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    A comparative study of γ-Fe2O3 and ε-Fe2O3 nanoparticles arising in borate glasses doped with Fe and Gd / O. S. Ivanova [et al.] // J. Sib. Fed. Univ. Math. Phys. - 2016. - Vol. 9, Is. 4. - P. 459–462 ; Журн. СФУ. Сер. "Математика и физика", DOI 10.17516/1997-1397-2016-9-4-459-462. - Cited References: 6. - The work was supported partly by the RFBR, 14-02-01211-a, and by the President of Russia Grant NSh-7559.2016.2. . - ISSN 1997-1397
   Перевод заглавия: Сравнительное изучение γ-Fe2O3 и ϵ-Fe2O3 наночастиц, формирующихся в стекле, допированном железом и гадолинием
Кл.слова (ненормированные):
magnetic nanoparticles -- magnetic circular dichroism -- magnetic measurements -- магнитные наночастицы -- магнитный круговой дихроизм -- магнитные измерения
Аннотация: Formation and properties of the iron oxides γ -Fe2O3 and ϵ-Fe2O3 nanoparticles arising in glasses of basic compositions Ge2O-K2O-Al2O3-B2O3 and K2O-Al2O3-B2O3 doped with different concentrations of Fe2O3 and Gd2O3 and subjected to the additional thermal treatment are studied. The X-ray diffraction, TEM microscopy, magnetooptical effects, and electron spin resonance study allow elucidating the matrix and Gd role in determining the nanoparticle properties.
Изучены свойства наночастиц γ-Fe2O3 и ϵ-Fe2O3, формирующихся в стеклах основного состава Ge2O-K2O-Al2O3-B2O3 и K2O-Al2O3-B2O3, допированных Fe2O3 и Gd2O3 и подвергнутых дополни- тельной термической обработке. Результаты исследования рентгеновской дифракции, электрон- ной микроскопии, магнитооптических эффектов и электронного спинового резонанса позволили объяснить роль матрицы и гадолиния в определении свойств наночастиц.

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Доп.точки доступа:
Ivanova, O. S.; Иванова, Оксана Станиславовна; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Edelman, I. S.; Эдельман, Ирина Самсоновна; Petrakovskaja, E. A.; Петраковская, Элеонора Анатольевна

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A comparative study of γ-Fe2O3 and ε-Fe2O3 nanoparticles arising in borate glasses doped with Fe and Gd / O. S. Ivanova [et al.] // VI Euro-Asian Symposium "Trends in MAGnetism" (EASTMAG-2016) : abstracts / ed.: O. A. Maksimova, R. D. Ivantsov. - Krasnoyarsk : KIP RAS SB, 2016. - Ст. P9.11. - P. 397. - References: 1. - The work was supported partly by the RFBR grant No. 14-02-01211 . - ISBN 978-5-904603-06-9
Кл.слова (ненормированные):
magnetic nanoparticles -- magnetic circular dichroism -- magnetic measurements

Доп.точки доступа:
Ivanova, O. S.; Иванова, Оксана Станиславовна; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Edelman, I. S.; Эдельман, Ирина Самсоновна; Petrakovskaja, E. A.; Петраковская, Элеонора Анатольевна; Euro-Asian Symposium "Trends in MAGnetism"(6 ; 2016 ; Aug. ; 15-19 ; Krasnoyarsk); "Trends in MAGnetism", Euro-Asian Symposium(6 ; 2016 ; Aug. ; 15-19 ; Krasnoyarsk); Институт физики им. Л.В. Киренского Сибирского отделения РАН

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Deich, L. I.
Absorption of light by glasses in the far infrared / L. I. Deich // Jetp Lett. - 1992. - Vol. 56, Is. 10. - P. 492-495. - Cited References: 9 . - ISSN 0021-3640

РУБ Physics, Multidisciplinary
Рубрики:
STATES
Аннотация: An explanation is proposed for the deviation from the Debye shape of the absorption curve of glasses in the far infrared.

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Доп.точки доступа:
Дейч, Лев Исаакович
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Effect of gadolinium on magnetic circular dichroism and electron magnetic resonance of ε-Fe2O3 nanoparticles formed in borate glasses / I. Edelman [et al.] // J. Non-Cryst. Solids. - 2019. - Vol. 506. - P. 68-79, DOI 10.1016/j.jnoncrysol.2018.12.006. - Cited References: 81. - The work is supported by Russian Academy of Sciences in the frame of the Project № 0356-2017-0030. . - ISSN 0022-3093
Кл.слова (ненормированные):
Iron oxides -- ε-Fe2O3 -- Borate glasses -- Nanoparticles -- Magnetic circular dichroism -- Electron magnetic resonance
Аннотация: A remarkable characteristic of borate glasses is the ability of forming magnetic nanoparticles at low doping with transition element oxides. We have studied structure and magnetic properties of iron oxide nanoparticles formed in borate glasses, in particular, concentration and temperature dependences of magnetic circular dichroism (MCD) and electron magnetic resonance (EMR) spectra. A series of glasses of molar composition 22.5K2O-22.5Al2O3–55B2O3 doped with 1.5 mass % of Fe2O3 and different contents of Gd2O3 from 0.1 to 1.0 mass % was prepared using a conventional melt quenching technique and subjected to an additional thermal treatment. The whole set of results allows to identify the predominant magnetic phase in these glasses as ε-Fe2O3 nanoparticles, with a considerable part of iron ions substituted by gadolinium. Analysis and computer simulations of the EMR spectra allow separating the contribution of electron paramagnetic resonance of diluted iron ions and together with the temperature dependences of magnetization demonstrate a superparamagnetic character of the nanoparticle magnetism.

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Держатели документа:
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
LOMA, UMR 5798 Universite de Bordeaux-CNRS, Talence cedex, 33405, France
Siberian Federal University, Krasnoyarsk, 660041, Russian Federation
Boreskov Institute of Catalysis, Siberian Branch of RAS, Novosibirsk, 630090, Russian Federation
NRC “Kurchatov Institute”, Moscow, 123182, Russian Federation
Vavilov State Optical Institute, St.-Petersburg, 199053, Russian Federation

Доп.точки доступа:
Edelman, I. S.; Эдельман, Ирина Самсоновна; Kliava, J.; Ivanova, O. S.; Иванова, Оксана Станиславовна; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Zaikovskii, V.; Petrakovskaja, E. A.; Петраковская, Элеонора Анатольевна; Zubavichus, Y.; Stepanov, S.
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Effect of interaction of components on thermal properties of ferroelectric nanocomposites / E. A. Mikhaleva [et al.] // Eleventh Seminar Porous Glasses-Special Glasses (PGL'2018) : Abstracts and program. - 2018. - Ст. 18. - P. 23. - Библиогр.: 2

,
Материалы конференции

Доп.точки доступа:
Mikhaleva, E. A.; Михалева, Екатерина Андреевна; Flerov, I. N.; Флёров, Игорь Николаевич; Kartashev, A. V.; Карташев, Андрей Васильевич; Gorev, M. V.; Горев, Михаил Васильевич; Bogdanov, E. V.; Богданов, Евгений Витальевич; Bondarev, V. S.; Бондарев, Виталий Сергеевич; Kogotkov, L. N.; Rysiakiewicz-Pasek, E.; "Porous Glasses-Special Glasses", Seminar(11 ; 2018 ; Sept. ; 12-16 ; Szklarska Poręba, Poland); Wroclaw University of Science and Technology
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Effect of strontium and barium doping on the magnetic state and electrical conductivity of GdCoO3 / N. B. Ivanova [et al.] // Phys. Solid State. - 2007. - Vol. 49, Is. 8. - P. 1498-1506, DOI 10.1134/S1063783407080161. - Cited References: 36 . - ISSN 1063-7834

РУБ Physics, Condensed Matter
Рубрики:
PEROVSKITE
   ORDER
   OXIDE
   BEHAVIOR
   GLASSES
   LACOO3
   PR
   GD
   SM
   ND
Аннотация: A coordinated investigation of the magnetic and electrical properties of polycrystalline cobalt oxide compounds CdCoO3, Gd0.9Ba0.1CoO3, and Gd0.9Sr0.1CoO3 is carried out. Undoped GdCoO3 reveals a low conductivity; a magnetic moment of 7.4 mu(B) per molecule, which is less than the theoretical value for the Gd3+ ion; and an asymptotic Curie temperature of -6 K. Doping GdCoO3 with barium and strontium to substitution of 10 at. % Gd brings about an increase in the conductivity and magnetic transitions at T = 300 K for Gd0.9Ba0.1CoO3 and T = 170 K for Gd0.9Sr0.1CoO3. The magnetization anomalies imply the formation of magnetic clusters. The behavior of the electrical conductivity at high temperatures suggests a variable activation energy. At low temperatures, Mott hopping conduction sets in.

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Публикация на русском языке Влияние допирования стронцием и барием на магнитное состояние и электропроводность GdCoO[3] [Текст] / Н. Б. Иванова [и др.] // Физ. тверд. тела. - 2007. - Т. 49 Вып. 8. - С. 1427-1435

Держатели документа:
Russian Acad Sci, Siberian Div, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
Univ Guadalajara, CUCEI, Dept Fis, Guadalajara 44430, Jalisco, Mexico
ИФ СО РАН
Kirensky Institute of Physics, Siberian Division, Russian Academy of Sciences, Krasnoyarsk 660036, Russian Federation
Departmento de Fisica, C.U.C.E.I., Universidade de Guadalajara, Guadalajara, Jalisco 44430, Mexico

Доп.точки доступа:
Ivanova, N. B.; Иванова, Наталья Борисовна; Kazak, N. V.; Казак, Наталья Валерьевна; Michel, C. R.; Balaev, A. D.; Балаев, Александр Дмитриевич; Ovchinnikov, S. G.; Овчинников, Сергей Геннадьевич; Vasil'ev, A. D.; Васильев, Александр Дмитриевич; Bulina, N. V.; Булина, Наталья Васильевна; Panchenko, E. B.
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Electron magnetic resonance and magnetooptical studies of nanoparticle-containing borate glasses / J. Kliava [et al.] // Journal of Magnetism and Magnetic Materials. - 2011. - Vol. 323, Is. 5. - P. 451-460, DOI 10.1016/j.jmmm.2010.09.045. - Cited Reference Count: 40. - RFBRRussian Foundation for Basic Research (RFBR) [07-02-92174]; CNRSCentre National de la Recherche Scientifique (CNRS)European Commission [07-02-92174]; Russian Federal Program [FCP NK-209P/GK P1227], This work was supported in part by RFBR-CNRS joint project, Grant no. 07-02-92174 and by the Russian Federal Program, project FCP NK-209P/GK P1227. It is a pleasure to thank I. Bruckental and Y. Yeshurun for the magnetization measurements. . - ISSN 0304-8853

ГРНТИ

29.19

Кл.слова (ненормированные):
borate glasses -- Electron magnetic resonance -- magnetic nanoparticles -- magnetooptics
Аннотация: We report electron magnetic resonance (EMR) and magnetooptical studies of borate glasses of molar composition 22.5K2O22.5Al2O 355B2O3 co-doped with low concentrations of Fe2O3

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Держатели документа:
CEMHTI,UPR3079 CNRS et Universit d'Orlans
CPMOH,UMR 5798,Universit Bordeaux 1-CNRS
CRMD,UMR 6619,Universit d'Orlans-CNRS
L.V. Kirensky Institute of Physics,Siberian Branch of the RAS
Synchrotron SOLEIL,L'Orme des Merisiers

Доп.точки доступа:
Kliava, J.; Edelman, I.; Ivanova, O.; Ivantsov, R.; Petrakovskaja, E. A.; Hennet, L.; Thiaudire, D.; Saboungi, M. L.
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Electron Paramagnetic Resonance and Gd3+ Clustering in the{xGd203-(1-x)(La203-Al203-B203-SiO2-GeO2)} Glasses [Text] / J. Kliava, R. Berger, A. A. Potseluyko [et al.] // The Physics of Metals and Metallography. - 2006. - Vol. 102, Suppl. 1. - P. S39-S41DOI 10.1134/S0031918X06140092. - Библиогр.: 6. - Krasnoyarsk Regional Science Foundation (grant no. 12F0045C).
Аннотация: A multicomponent glass system 20La2O3–22Al2O3–23B23–35(SiO2+ GeO2) in which part of La2O3is substituted by Gd2O3 in different concentrations has been studied by EPR. The EPR spectra show the presence of clustering at higher Gd contents. At low temperatures, the cluster-related resonance signal is altered in shape, indicating the appearance of a magnetic anisotropy field.

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Держатели документа:
CPMOH, Üniversite Bordeaux–I, 33405 Talence Cedex, France
Kirensky Institute of Physics, Siberian Division, Russian Academy of Sciences, Krasnoyarsk 660036, Russia
Vavilov State Optical Institute, St. Petersburg, 199034 Russia

Доп.точки доступа:
Kliava, J.; Berger, R.; Potseluyko, A. A.; Поцелуйко, Анатолий Артёмович; Edelman, I. S.; Petrakovskaya, E. A.; Петраковская, Элеонора Анатольевна; Zarubina, T.
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EMR spectra of borat glasses containing two types of transition ion simultaneously [Text] / Kliava J., Marbeuf A., Edelman I., Ivanova O., Petrakovskaja E., Ivantsov R. // EUROMAR 2008 Conference : St.Peterbsburg, 2008, [6-11 July]. - 2008. - p. 221

Доп.точки доступа:
Kliava, J.; Marbeuf, A.; Edelman, I. S.; Эдельман, Ирина Самсоновна; Ivanova, O. S.; Иванова, Оксана Станиславовна; Petrakovskaja, E. A.; Петраковская, Элеонора Анатольевна; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; "Магнитный резонанс для будущего", Международный конгресс(2008 ; июль ; Санкт-Петербург); "Euromar", International Conference(2008 ; Jul. ; St.-Peterburg)
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10.

Ensembles of γ-Fe2O3 nanoparticles formed during devitrification of borate glasses / O. S. Ivanova [et al.] // Solid State Phenom. : Selected, peer reviewed papers. - 2014. - Vol. 215: Trends in Magnetism: Nanomagnetism (EASTMAG-2013). - P. 173-178, DOI 10.4028/www.scientific.net/SSP.215.173. - Cited References: 16 . - ISSN 978-30383. - ISSN 1662-9779
Кл.слова (ненормированные):
Magnetic nanoparticles -- Magneto-optical properties
Аннотация: Structural, magnetic and magneto-optical properties of borate glasses co-doped with Fe and the lager radius ions are presented. Maghemite, ?-Fe2O3, nanoparticles arise in the glasses as a result of their thermal treatment in different regimes. Magnetization FC and ZFC temperature dependences demonstrate the superparamagnetic behavior of the particles with the blocking temperature below the room temperature. The EMR spectra measurements revealed a significant anisotropy with a large contribution of the nanoparticles' surface anisotropy. The FR maximum centered near 700 nm is a characteristic feature of the investigated glasses. © (2014) Trans Tech Publications, Switzerland.

Доп.точки доступа:
Ovchinnikov, S. G. \ed.\; Овчинников, Сергей Геннадьевич; Samardak, A. \ed.\; Ivanova, O. S.; Иванова, Оксана Станиславовна; Edelman, I. S.; Эдельман, Ирина Самсоновна; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Petrakovskaja, E. A.; Петраковская, Элеонора Анатольевна; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Trofimova, N. N.; Zubavichus, Y. V.; Euro-Asian Symposium "Trends in MAGnetism": Nanomagnetism(5 ; 2013 ; sept. ; 15-21 ; Vladivostok)
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11.

Ensembles OF[[d]]γ[[/d]]-Fe[[d]]2[[/d]]O[[d]]3[[/d]] nanoparticles formed during devitrification of borate glasses [Текст] / O. S. Ivanova [и др.] // V Euro-Asian simposium "Trend in MAGnetism": Nanomagnetism : abstracts. - Vladivostok : FEFU, 2013. - P138 . - ISBN 978-5-7444-3124-2

Доп.точки доступа:
Ivanova, O. S.; Иванова, Оксана Станиславовна; Edelman, I. S.; Эдельман, Ирина Самсоновна; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Petrakovskaya, E. A.; Петраковская, Элеонора Анатольевна; Великанов, Дмитрий Анатольевич; Velikanov, D. A.; Trofimova, N. N.; Трофимова, Н. Н.; Zubavichus, Y. V.; Зубавичус, Я. В.; Euro-Asian Symposium "Trends in MAGnetism": Nanomagnetism(5 ; 2013 ; Sept. ; 15-21 ; Vladivostok)
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12.

    Euro-asian symposium "Trends in magnetism" (EASTMAG-2004) : Abstract book / Рос. акад. наук, Сиб. отд-ние, Ин-т физики им. Л.В. Киренского, Краснояр. гос. ун-т, Краснояр. гос. технич. ун-т, Урал. отд-ние , Ин-т физики металлов. Euro-asian symp. "Trends in magnetism" ; предс. орг. комит. К. С. Александров ; зам. предс. С. Г. Овчинников ; чл. орг. комит. В. А. Игнатченко [и др.]. - Krasnoyarsk : [б. и.], 2004. - 418 с. - Bibliogr. at the end of the articles - Auth. ind. - 350 экз. - Б. ц.
Перевод заглавия: Евро-азиатский симпозиум "Прогресс в магнетизме"
Приложение:
Program of Euro-asian symposium "Trends in magnetism" (EASTMAG-2004). - Krasnoyarsk : Kirensky Instit. Phys. SB RAS, 2004. - 83
    Содержание:
Fundamental magnetic properties
Transport phenomena and spin electronics
Magnetism and strongly correleted electron systems
Spin glasses, disordered magnetic systems
Dynamics of spin systems and magnetic resonances
Magnetooptics and X-ray magnetooptics
Magnetic mechanism of the superconductivity
Domain structure and magnetization processes
Thin magnetic films and multilayers
Magnetic particles and nanocrystalline materials
Molecular magnetism
Magnetic storage/memory and applications
   Перевод заглавия: Евро-азиатский симпозиум "Прогресс в магнетизме"

Держатели документа:
Институт физики им. Л.В. Киренского СО РАН

Доп.точки доступа:
Александров, Кирилл Сергеевич \предс. орг. ком.\; Aleksandrov, K. S.; Овчинников, Сергей Геннадьевич \зам. предс.\; Ovchinnikov, S. G.; Игнатченко, Вальтер Алексеевич \чл. орг. ком.\; Ignatchenko, V. A.; Сапожников, В. \чл. орг. ком.\; Патрин, Геннадий Семёнович \чл. орг. ком.\; Patrin, G. S.; Вальков, Валерий Владимирович \чл. орг. ком.\; Val'kov, V. V.; Волков, Никита Валентинович \чл. орг. ком.\; Volkov, N. V.; Казак, Наталья Валерьевна \чл. орг. ком.\; Kazak, N. V.; Российская академия наук; Сибирское отделение РАН; Институт физики им. Л.В. Киренского Сибирского отделения РАН; Красноярский государственный университет; Красноярский государственный технический университет; Институт физики металлов Уральского отделения РАН; Научный совет по физике конденсированных сред РАН; Научный совет РАН по физике низких температур; Красноярский научный центр Сибирского отделения РАН; Euro-asian symposium "Trends in magnetism" (2 ; 2004 ; Aug. 24-27 ; Krasnoyarsk); "Trends in magnetism", Euro-Asian Symposium (2 ; 2004 ; Aug. 24-27 ; Krasnoyarsk)
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13.

Deich, L. I.
Far-infrared attenuation in glasses / L. I. Deich // Phys. Rev. B. - 1994. - Vol. 49, Is. 1. - P. 109-113, DOI 10.1103/PhysRevB.49.109. - Cited References: 29 . - ISSN 0163-1829

РУБ Physics, Condensed Matter
Рубрики:
VITREOUS SILICA
   TEMPERATURE
   MODEL
   LOCALIZATION
   ABSORPTION
   SOLIDS
   STATES
Аннотация: The influence of quasilocal vibrations on the far-infrared spectra of glasses is investigated under the supposition that the quasilocal vibrations are directly inactive in the attenuation. It is shown that taking into account phonon-quasilocal-vibration coupling and both medium- and short-range structure of the inhomogeneities of a photon-phonon coupling parameter can give rise to an attenuation curve similar to one observed for a-SiO2 and related materials.

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Держатели документа:
L. V. Kirensky Institute of Physics, Krasnoyarsk, 660036, Russian Federation

Доп.точки доступа:
Дейч, Лев Исаакович
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14.

Formation and evolution of magnetic nanoparticles in borate glass simultaneously doped with Fe and Mn oxides / J. . Kliava [et al.] // J. Appl. Phys. - 2008. - Vol. 104, Is. 10. - Ст. 103917, DOI 10.1063/1.3021289. - Cited References: 37. - A financial support from the Russian Foundation for Basic Research (RFBR)-CNRS (Grant No. 07-02-92174) is highly appreciated. R. Ivantsov is grateful to the Russian Science Support Foundation. Y. Yeshurun acknowledges the support of the Israel Scienc Foundation (ISF). . - ISSN 0021-8979

РУБ Physics, Applied
Рубрики:
COBALT FERRITE PARTICLES
   SUPERPARAMAGNETIC RESONANCE
   GAMMA-FE2O3 NANOPARTICLES
   MATRIX
   SIZE
   SYSTEMS
Кл.слова (ненормированные):
aluminium compounds -- borate glasses -- coercive force -- Faraday effect -- heat treatment -- iron compounds -- magnetic hysteresis -- magnetic particles -- magnetic susceptibility -- manganese compounds -- Mossbauer effect -- nanoparticles -- paramagnetic materials -- potassium compounds -- remanence -- superparamagnetism -- transmission electron microscopy -- X-ray chemical analysis -- Atomic spectroscopy -- Auger electron spectroscopy -- Crystal structure -- Electric relays -- Electronic medical equipment -- Ferrite -- Ferrites -- Glass -- Heat treatment -- Hysteresis -- Hysteresis loops -- Magnetic properties -- Magnetic resonance measurement -- Magnetic susceptibility -- Magnetism -- Manganese -- Manganese compounds -- Molybdenum -- Nanoparticles -- Optical properties -- Ozone water treatment -- Polydispersity -- Superparamagnetism -- Borate glasses -- Concentration ratios -- Electron magnetic resonances -- Emr spectrums -- Experimental techniques -- Faraday rotations -- Glass compositions -- Glass matrixes -- Glass preparations -- Magnetic measurements -- Magnetic nano particles -- Magnetic orders -- Magnetically ordered systems -- Magneto-optical properties -- Manganese ferrites -- Mean diameters -- Mn oxides -- Phase states -- Polydisperse nanoparticles -- Remnant magnetizations -- Ssbauer spectroscopies -- Superparamagnetic -- Superparamagnetic states -- Thermal treatments -- Variable temperatures -- Magnetic materials
Аннотация: Evolution of the phase state of paramagnetic additions at various stages of synthesis and subsequent thermal treatment of glasses of the system Al(2)O(3)-K(2)O-B(2)O(3) simultaneously doped with Fe(2)O(3) and MnO is studied by means of a combination of experimental techniques: Faraday rotation (FR), electron magnetic resonance (EMR), transmission electron microscopy (TEM), Mossbauer spectroscopy, and magnetic measurements. Both FR and EMR show that magnetically ordered clusters occur already at the first stage of the glass preparation. In particular, for the ratio of the Fe and Mn oxides in the charge close to 3:2, fine magnetic nanoparticles are formed with characteristics similar to those of manganese ferrite. By computer simulating the EMR spectra at variable temperatures, a superparamagnetic nature of these nanoparticles is confirmed and their mean diameter is estimated as approximately 3.2 nm. In the thermally treated glasses larger magnetic nanoparticles are formed, giving rise to FR spectra, characteristic of magnetically ordered systems, and the EMR spectra different from those in as-prepared glasses but also showing superparamagnetic narrowing. The Mossbauer spectroscopy corroborates the manganese ferrite structure of the nanoparticles and indicates their coexistence in the ferrimagnetic and superparamagnetic states. The TEM shows the presence of polydisperse nanoparticles on the background of the glass matrix, and electron diffraction of a selected region containing larger particles indicates a crystal structure close to that of MnFe(2)O(4). Energy-dispersive atomic x-ray spectra confirm that the major part of Fe and Mn introduced to the glass composition is gathered in the particles, with the concentration ratio close to 2:1, characteristic of bulk MnFe(2)O(4). Magnetic hysteresis loops of samples subjected to an additional thermal treatment demonstrate a strong increase in the coercive force, remnant magnetization, and high-field magnetic susceptibility with temperature decrease. The consistent results obtained using various techniques demonstrate that the formation of nanoparticles with characteristics close to those of MnFe(2)O(4) confers to these glasses magnetic and magneto-optical properties typical of substances possessing magnetic order.

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Держатели документа:
[Kliava, J.] Univ Bordeaux 1, CNRS, UMR 5798, CPMOH, F-33405 Talence, France
[Edelman, I.
Ivanova, O.
Ivantsov, R.
Bayukov, O.
Petrakovskaja, E.
Stepanov, S.] RAS, Siberian Branch, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
[Zaikovskiy, V.] RAS, Siberian Branch, Boreskov Inst Catalysis, Novosibirsk 630090, Russia
[Bruckental, I.
Yeshurun, Y.] Bar Ilan Univ, Dept Phys, IL-52900 Ramat Gan, Israel
[Stepanov, S.] SI Vavilov State Opt Inst, St Petersburg 199034, Russia
ИФ СО РАН
CPMOH, Universit? Bordeaux, 1-CNRS UMR 5798, 33405 Talence Cedex, France
Kirensky Institute of Physics, Siberian Branch of RAS, 660036 Krasnoyarsk, Russian Federation
Boreskov Institute of Catalysis, Siberian Branch, RAS, 630090 Novosibirsk, Russian Federation
Department of Physics, Bar-Ilan University, Ramat-Gan 52900, Israel
S. I. Vavilov State Optical Institute, St. Petersburg 199034, Russian Federation

Доп.точки доступа:
Kliava, J.; Edelman, I. S.; Эдельман, Ирина Самсоновна; Ivanova, O. S.; Иванова, Оксана Станиславовна; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Bayukov, O. A.; Баюков, Олег Артемьевич; Petrakovskaja, E. A.; Петраковская, Элеонора Анатольевна; Zaikovskiy, V.; Bruckental, I.; Yeshurun, Y.; Stepanov, S.
}
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15.

Formation, characterization and magnetic properties of maghemite γ-Fe2O3 nanoparticles in borate glasses / I. S. Edelman [et al.] // J. Alloys Compd. - 2015. - Vol. 624. - P. 60-67, DOI 10.1016/j.jallcom.2014.11.059. - Cited References: 25. - This work was supported partly by the Russian Foundation for Basic Research - Russia, Grant No. 14-02-01211-a and by the President of Russia Grant No. NSh-2886.2014.2. This work was performed using the equipment of Unique Scientific Facility "Kurchatov Synchrotron Radiation Source'' supported by the Russian Ministry of Science and Education (project code RFMEFI61914X0002). . - ISSN 0925-8388

РУБ Chemistry, Physical + Materials Science, Multidisciplinary + Metallurgy & Metallurgical Engineering
Рубрики:
SUPERPARAMAGNETIC RESONANCE
   HYSTERESIS LOOPS
   EXCHANGE BIAS
   IONS
   MATRIX
Кл.слова (ненормированные):
Nanostructures -- Crystal structure and symmetry -- Magnetic measurements
Аннотация: A new type of nanocomposite materials based on maghemite, γ-Fe2O3, nanoparticles dispersed in borate glasses co-doped with low contents of iron together with the larger radius element combinations: Y and Bi, or Sm and Pb, or Y and Pb is studied. Nanoparticles arise as a result of heat treatment of the glasses which gives them properties characteristic of magnetically ordered substances. Transmission electron microscopy and XRD show that only one magnetic phase, namely γ-Fe2O3 nanoparticles, occurs in glasses subjected to the thermal treatment at 540 °C during 24 h independently on the doping element nature. At the same time doping element and their concentrations ratio in every combination affect the particles average size and glass magnetic properties, such as magnetization temperature dependences, Faraday rotation value and electron magnetic resonance spectrum characteristics.

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Держатели документа:
RAS, Siberian Branch, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
Siberian Fed Univ, Krasnoyarsk 660036, Russia
NRC Kurchatov Inst, Moscow 123182, Russia
RAS, Siberian Branch, Boreskov Inst Catalysis, Novosibirsk 630090, Russia
Novosibirsk State Univ, Novosibirsk 630090, Russia

Доп.точки доступа:
Edelman, I. S.; Эдельман, Ирина Самсоновна; Ivanova, O. S.; Иванова, Оксана Станиславовна; Petrakovskaja, E. A.; Петраковская, Элеонора Анатольевна; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Tarasov, I. A.; Тарасов, Иван Анатольевич; Zubavichus, Y. V.; Trofimova, N. N.; Zaikovskii, V. I.; Russian Foundation for Basic Research - Russia [14-02-01211-a]; President of Russia [NSh-2886.2014.2]; Russian Ministry of Science and Education [RFMEFI61914X0002]
}
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16.

Heat capacity and thermal expansion of nanosized ferroelectric (NH4)2SO4 embedded in borosilicate glasses / E. A. Mikhaleva, M. V. Gorev, V. S. Bondarev [et al.] // J. Non-Cryst. Solids. - 2022. - Vol. 597. - Ст. 121935, DOI 10.1016/j.jnoncrysol.2022.121935. - Cited References: 29. - The authors are grateful to Dr. Ewa Rysiakiewicz-Pasek (Wroclaw University of Science and Technology, Poland) for the preparation and characterization of borosilicate glasses. X-ray and dilatometric data were obtained using the equipment of Krasnoyarsk Regional Center of Research Equipment of Federal Research Center “Krasnoyarsk Science Center SB RAS” . - ISSN 0022-3093
Кл.слова (ненормированные):
Nanocomposite -- Ferroelectrics -- Phase transition -- Thermal expansion -- Entropy
Аннотация: The thermal properties of nanocomposites obtained by incorporating a ferroelectric (NH4)2SO4 (AS) into porous glasses (PG) was studied for the first time. X-ray diffraction studies showed a strong increase in the ratio of the size of nanocrystallites grown in glass matrices to pore size, dcryst/ dpore = 0.47→1.50→5.00, with a decrease in dpore = 320→46→7 nm. Calorimetric and dilatometric measurements showed a change from a first-order phase transition in AS single crystal to a second-order transformation in AS nanocrystallites. A restricted geometry also led to a significant decrease in the anomalous entropy in AS+PG samples compared to AS (J/mol∙K): 17.7 (AS)→12.4 (AS+PG320)→10.4 (AS+PG46)→8.1 (AS+PG7). A discussion of the nontrivial behavior of the phase transition temperature in embedded AS was carried out using the degree of PG filling, the ratio dcryst/dpore, texture, and the volumetric and linear baric coefficients for the bulk AS.

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Держатели документа:
Federal Research Center KSC SB RAS, Kirensky Institute of Physics, Krasnoyarsk, 660036, Russian Federation
Siberian Federal University, Krasnoyarsk, 660074, Russian Federation
Federal Research Center "Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of Sciences, Krasnoyarsk, 660036, Russian Federation
Ioffe Physico-Technical Institute, RAS, St.-Petersburg, 194021, Russian Federation

Доп.точки доступа:
Mikhaleva, E. A.; Михалева, Екатерина Андреевна; Gorev, M. V.; Горев, Михаил Васильевич; Bondarev, V. S.; Бондарев, Виталий Сергеевич; Molokeev, M. S.; Молокеев, Максим Сергеевич; Zaitsev, A. I.; Зайцев, Александр Иванович; Nemtsev, I. V.; Fokin, A. V.; Flerov, I. N.; Флёров, Игорь Николаевич
}
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17.

Heat treatment stimulation of the magnetic nanoparticles formation in borate glasses doped with transition elements / I. Edelman [et al.] // Heat Treat.: Theory, Tech. and Appl. : Chapter. - New York : Nova Science Publishers, 2011. - P. 225-239 . - ISBN 978-161728348-2
Аннотация: Evolution of the magnetic nanoparticles characteristics in glasses of the system 22.5 Al2O3 - 22.5 K2O - 55 B2O3 co-doped with Fe2O3 and MnO simultaneous is studied at different stages of the post-synthesis heat treatment with transmission electron microscopy (TEM) images, selected area electron diffraction (SAED), energy dispersive X-ray analysis (EDAX), and magneto-optical Faraday rotation (FR). Heat treatment of the glasses results in substantial changes of their structure and properties: ferrite nanoparticles of different size, composition, and structure arise in glass matrices. For several series of glasses with the same composition and molar concentration of the paramagnetic additions, the heat treatment regimes (temperature and duration) have been shown to be the main factors controlling the particle size and the order in the crystallite arrangements. Ensembles of particles in theirs turn determine magnetic and magneto-optical properties of glass as a whole. A correlation between the characteristics of nanoparticles and the heat treatment regimes is discussed qualitatively.

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Держатели документа:
Kirensky Institute of Physics, Siberian Branch of RAS, Krasnoyarsk, Russian Federation
S. I. Vavilov State Optical Institute, St.Petersburg, Russian Federation
Boreskov Institute of Catalysis, Siberian Branch of RAS, Novosibirsk, Russian Federation

Доп.точки доступа:
Edelman, I. S.; Эдельман, Ирина Самсоновна; Ivanova, O. S.; Иванова, Оксана Станиславовна; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Stepanov, S.; Zaikovskiy, V. I.
}
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18.

Identification of ε-Fe2O3 nano-phase in borate glasses doped with Fe and Gd / O. S. Ivanova [et al.] // J. Magn. Magn. Mater. - 2016. - Vol. 401. - P. 880-889, DOI 10.1016/j.jmmm.2015.10.126. - Cited References: 40. - This work was supported partly by the Russian Foundation for Basic Research, Grants No 14-02-01211-a and by the President of Russia Grant No. NSh-2886.2014.2. Authors are grateful to G.A. Bukhtiyarova and U.N. Martyanov for the assistance in the ε-Fe2O3 nanoparticles prepared by a wet chemical pore filling impregnation method and for the discussion of the obtained results . - ISSN 0304-8853

РУБ Materials Science, Multidisciplinary + Physics, Condensed Matter
Рубрики:
MAGNETIC-PROPERTIES
   IRON-OXIDE
   NANOPARTICLES
   CERAMICS
   CRYSTAL
   PARTICLES
   SURFACE
Кл.слова (ненормированные):
Magnetic nanoparticles -- ε-Fe2O3 -- Magnetic circular dichroism -- Electron magnetic resonance
Аннотация: A new type of magnetic nanoparticles was revealed in borate glasses co-doped with low contents of iron and gadolinium. Structure and magnetic properties of the particles differ essentially from that of the α-Fe2O3, γ-Fe2O3, or Fe3O4 nanoparticles which were detected earlier in similar glass matrices. Transmission electron microscopy including STEM-HAADF and EDX, synchrotron radiation-based XRD, static magnetic measurements, magnetic circular dichroism, and electron magnetic resonance studies allow referring the nanoparticles to the iron oxide phase-ε-Fe2O3. Analysis of the data set has shown that it is Gd atoms that govern the process of nanoparticles' nucleation and its incorporation into the particles in different proportions can be used to adjust their magnetic and magneto-optical characteristics. © 2015 Elsevier B.V.

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Держатели документа:
L.V. Kirensky Institute of Physics, Siberian Branch of RAS, Krasnoyarsk, Russian Federation
Siberian Federal University, Krasnoyarsk, Russian Federation
NRC Kurchatov Institute, Moscow, Russian Federation
Boreskov Institute of Catalysis, Siberian Branch of RAS, Novosibirsk, Russian Federation
Novosibirsk State University, Novosibirsk, Russian Federation
Vavilov State Optical Institute, All-Russia Research Center, Petersburg, Russian Federation

Доп.точки доступа:
Ivanova, O. S.; Иванова, Оксана Станиславовна; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Edelman, I. S.; Эдельман, Ирина Самсоновна; Petrakovskaja, E. A.; Петраковская, Элеонора Анатольевна; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Zubavichus, Y. V.; Zaikovskii, V .I.; Stepanov, S. A.
}
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19.

    Influence of Glass Matrix on Magneto-Optical Activity of f-f Transitions in Dy(3+) Ion / A. L. Sukhachev, A. Ya. Strokova, A. V. Malakhovskii // Solid State Phenomena. - 2011. - Vol. 168-169. - P. 557-560, DOI 10.4028/www.scientific.net/SSP.168-169.557. - Cited Reference Count: 4 . - ISBN 1012-0394
Рубрики:
Materials Science, Multidisciplinary
   Physics, Condensed Matter
Кл.слова (ненормированные):
magnetic circular dichroism -- magneto-optical activity -- rare earth glasses
Аннотация: The absorption and magnetic circular dichroism spectra of f-f transitions (6)H(15/2) -> (6)F(3/2), (6)F(5/2), (6)(F(7/2) + H(5/2)) and (6)(F(9/2) + H(7/2)) in Dy(3+) ion were studied in the glasses: Dy(2)O(3)-P(2)O(5)-SiO(2)-GeO(2) and Dy(2)O(3)-La(2)O(3)-Al(2)O(3)-B(2)O(3)-SiO(2)-GeO(2) with different concentrations of Dy(3+) ions in temperature range 100-300 K. :Basing on this data, absolute values and temperature dependences of the paramagnetic magneto-optical activity (MOA) of the transitions were determined. The origin of the MOA of f-f transitions was analyzed with the help of two models. In the first model, MOA is considered as a consequence of admixture of states with opposite parity by odd components of crystal field. The second approach is based on the Judd-Ofelt theory. The same f-f transitions reveal different values and temperature dependences in different glasses, what testifies to a different symmetry of the nearest environment of Dy(3+) ions in these glasses.

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Держатели документа:
SB RAS, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia

Доп.точки доступа:
Sukhachev, A. L.; Сухачев, Александр Леонидович; Strokova, A. Yu.; Строкова, Алёна Юрьевна; Malakhovskii, A. V.; Малаховский, Александр Валентинович; Russian Acad Sci, Inst Metal Phys; Euro-Asian Symposium "Trends in MAGnetism"(4 ; 2010 ; Jun.-Jul. ; Ekaterinburg); "Trends in MAGnetism", Euro-Asian Symposium(4 ; 2010 ; Jun.-Jul. ; Ekaterinburg)
}
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20.

Intensities f-f transitions in Pr3+ and Dy3+ in glasses in the near-IR spectral range / I. S. Edelman [et al.] // Phys. Solid State. - 2001. - Vol. 43, Is. 6. - P. 1037-1042, DOI 10.1134/1.1378142. - Cited References: 21 . - ISSN 1063-7834

РУБ Physics, Condensed Matter
Рубрики:
OXIDE GLASSES
Аннотация: The absorption spectra of Pr3+ and Dy3+ ions in three glass matrices (SiO2-P2O5-GeO2, Al2O3-B2O3-SiO2, and LiB3O5) are thoroughly studied in the near-IR spectral range (4600-14 300 cm(-1)). The temperature dependences of the intensity, the width, and the location of the absorption bands observed are investigated for the first time. It is shown that the f-f transitions in the studied glasses ate allowed by static odd distortions in the environment of the rare-earth ions and these distortions decrease with an increase in temperature. A comparative analysis of the absorption band parameters and their temperature behavior in different materials makes it possible to determine the differences in magnitudes, symmetries, and dispersions of the distortions in the nearest environment of rare-earth ions in different glasses. (C) 2001 MAIK "Nauka/Interperiodica".

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Держатели документа:
Russian Acad Sci, LV Kirensky Phys Inst, Siberian Div, Krasnoyarsk 660036, Russia
Bar Ilan Univ, IL-52900 Ramat Gan, Israel
SI Vavilov State Opt Inst, All Russia Res Ctr, St Petersburg 199034, Russia
ИФ СО РАН

Доп.точки доступа:
Edelman, I. S.; Эдельман, Ирина Самсоновна; Malakhovskii, A. V.; Малаховский, Александр Валентинович; Potseluyko, A. M.; Zarubina, T. V.; Zamkov, A. V.; Замков, Анатолий Васильевич
}
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