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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : LOSEVA G. V., MUKOED G. M., Ovchinnikov S. G., RYABINKINA L. I.
Заглавие : ELECTRIC AND MAGNETIC-PROPERTIES OF MES.FE2O3 OXYSULFIDES
Место публикации : Fiz. Tverd. Tela: MEZHDUNARODNAYA KNIGA, 1992. - Vol. 34, Is. 6. - P1765-1769. - ISSN 0367-3294
Примечания : Cited References: 16
Предметные рубрики: INSULATOR TRANSITION
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Sal'nikova E. I., Denisenko Y., Aleksandrovsky A. S., Kolesnikov I. E., Lahderanta E., Andreev P. O., Azarapin N. O., Andreev O. V., Basova S. A., Matigorov A. V.
Заглавие : Synthesis and optical properties RE2O2S:Ln (RE = La, Y; Ln = Ce, Eu, Dy, Er)
Место публикации : J. Solid State Chem. - 2019. - Vol. 279. - Ст.120964. - ISSN 00224596 (ISSN), DOI 10.1016/j.jssc.2019.120964
Примечания : Cited References: 53
Аннотация: The phase formation sequence was studied in the preparation of solid solutions of RE2O2S: Ln’ (RE = La, Y; Ln’ = Ce, Eu, Dy, Er) by the reduction of the match co-precipitated sulfates, followed by sulfidization of the reduction products. For uniform distribution of cations in the matrix, a method of chemical homogenization was used, consisting in the preparation of an aqueous solution containing all the necessary cations and their subsequent precipitation in the form of sulfates. The use of sulfates as precursors facilitates the process of obtaining solid solutions of oxysulfides, since sulfates already contain SO4 2--ions. The phase and morphological certification of the obtained solid solutions was carried out. The study of steady state luminescent properties demonstrated characteristic bands which are assigned to 4f-4f and 5d-4f transition. The obtained results showed the possibility of applying the method to synthesize optical ceramics based on solid solutionsRE2O2S: Ln (RE = La, Y; Ln = Ce, Eu, Dy, Er).
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Sal'nikova E. I., Denisenko Y. G., Kolesnikov I. E., Lahderanta E., Andreev O. V., Azarapin N. O., Basova S. A., Gubin A. A., Oreshonkov A. S.
Заглавие : Synthesis and luminescent properties of (RE0.95Ln0.05)2O2S (RE = La, Y; Ln = Ho, Tm)
Место публикации : J. Solid State Chem. - 2021. - Vol. 293. - Ст.121753. - ISSN 00224596 (ISSN), DOI 10.1016/j.jssc.2020.121753
Примечания : Cited References: 33
Аннотация: Solid solutions of oxysulfides (RE0.95Ln0.05)2O2S (RE = La, Y; Ln = Ho, Tm) were obtained by hydrogen reduction of the co-precipitated sulfates followed by sulfidation of the reaction products. The crystal chemical characteristics of the obtained compounds were refined by the Rietveld method. Morphological certification of particles in the dynamics of synthesis was performed. Most of the particles produced by chemical reactions have a cut that indicates the formation of a compound with a hexagonal syngony with angles of 60 and 120°. This indicates that the thermal effect of gaseous reagents H2, H2S on sulfates leads to heterogeneous reactions of thermal dissociation and the formation of new phases. Steady state luminescence properties displayed characteristic sharp bands corresponding to 4f-4f transitions. Luminescence decay curves of all studied samples showed monoexponential decay with microsecond and hundreds microsecond lifetimes depending on doping ions. Calculated color coordinates of Ho3+ and Tm3+-doped powders make them promising candidates to be used as phosphors.
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