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Dimethylsulfoxide as a media for one-stage synthesis of the Fe3O4-based ferrofluids with a controllable size distribution / V. L. Kirillov [et al.]> // Mater. Chem. Phys. - 2019. - Vol. 225. - P. 292-297, DOI 10.1016/j.matchemphys.2019.01.003. - Cited References: 36. - This work was supported by the Russian Science Foundation , project no. 17-12-01111.
. - ISSN 0254-0584 Кл.слова (ненормированные): Ferrofluid -- Magnetite nanoparticles -- One-step synthesis -- Superparamagnetic nanoparticles -- Ferromagnetic resonance Аннотация: The ultrafine (d = 4 nm) magnetite ferrofluid with a narrow nanoparticle size distribution has been synthesized in one stage at room temperature from a solution of iron(II) and (III) chlorides in dimethylsulfoxide (DMSO) with the propylene epoxide admixture. This is the first example of obtaining a stable concentrated ultrafine magnetite/DMSO ferrofluid at room temperature. X-ray diffraction, transmission electron microscopy, ferromagnetic resonance, Mossbauer spectroscopy, and magnetostatic study have been used to elucidate the role of DMSO and the H2O/DMSO ratio in the formation of a stable colloid with a desired nanoparticle size. The initial stages of the magnetite nanoparticles formation have been investigated by the ferromagnetic resonance technique.
Смотреть статью, Scopus, WOS, Читать в сети ИФ Держатели документа: Boreskov Institute of Catalysis, Russian Academy of Sciences, Siberian Branch, Novosibirsk, 630090, Russian Federation Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation Доп.точки доступа: Kirillov, V. L.; Yakushkin, S. S.; Balaev, D. A.; Балаев, Дмитрий Александрович; Dubrovskiy, A. A.; Дубровский, Андрей Александрович; Semenov, S. V.; Семёнов, Сергей Васильевич; Knyazev, Yu. V.; Князев, Юрий Владимирович; Bayukov, O. A.; Баюков, Олег Артемьевич; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Yatsenko, D. A.; Martyanov, O. N. } Найти похожие
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