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Temperature/component-dependent luminescence in lead-free hybrid metal halides for temperature sensor and anti-counterfeiting / G. Zhou, Y. Wang, Y. Mao [et al.] // Adv. Funct. Mater. - 2024. - Ст. 2401860, DOI 10.1002/adfm.202401860. - Cited References: 89. - G.J.Z. and Y.T.W. contributed equally to this work. This work was supported by the National Natural Science Foundation of China (No.52202177, 22271211), Fundamental Research Program of Shanxi Province (No.20210302124054), Science and Technology Innovation Project of Colleges and Universities in Shanxi Province (No.2021L262), 1331 Project of Shanxi Province, Postgraduate Innovation Project of Shanxi Province (No.2023KY462), and supported by the Ministry of Science and High Education of Russian Federation (No.FSRZ-2023-0006). The authors would like to thank Prof. Haijun Jiao, Leibniz-Institut für Katalyse e.V., Germany, for the theoretical support on the electron-transition mechanism . - Article in press. - ISSN 1616-301X. - ISSN 1616-3028
Кл.слова (ненормированные):
electron-transition -- hybrid metal halides -- optical-functional applications -- self-trapped excitons -- tunable photoluminescence
Аннотация: Hybrid metal halides (HMHs) have emerged as a promising platform for optically functional crystalline materials, but it is extremely challenging to thoroughly elucidate the electron transition coupled to additional ligand emission. Herein, to discover sequences of lead-free HMHs with distinct optically active metal cations are aimed, that is, Sb3+ (5s2) with the lone-pair electron configuration and In3+ (4d10) with the fully-filled electron configuration. (Me2NH2)4MCl6·Cl (Me = −CH3, M = Sb, In) exhibits the superior temperature/component-dependent luminescence behaviors resulting from the competition transition between triplet-states (Tn-S0) self-trapped excitons (STEs) of inorganic units and singlet-state (S1-S0) of organic cations, which is manipulated by the optical activity levels of [SbCl6]3− and [InCl6]3−. The bonding differences between Sb3+/In3+ and Cl− in terms of electronic excitation and hybridization are emphasized, and the different electron-transition mechanisms are established according to the PL spectra at the extreme temperature of 5 to 305 K and theoretical calculations. By fine-tuning the B-site Sb3+/In3+ alloying, the photoluminescence quantum yield (PLQY = 81.5%) and stability are optimized at 20% alloying of Sb3+. This research sheds light on the rules governing PL behaviors of HMHs, as well as exploring the optical-functional application of aviation temperature sensors and access-control systems.

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Держатели документа:
Key Laboratory of Magnetic Molecules and Magnetic Information Materials (Ministry of Education), School of Chemistry and Material Science, Shanxi Normal University, Taiyuan 030031, P. R. China
Laboratory of Crystal Physics, Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk 660036, Russia
International Research Center of Spectroscopy and Quantum Chemistry-IRC SQC, Siberian Federal University, Krasnoyarsk 660041, Russia
State Key Laboratory of Luminescent Materials and Devices, Guangdong Provincial Key Laboratory of Fiber Laser Materials and Applied Techniques, Guangdong Engineering Technology Research and Development Center of Special Optical Fiber Materials and Devices, School of Physics and Optoelectronics, South China University of Technology, Guangzhou, Guangdong 510641, P. R. China
College of Chemistry & Chemical Engineering, Key Laboratory of Interface Science and Engineering in Advanced Material, Ministry of Education, Taiyuan University of Technology, Taiyuan, Shanxi 030024, P. R. China

Доп.точки доступа:
Zhou, G.; Wang, Y.; Mao, Y.; Guo, C.; Zhang, J.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Xia, Z.; Zhang, X.-M.
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    Синтез, кристаллическая структура и термодинамические свойства апатитоподобных ванадато-германатов свинца гадолиния / Л. Т. Денисова, М. С. Молокеев, Е. О. Голубева, Н. А. Галиахметова // Журн. СФУ. Химия. - 2022. - Т. 15, № 1. - Ст. 128-136 ; J. Sib. Fed. Univ. Chem. - 2022, DOI 10.17516/1998-2836-0277. - Библиогр.: 25. - Авторы выражают благодарность Красноярскому региональному центру коллективного пользования ФИЦ КНЦ СО РАН. Работа выполнена при частичной финансовой поддержке в рамках государственного задания на науку ФГАОУ ВО «Сибирский федеральный университет», номер проекта FSRZ‑2020–0013 . - ISSN 1998-2836. - ISSN 2313-6049
   Перевод заглавия: Synthesis, crystal structure and thermodynamic properties of apatite-like lead gadolinium vanadato-germanates
Кл.слова (ненормированные):
апатиты -- твердофазный синтез -- кристаллическая структура -- высокотемпературная теплоемкость -- термодинамические свойства -- apatites -- solid-phase synthesis -- crystal structure -- high-temperature heat capacity -- thermodynamic properties
Аннотация: Методом твердофазных реакций обжигом на воздухе стехиометрических смесей PbO, Gd2O3, GeO2 и V2O5 в интервале температур 773–1073 K синтезированы апатиты Pb10-xGdx(GeO4)2+x(VO4)4-x (x = 0.5, 1.0). С использованием рентгеноструктурного анализа определена их кристаллическая структура. Методом дифференциальной сканирующей калориметрии измерена высокотемпературная теплоемкость (350–1000 K). По экспериментальным данным Cp = f(T) рассчитаны термодинамические свойства апатитов.
The Pb10-xGdx(GeO4)2+x(VO4)4-x (x = 0.5, 1.0) apatites were synthesized by the solid-phase synthesis by roasting stoichiometric mixtures of PbO, Gd2O3, GeO2, and V2O5 in air at temperatures of 773–1073 K. Their crystal structure was determined using X‑ray diffraction analysis. The high-temperature heat capacity (350–1000 K) was measured by differential scanning calorimetry. The experimental data Cp = f (T) were used to calculate the thermodynamic properties of apatites.

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Держатели документа:
Сибирский федеральный университет, Российская Федерация, Красноярск
Институт физики им. Л. В. Киренского ФИЦ КНЦ СО РАН, Российская Федерация, Красноярск

Доп.точки доступа:
Денисова, Л. Т.; Молокеев, Максим Сергеевич; Molokeev, M. S.; Голубева, Е. О.; Галиахметова, Н. А.; Siberian Federal University [FSRZ-2020-0013]

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Temperature dependent structural, dielectric, Raman, piezoresponse and photoluminescence investigations in sol-gel derived BCZT ceramics / I. Coondoo, A. Krylov, D. K. Sharma [et al.] // Mater. Chem. Phys. - 2022. - Vol. 277. - Ст. 125526, DOI 10.1016/j.matchemphys.2021.125526. - Cited References: 82. - I.C. and J.S.K would like to acknowledge financial assistance by national funds (OE), through FCT – Fundação para a Ciência e a Tecnologia, I.P., in the scope of the framework contract foreseen in the numbers 4, 5 and 6 of the article 23, of the Decree-Law 57/2016, of August 29, changed by Law 57/2017, of July 19. This work was developed within the scope of the project CICECO-Aveiro Institute of Materials, UIDB/50011/2020 & UIDP/50011/2020, financed by national funds through the FCT/MCTES. This work was partially developed within the scope of the project i3N, UIDB/50025/2020 & UIDP/50025/2020, financed by national funds through the FCT/MEC. Part of this work (A.K.) was supported by the Ministry of Science and Higher Education of the Russian Federation (grant no. 075-15-2021-588). This research used resources of the Ural Center for Shared Use “Modern nanotechnology”, Ural federal University, Russia and the Krasnoyarsk Regional Center of Research Equipment of Federal Research Center “Krasnoyarsk Science Center SB RAS”. The authors thank Dr. Gonzalo Irurueta, Center for Mechanical Engineering and Automation, University of Aveiro, Portugal and Dr. E. Venkata Ramana, Department of Physics, University of Aveiro, Portugal . - ISSN 0254-0584
Кл.слова (ненормированные):
Lead-free piezoelectrics -- Sol-gel -- Phase transitions -- Raman spectroscopy -- PFM -- Photoluminescence
Аннотация: 0.5Ba(Ti0.8Zr0.2)O3-0.5(Ba0.7Ca0.3)TiO3 [50BZT-50BCT or BCZT] based compounds have been the focus of a lot of research, particularly motivated by their high piezoelectric effect. However, the literature lacks an elaborate investigation of the phase transition behavior in BCZT ceramics obtained by wet chemistry processing. Here, we present an in-depth study on the temperature dependence of x-ray diffraction (XRD), Raman scattering, dielectric properties, local piezoresponse and photoluminescence (PL) to investigate the sequence of phase transitions in the BCZT ceramic synthesized via a chemical route. Phase formation was determined by Rietveld analysis of XRD data, while compositional homogeneity and elemental quantification of the compound was validated using energy dispersive x-ray spectroscopy (EDX) and x-ray photoelectron spectroscopy (XPS) studies. Detailed fitting of XPS data indicated the existence of Ti3+ species (∼6%) in the prepared BCZT. Phase transitions were examined by analyzing the modifications in the XRD profile of Bragg reflection {200} and anomalies observed in the temperature variation of dielectric and Raman spectra studied over a wide temperature range starting from 10K to beyond Curie temperature. Crystallographic transformation temperatures obtained from dielectric measurement agreed well with those assessed from the temperature evolution of Raman spectra. In addition to other transitions, Raman scattering results revealed the existence of a transition from to phase near −175 °C, a transition that has not been interpreted in BCZT (and generally not observed in parent BaTiO3 compound). The luminescence response was studied by photoluminescence (PL) spectroscopy in the temperature range 15–300 K. The position of the PL peak was observed to shift with temperature and discontinuities in the wavelength shift were noted near phase transitions. Evolution of domain morphology with temperature was examined by piezoresponse force microscopy technique. Consolidated results assign the phase sequence in sol-gel derived BCZT as: R(R3c)→-175±10°CR(R3m)→-50±10°CO→40±10°CT→120±10°CC.

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Department of Physics & CICECO – Aveiro Institute of Materials, University of Aveiro, Aveiro, 3810-193, Portugal
Laboratory of Molecular Spectroscopy, Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
DEMaC & CICECO – Aveiro Institute of Materials, University of Aveiro, Aveiro, 3810-193, Portugal
School of Natural Sciences and Mathematics, Ural Federal University, Ekaterinburg, 620026, Russian Federation
I3N-Aveiro, Department of Physics, University of Aveiro, Aveiro, 3810-193, Portugal
Physical Materials Science and Composite Materials Centre, Research School of Chemistry & Applied Biomedical Sciences, National Research Tomsk Polytechnic University, Tomsk, 634050, Russian Federation

Доп.точки доступа:
Coondoo, I.; Krylov, A. S.; Крылов, Александр Сергеевич; Sharma, D. K.; Krylova, S. N.; Крылова, Светлана Николаевна; Alikin, D.; Kumar, J. S.; Mirzorakhimov, A.; Melnikova, N.; Soares, M. J.; Kholkin, A. L.
}
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Synthesis, crystal structure and thermodynamic properties of apatite Pb3Bi2(GeO4)3 / L. T. Denisova, M. S. Molokeev, E. O. Golubeva [и др.] // Phys. Solid State. - 2022. - Vol. 64, Is. 7. - P. 889-893, DOI 10.21883/PSS.2022.07.54599.312. - Cited References: 30. - This work was partially supported within the scope of the state assignment for science of FSAEI HE ”Siberian Federal University“, project number FSRZ-2020-0013 . - ISSN 1063-7834. - ISSN 1090-6460
Кл.слова (ненормированные):
apatite bismuth-lead germanate -- solid-phase synthesis -- high-temperature heat capacity -- thermodynamic properties
Аннотация: Apatite Pb3Bi2(GeO4)3 was obtained by the solid-phase method from the initial oxides of PbO, Bi2O3 and GeO2 by sequential firing in air at temperatures of 773–1003 K. Its crystal structure has been refined by X-ray diffraction. The high-temperature heat capacity (350–1000 K) of this compound was measured by differential scanning calorimetry. Based on these data, the main thermodynamic functions are calculated.

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Публикация на русском языке Синтез, кристаллическая структура и термодинамические свойства апатита Pb3Bi2(GeO4)3 [Текст] / Л. Т. Денисова, М. С. Молокеев, Е. О. Голубева [и др.] // Физ. тверд. тела. - 2022. - Т. 64 Вып. 7. - С. 886-890

Держатели документа:
Siberian Federal University, Krasnoyarsk, Russia
Kirensky Institute of Physics, Federal Research Center KSC SB, Russian Academy of Sciences, Krasnoyarsk, Russia

Доп.точки доступа:
Denisova, L. T.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Golubeva, E. O.; Belousova, N. V.; Denisov, V. M.
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Efficiency of energy harvesting and storage using a multilayer capacitor based on BaTi0.86Sn0.14O3 ferroelectric lead-free ceramics / V. D. Fokina, V. S. Bondarev, E. I. Pogoreltsev, I. N. Flerov // Ceram. Int. - 2022. - Vol. 48, Is. 22. - P. 32966-32972, DOI 10.1016/j.ceramint.2022.07.227. - Cited References: 45 . - ISSN 0272-8842
Кл.слова (ненормированные):
Ferroelectric properties -- BaTiO3 and titanates -- Capacitors -- Energy harvesting/storage
Аннотация: The study of the parameters of energy harvesting and storage in the lead-free solid solution BaTi0.86Sn0.14O3 (BTSnO) was performed. The permittivity shows the behavior similar to a diffuse phase transition with the critical exponent γ = 1.84, which is close to the value characteristic of relaxors. Large values of the recoverable energy density, Wrec=(5.8–7.0)∙104 J/m3, and the energy storage efficiency coefficient, η=(82–94) %, are implemented in a wide temperature range, 30–87°С, at a low electric field, E = 18.5 kV/cm. For the first time, the analysis of the Olsen cycle was performed using two phase diagrams: polarization – electric field and entropy – temperature. A fairly good agreement was found between the values of the energy conversion density, ND ≈ 0.15 J/cm3, which was determined using two approaches. A universal parameter is proposed for comparing the energy harvesting density for the materials studied in different ranges of temperature and electric fields.

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Держатели документа:
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
Siberian Federal University, Krasnoyarsk, 660074, Russian Federation

Доп.точки доступа:
Fokina, V. D.; Фокина, Валентина Дмитриевна; Bondarev, V. S.; Бондарев, Виталий Сергеевич; Pogoreltsev, E. I.; Погорельцев, Евгений Ильич; Flerov, I. N.; Флёров, Игорь Николаевич
}
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Solvatochromic Photoluminescent Effects in All-Inorganic Manganese(II)-Based Perovskites by Highly Selective Solvent-Induced Crystal-to-Crystal Phase Transformations / H. Xiao, P. P. Dang, X. H. Yun [et al.] // Angew. Chem. Int. Edit. - 2021. - Vol. 60, Is. 7. - P. 3699-3707, DOI 10.1002/anie.202012383. - Cited References: 85. - This work was supported by National Natural Science Foundation of China (NSFC 51932009, 51772288, 52072349, 51672259) and the Joint Fund Project to Promote Science and Technology Cooperation Across the Taiwan Straits (U2005212), the Science and Technology Cooperation Fund between Chinese and Australian Governments (2017YFE0132300), CAS-Croucher Funding Scheme for Joint Laboratories (CAS18204), Chinese Academy of Sciences (YZDY-SSWJSC018) . - ISSN 1433-7851. - ISSN 1521-3773

РУБ Chemistry, Multidisciplinary
Рубрики:
LEAD-FREE
   HALIDE PEROVSKITE
   NANOCRYSTALS
   MN2+
   LUMINESCENCE
Кл.слова (ненормированные):
lead-free materials -- low-dimensional perovskites -- luminescence -- manganese -- phase transitions
Аннотация: The development of lead‐free perovskite photoelectric materials has been an extensive focus in the recent years. Herein, a novel one‐dimensional (1D) lead‐free CsMnCl3(H2O)2 single crystal is reported with solvatochromic photoluminescence properties. Interestingly, after contact with N,N‐dimethylacetamide (DMAC) or N,N‐dimethylformamide (DMF), the crystal structure can transform from 1D CsMnCl3(H2O)2 to 0D Cs3MnCl5 and finally transform into 0D Cs2MnCl4(H2O)2. The solvent‐induced crystal‐to‐crystal phase transformations are accompanied by loss and regaining of water of crystallization, leading to the change of the coordination number of Mn2+. Correspondingly, the luminescence changes from red to bright green and finally back to red emission. By fabricating a test‐paper containing CsMnCl3(H2O)2, DMAC and DMF can be detected quickly with a response time of less than one minute. These results can expand potential applications for low‐dimensional lead‐free perovskites.

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Держатели документа:
Chinese Acad Sci, Changchun Inst Appl Chem, State Key Lab Rare Earth Resource Utilizat, 5625 Renmin St, Changchun 130022, Peoples R China.
Univ Sci & Technol China, Hefei 230026, Peoples R China.
China Univ Geosci, Fac Mat Sci & Chem, Minist Educ, Engn Res Ctr Nanogeomat, Wuhan 430074, Peoples R China.
RAS, SB, Lab Crystal Phys, Kirensky Inst Phys,Fed Res Ctr,KSC, Krasnoyarsk 660036, Russia.
Siberian Fed Univ, Krasnoyarsk 660041, Russia.
Far Eastern State Transport Univ, Dept Phys, Khabarovsk 680021, Russia.

Доп.точки доступа:
Xiao, Hui; Dang, Peipei; Yun, Xiaohan; Li, Guogang; Wei, Y.i.; Xiao, Xiao; Zhao, Yajie; Molokeev, M. S.; Молокеев, Максим Сергеевич; Cheng, Ziyong; Lin, Jun
}
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    Solvatochromic photoluminescent effects in all-inorganic manganese(II)-based perovskites by highly selective solvent-induced crystal-to-crystal phase transformations / H. Xiao, P. Dang, X. Yun [et al.] // Angew. Chem. - 2021. - Vol. 133, Is. 7. - P. 3743-3751, DOI 10.1002/ange.202012383. - Cited References: 73. - This work was supported by National Natural Science Foundation of China (NSFC 51932009, 51772288, 52072349, 51672259) and the Joint Fund Project to Promote Science and Technology Cooperation Across the Taiwan Straits (U2005212), the Science and Technology Cooperation Fund between Chinese and Australian Governments (2017YFE0132300), CAS-Croucher Funding Scheme for Joint Laboratories (CAS18204), Chinese Academy of Sciences (YZDY-SSWJSC018) . - ISSN 1521-3757
   Перевод заглавия: Сольватохромные фотолюминесцентные эффекты в полностью неорганическом перовските на основе марганца (II), вызванные высокоселективными фазовыми превращениями кристалла-кристалл, индуцированными растворителем
Кл.слова (ненормированные):
lead-free materials -- low-dimensional perovskites -- luminescence -- manganese -- phase transitions
Аннотация: The development of lead‐free perovskite photoelectric materials has been an extensive focus in the recent years. Herein, a novel one‐dimensional (1D) lead‐free CsMnCl3(H2O)2 single crystal is reported with solvatochromic photoluminescence properties. Interestingly, after contact with N,N‐dimethylacetamide (DMAC) or N,N‐dimethylformamide (DMF), the crystal structure can transform from 1D CsMnCl3(H2O)2 to 0D Cs3MnCl5 and finally transform into 0D Cs2MnCl4(H2O)2. The solvent‐induced crystal‐to‐crystal phase transformations are accompanied by loss and regaining of water of crystallization, leading to the change of the coordination number of Mn2+. Correspondingly, the luminescence changes from red to bright green and finally back to red emission. By fabricating a test‐paper containing CsMnCl3(H2O)2, DMAC and DMF can be detected quickly with a response time of less than one minute. These results can expand potential applications for low‐dimensional lead‐free perovskites.

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Держатели документа:
State Key Laboratory of Rare Earth Resource Utilization, Changchun Institute of Applied Chemistry, Chinese Academy of Sciences, 5625 Renmin Street, Changchun, 130022 China
University of Science and Technology of China, Hefei, 230026 China
Engineering Research Center of Nano-Geomaterials of Ministry of Education, Faculty of Materials Science and Chemistry, China University of Geosciences, Wuhan, 430074 China
Laboratory of Crystal Physics, Kirensky Institute of Physics, Federal Research Center KSC SB RAS, 660036 Krasnoyarsk, Russia
Siberian Federal University, 660041 Krasnoyarsk, Russia
Department of Physics, Far Eastern State Transport University, 680021 Khabarovsk, Russia

Доп.точки доступа:
Xiao, Hui; Dang, Peipei; Yun, Xiaohan; Li, Guogang; Wei, Yi; Xiao, Xiao; Zhao, Yajie; Molokeev, M. S.; Молокеев, Максим Сергеевич; Cheng, Ziyong; Lin, Jun
}
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Temperature-dependent Raman spectroscopy, domain morphology and photoluminescence studies in lead-free BCZT ceramic / I. Coondoo, N. Panwar, S. Krylova [et al.] // Ceram. Int. - 2021. - Vol. 47, Is. 2. - P. 2828-2838, DOI 10.1016/j.ceramint.2020.09.137. - Cited References: 65. - I.C. would like to thank financial assistance by national funds (OE), through FCT – Fundação para a Ciência e a Tecnologia, I.P., in the scope of the framework contract foreseen in the numbers 4, 5 and 6 of the article 23, of the Decree-Law 57/2016, of August 29, changed by Law 57/2017, of July 19. This work was developed within the scope of the project CICECO-Aveiro Institute of Materials, UIDB/50011/2020 & UIDP/50011/2020, financed by national funds through the Portuguese Foundation for Science and Technology / MCTES . The authors would also like to acknowledge the Ural Center for Shared Use “Modern nanotechnology”, Ural Federal University, Russia and the Krasnoyarsk Regional Center of Research Equipment of Federal Research Center “Krasnoyarsk Science Center SB RAS”. The authors would like to thank Dr. E. Venkata Ramana, Department of Physics, University of Aveiro for the dielectric measurements. The work was supported by Government of the Russian Federation (Act 211, 440 Agreement 02.A03.21.0006) . - ISSN 0272-8842
Кл.слова (ненормированные):
Lead-free ceramics -- Raman spectroscopy -- Domain morphology -- Photoluminescence
Аннотация: Present work focuses on detailed temperature-dependent X-ray diffraction, Raman scattering, domain configuration, and photoluminescence (PL) studies in the (Ba0·85Ca0.15) (Zr0·10Ti0.90)O3 (BCZT) ceramics. The comprehensive Raman spectroscopy analysis in the present work not only validates the presence of the intermediate orthorhombic phase in BCZT, but also provides evidence of another transition: rhombohedral R3c phase to R3m at low temperature. Temperature behaviour of the lowest frequency transverse optical mode (soft E (TO) phonon) and hard modes was studied. Temperature dependence of peak positions, intensities, and linewidths of Raman phonon modes signalled the presence of phase transitions near −50 ± 5 °C, 0±5 °C, 35±5 °C and 110 ± 10 °C. Evolution of domain morphology occurring at phase transitions above room temperature was studied by piezoresponse force microscopy technique. Analysis of PL spectra revealed disorder/heterogeneity in the sample and indicated the existence of self-trapped excitons. PL spectra are composed of four distinct colour components (~2.55eV:blue, ~2.32eV:green, ~2.08eV:orange and ~1.78eV:red).

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Держатели документа:
Department of Physics & CICECO – Aveiro Institute of Materials, University of Aveiro, Aveiro, 3810-193, Portugal
Department of Physics, Central University of Rajasthan, BandarsindriRajasthan 305817, India
Laboratory of Molecular Spectroscopy, Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk660036, Russian Federation
School of Natural Sciences and Mathematics, Ural Federal University, Ekaterinburg620026, Russian Federation
I3N-Aveiro, Department of Physics, University of Aveiro, Aveiro, 3810-193, Portugal

Доп.точки доступа:
Coondoo, I.; Panwar, N.; Krylova, S. N.; Крылова, Светлана Николаевна; Krylov, A. S.; Крылов, Александр Сергеевич; Alikin, D.; Jakka, S. K.; Turygin, A.; Shur, V. Y.; Kholkin, A. L.
}
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Crystal structure, luminescence, and thermodynamic properties of Pb10–xEux(GeO4)2+x(VO4)4–x (x = 0.1, 0.2, 0.3) substituted apatites / L. T. Denisova, M. S. Molokeev, A. S. Aleksandrovskii [et al.] // Inorg. Mater. - 2021. - Vol. 57, Is. 11. - P. 1158-1166, DOI 10.1134/S0020168521110030. - Cited References: 26. - This work was supported in part by the Russian Federation Ministry of Science and Higher Education as part of the state research target for the Siberian Federal University federal state autonomous educational institution of higher education, project no. FSRZ-2020-0013 . - ISSN 0020-1685
Кл.слова (ненормированные):
apatites -- lead europium germanatovanadates -- X-ray diffraction -- structure -- luminescence -- high-temperature heat capacity
Аннотация: Pb10 – xEux(GeO4)2 + x(VO4)4 – x (x = 0.1, 0.2, 0.3) Eu-substituted lead germanatovanadates with the apatite structure have been prepared by solid-state reactions, via firing in air in the temperature range 773–1073 K, using oxides (PbO, Eu2O3, GeO2, and V2O5) as starting materials. Using X-ray diffraction, we have determined the hexagonal cell parameters (sp. gr. P63/m) of the synthesized phases and refined their crystal structure (the atomic position coordinates, isotropic thermal parameters, and principal bond lengths in their structure are presented). We have measured the luminescence spectra of the Pb10 – xEux(GeO4)2 + x(VO4)4 – x (x = 0.1, 0.2, 0.3) apatites and shown that europium concentration has little effect on the shape of the luminescence spectra. Using experimental heat capacity data obtained for polycrystalline samples by differential scanning calorimetry in the temperature range 350–1050 K, we calculated the main thermodynamic functions of the Eu-substituted lead germanatovanadates.

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Публикация на русском языке Кристаллическая структура, люминесцентные и термодинамические свойства замещенных апатитов Pb10 – xEux(GeO4)2 + x(VO4)4 – x (x = 0.1, 0.2, 0.3) [Текст] / Л. Т. Денисова, М. С. Молокеев, А. С. Александровский [и др.] // Неорган. матер. - 2021. - Т. 57 № 11. - С. 1226-1234

Держатели документа:
Siberian Federal University, Krasnoyarsk, 660041, Russian Federation
Kirensky Institute of Physics, Krasnoyarsk Scientific Center (Federal Research Center), Siberian Branch, Russian Academy of Sciences, Krasnoyarsk, 660036, Russian Federation
Baikov Institute of Metallurgy and Materials Science, Russian Academy of Sciences, Moscow, 119334, Russian Federation

Доп.точки доступа:
Denisova, L. T.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Aleksandrovskii, A. S.; Александровский, Александр Сергеевич; Kargin, Y. F.; Golubeva, E. O.; Denisov, V. M.
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10.

    Review of lead-free Bi-based dielectric ceramics for energy-storage applications / L. S. Li, P. Y. Fan, M. Q. Wang [et al.] // J. Phys. D. - 2021. - Vol. 54, Is. 29. - Ст. 293001, DOI 10.1088/1361-6463/abf860. - Cited References: 177. - The authors gratefully acknowledge the support of the National Natural Science Foundation of China (Nos. 51672092, U1732117 and 51902111), the China Postdoctoral Science Foundation (No. 2019M662602), the Natural Science Foundation of Guangxi (AA138162, GA245006, FA198015, and AA294014), the High-Level Innovation Team and Outstanding Scholar Program of Guangxi Institutes, and the Open Fund of the Guangxi Key Laboratory of Information Materials (No.191015-K). The authors thank the projects supported by the Guangdong HUST Industrial Technology Research Institute, the Guangdong Provincial Key Laboratory of Digital Manufacturing Equipment (2020B1212060014) and the DongGuan Innovative Research Team Program (2020607101007). The authors wish to thank the Analytical and Testing Center of Huazhong University of Science and Technology for their help with related tests. In particular, the authors appreciate the valuable suggestions and comments made by the the anonymous reviewers and the editor, Professor Huiyun Liu . - ISSN 0022-3727. - ISSN 1361-6463
   Перевод заглавия: Обзор: Bi-содержащие бессвинцовые керамики для устройств хранения энергии

РУБ Physics, Applied
Рубрики:
TRANSMISSION ELECTRON-MICROSCOPY
STRONTIUM-TITANATE CERAMICS
Кл.слова (ненормированные):
dielectric materials -- energy storage -- lead-free -- Bi-based ceramics
Аннотация: Dielectric energy-storage ceramics have the advantages of high power density and fast charge and discharge rates, and are considered to be excellent candidate materials for pulsed power-storage capacitors. At present, the application of dielectric energy-storage ceramics is hindered by their low energy density and the fact that most of them contain elemental lead. Therefore, lead-free dielectric energy-storage ceramics with high energy storage density have become a research hot spot. In this paper, we first present the requirements that dielectric energy-storage capacitors impose on the properties of ceramic materials. We then review our previous research work combined with research progress into bismuth (Bi)-based lead-free energy-storage ceramics including Bi0.5Na0.5TiO3 (BNT), BiFeO3, and Bi0.2Sr0.7TiO3, in which the composition design ideas and related energy-storage characteristics of BNT-based lead-free energy-storage ceramics are emphasized. At the same time, we highlight the problems faced by Bi-based lead-free energy-storage ceramics and some strategies for addressing them. Finally, we examine the future prospects of research into Bi-based lead-free energy-storage ceramics.

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Держатели документа:
Huazhong Univ Sci & Technol, State Key Lab Mat Proc & & Mould Technol, Sch Mat Sci & Engn, Wuhan 430074, Peoples R China.
Guangdong HUST Ind Technol Res Inst, Dongguan 523808, Peoples R China.
Fukuoka Univ, Fac Sci, Fukuoka 8140180, Japan.
Brno Univ Technol, Cent European Inst Technol CEITEC, Brno, Czech Republic.
RAS, SB, Kirensky Inst Phys, Akademgorodok 50-38, Krasnoyarsk 660036, Russia.
Tsinghua Univ, Sch Vehicle & Mobil, State Key Lab Automot Safety & Energy, Beijing 100084, Peoples R China.
Guilin Univ Technol, Guangxi Key Lab Opt & Elect Mat & Devices, Guilin 541004, Peoples R China.

Доп.точки доступа:
Li, Lisong; Fan, Pengyuan; Wang, Mengqi; Takesue, Naohisa; Salamon, David; Vtyurin, A. N.; Втюрин, Александр Николаевич; Zhang, Yangjun; Tan, Hua; Nan, B.o.; Lu, Y.a.; Liu, Laijun; Zhang, Haibo
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