэффициентов отражения по мощности, измеренных на горизонтальной и вертикальной поляризациях. Среднеквадратическое отклонение и коэффициент детерминации между восстановленными и измеренными значениями объёмной влажности в поверхностном слое почвы толщиной 10 см оказались равны 2,2 % и 0,91 соответственно. Исследование показывает перспективность разработки поляриметрических многочастотных радиолокационных систем комбинированного сверхвысокочастотного и дециметрового диапазонов для дистанционного зондирования профилей влажности пахотного слоя почв.This report experimentally confirmed the fundamental possibility of remote sensing of moisture profiles in the arable soil layer with practical acceptable accuracy based on polarimetric measurements of the reflection coefficient at two frequencies of 630 MHz and 5.4 GHz. Reflection coefficients were measured at an angle of 35° by the impulse method, during natural cycles of the evaporation and moistening of soil arable layer in a plot of an agricultural field under steam in the area of Minino village, Krasnoyarsk region. Soil moisture profiles were retrieved in the course of solving the inverse problem, in which cost function was the ratio of the backscattering coefficients taken on coincident linear polarizations. The ratio of the backscattering coefficients was estimated by the scalar Kirchhoff approximation in the form of a ratio of power reflection coefficients, which were measured on horizontal and vertical polarizations. The standard deviation and the determination coefficient between the retrieved and measured soil moisture in the 10 cm topsoil were 2.2 % and 0.91, respectively. The study shows the prospects of developing polarimetric multi-frequency radar systems of combined UHF and SHF bands for remote sensing of moisture profiles in the arable layer of soils.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Bataleva Y. V., Palyanov Y. N., Borzdov Y. M., Novoselov I. D., Bayukov O. A.
Заглавие : An effect of reduced S-rich fluids on diamond formation under mantle-slab interaction
Место публикации : Lithos. - 2019. - Vol. 336-337. - P.27-39. - ISSN 00244937 (ISSN), DOI 10.1016/j.lithos.2019.03.027
Примечания : Cited References: 73. - This work was supported by the Russian Science Foundation under Grant No. 14-27-00054 and a state assignment of IGM SB RAS. The authors thank S. Ovchinnikov for his assistance in implementation of the Mossbauer spectroscopy measurements.
Аннотация: Experimental study, dedicated to understanding the effect of S-rich reduced fluids on the diamond-forming processes under subduction settings, was performed using a multi-anvil high-pressure split-sphere apparatus in Fe3C-(Mg,Ca)CO3-S and Fe0-(Mg,Ca)CO3-S systems at the pressure of 6.3 GPa, temperatures in the range of 900–1600 °C and run time of 18–60 h. At the temperatures of 900 and 1000 °C in the carbide-carbonate-sulfur system, extraction of carbon from cohenite through the interaction with S-rich reduced fluid, as well as C0-producing redox reactions of carbonate with carbide were realized. As a result, graphite formation in assemblage with magnesiowüstite, cohenite and pyrrhotite (±aragonite) was established. At higher temperatures (≥1100 °C) formation of assemblage of Fe3+-magnesiowüstite and graphite was accompanied by generation of fO2-contrasting melts - metal-sulfide with dissolved carbon (Fe-S-C) and sulfide-oxide (Fe-S-O). In the temperature range of 1400–1600 °C spontaneous diamond nucleation was found to occur via redox interactions of carbide or iron with carbonate. It was established, that interactions of Fe-S-C and Fe-S-O melts as well as of Fe-S-C melt and magnesiowüstite, were С0-forming processes, accompanied by disproportionation of Fe. These resulted in the crystallization of Fe3+-magnesiowüstite+graphite assemblage and growth of diamond. We show that a participation of sulfur in subduction-related elemental carbon-forming processes results in sharp decrease of partial melting temperatures (~300 °C), reducting the reactivity of the Fe-S-C melt relatively to FeC melt with respect to graphite and diamond crystallization and decrease of diamond growth rate.
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Вид документа : Статья из журнала
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Автор(ы) : Bataleva Y., Palyanov Y., Borzdov Y., Bayukov O. A.
Заглавие : Processes and conditions of the origin for Fe3+-bearing magnesiowustite under lithospheric mantle pressures and temperatures
Место публикации : Minerals. - 2019. - Vol. 9, Is. 8. - Ст.474. - ISSN 2075163X (ISSN), DOI 10.3390/min9080474
Примечания : Cited References: 82. - This research was performed by state assignment of IGM SB RAS (project No. 0330-2016-0007).
Предметные рубрики: Mineral Geochemistry and Geochronology
Аннотация: An experimental study, implicated in the revealing of the conditions for the origin for Fe3+-bearing magnesiowüstite in the lithospheric mantle, was performed using Mössbauer spectroscopy of pre-synthesized samples. Experiments were carried out using a multi-anvil high-pressure split-sphere apparatus at 6.3–7.5 GPa, in the range of 1100–1650 °C in carbonate-metal, carbonate–oxide-metal, carbonate-oxide, carbide-oxide and carbonate–metal-sulphur systems. In three experimental series, oxygen fugacity gradient in the samples was created, which enabled the study of the processes of magnesiowüstite formation under oxidizing and reducing conditions (ΔlogfO2 (FMQ) values from −1 to −5). It was established that Fe3+-bearing magnesiowüstite can form both in assemblage with oxidized phases, such as carbonate or with reduced ones—metal, carbides, sulphides, graphite and diamond. According to the Mössbauer spectroscopy, the composition of synthesized magnesiowüstite varied within a range of Fe3+/ΣFe values from 0 to 0.3, with IV and VI coordination of Fe3+ depending on P, T, fO2, x-parameters. It was established that Fe3+-bearing magnesiowüstite formation processes under upper mantle P,T-conditions include redox reactions, with magnesiowüstite being (1) reductant or (2) product of interaction, (3) crystallization processes of magnesiowüstite from an oxidized melt, where magnesiowüstite acts as a sink for ferric iron and (4) iron disproportionation.
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10.

Вид документа : Статья из сборника (выпуск продолж. издания)
Шифр издания :
Автор(ы) : Balyzin M., Sadrieva Z., Belyakov M. A., Kapitanova P., Sadreev A. F., Bogdanov A.
Заглавие : Bound state in the continuum in 1D chain of dielectric disks: Theory and experiment
Коллективы : International Conference on Metamaterials and Nanophotonics
Место публикации : J. Phys. Conf. Ser. - 2018. - Vol. 1092: 3rd International Conference on Metamaterials and Nanophotonics, METANANO 2018 (17 - 21 September 2018). - Ст.012012. - , DOI 10.1088/1742-6596/1092/1/012012
Примечания : Cited References: 11. - This work is supported by RSF (17-12-01581)
Ключевые слова (''Своб.индексиров.''): 1-d chains--bound state--ceramic disks--dielectric disks--ghz frequencies--material loss--quadratic growth--zero angular momentum
Аннотация: In this work we experimentally observe a symmetry protected optical bound state in the continuum (BIC) with zero angular momentum in 1D array of ceramic disks at GHz frequencies. We analyze the dependence of Q factor of BIC on the number of the disks and the level of the material losses. We confirmed theoretical prediction about quadratic growth of the Q factor with the number of the disks and its following saturation due to material losses.
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