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Formation and evolution of magnetic nanoparticles in borate glass simultaneously doped with Fe and Mn oxides / J. . Kliava [et al.] // J. Appl. Phys. - 2008. - Vol. 104, Is. 10. - Ст. 103917, DOI 10.1063/1.3021289. - Cited References: 37. - A financial support from the Russian Foundation for Basic Research (RFBR)-CNRS (Grant No. 07-02-92174) is highly appreciated. R. Ivantsov is grateful to the Russian Science Support Foundation. Y. Yeshurun acknowledges the support of the Israel Scienc Foundation (ISF). . - ISSN 0021-8979

РУБ Physics, Applied
Рубрики:
COBALT FERRITE PARTICLES
   SUPERPARAMAGNETIC RESONANCE
   GAMMA-FE2O3 NANOPARTICLES
   MATRIX
   SIZE
   SYSTEMS
Кл.слова (ненормированные):
aluminium compounds -- borate glasses -- coercive force -- Faraday effect -- heat treatment -- iron compounds -- magnetic hysteresis -- magnetic particles -- magnetic susceptibility -- manganese compounds -- Mossbauer effect -- nanoparticles -- paramagnetic materials -- potassium compounds -- remanence -- superparamagnetism -- transmission electron microscopy -- X-ray chemical analysis -- Atomic spectroscopy -- Auger electron spectroscopy -- Crystal structure -- Electric relays -- Electronic medical equipment -- Ferrite -- Ferrites -- Glass -- Heat treatment -- Hysteresis -- Hysteresis loops -- Magnetic properties -- Magnetic resonance measurement -- Magnetic susceptibility -- Magnetism -- Manganese -- Manganese compounds -- Molybdenum -- Nanoparticles -- Optical properties -- Ozone water treatment -- Polydispersity -- Superparamagnetism -- Borate glasses -- Concentration ratios -- Electron magnetic resonances -- Emr spectrums -- Experimental techniques -- Faraday rotations -- Glass compositions -- Glass matrixes -- Glass preparations -- Magnetic measurements -- Magnetic nano particles -- Magnetic orders -- Magnetically ordered systems -- Magneto-optical properties -- Manganese ferrites -- Mean diameters -- Mn oxides -- Phase states -- Polydisperse nanoparticles -- Remnant magnetizations -- Ssbauer spectroscopies -- Superparamagnetic -- Superparamagnetic states -- Thermal treatments -- Variable temperatures -- Magnetic materials
Аннотация: Evolution of the phase state of paramagnetic additions at various stages of synthesis and subsequent thermal treatment of glasses of the system Al(2)O(3)-K(2)O-B(2)O(3) simultaneously doped with Fe(2)O(3) and MnO is studied by means of a combination of experimental techniques: Faraday rotation (FR), electron magnetic resonance (EMR), transmission electron microscopy (TEM), Mossbauer spectroscopy, and magnetic measurements. Both FR and EMR show that magnetically ordered clusters occur already at the first stage of the glass preparation. In particular, for the ratio of the Fe and Mn oxides in the charge close to 3:2, fine magnetic nanoparticles are formed with characteristics similar to those of manganese ferrite. By computer simulating the EMR spectra at variable temperatures, a superparamagnetic nature of these nanoparticles is confirmed and their mean diameter is estimated as approximately 3.2 nm. In the thermally treated glasses larger magnetic nanoparticles are formed, giving rise to FR spectra, characteristic of magnetically ordered systems, and the EMR spectra different from those in as-prepared glasses but also showing superparamagnetic narrowing. The Mossbauer spectroscopy corroborates the manganese ferrite structure of the nanoparticles and indicates their coexistence in the ferrimagnetic and superparamagnetic states. The TEM shows the presence of polydisperse nanoparticles on the background of the glass matrix, and electron diffraction of a selected region containing larger particles indicates a crystal structure close to that of MnFe(2)O(4). Energy-dispersive atomic x-ray spectra confirm that the major part of Fe and Mn introduced to the glass composition is gathered in the particles, with the concentration ratio close to 2:1, characteristic of bulk MnFe(2)O(4). Magnetic hysteresis loops of samples subjected to an additional thermal treatment demonstrate a strong increase in the coercive force, remnant magnetization, and high-field magnetic susceptibility with temperature decrease. The consistent results obtained using various techniques demonstrate that the formation of nanoparticles with characteristics close to those of MnFe(2)O(4) confers to these glasses magnetic and magneto-optical properties typical of substances possessing magnetic order.

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Держатели документа:
[Kliava, J.] Univ Bordeaux 1, CNRS, UMR 5798, CPMOH, F-33405 Talence, France
[Edelman, I.
Ivanova, O.
Ivantsov, R.
Bayukov, O.
Petrakovskaja, E.
Stepanov, S.] RAS, Siberian Branch, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
[Zaikovskiy, V.] RAS, Siberian Branch, Boreskov Inst Catalysis, Novosibirsk 630090, Russia
[Bruckental, I.
Yeshurun, Y.] Bar Ilan Univ, Dept Phys, IL-52900 Ramat Gan, Israel
[Stepanov, S.] SI Vavilov State Opt Inst, St Petersburg 199034, Russia
ИФ СО РАН
CPMOH, Universit? Bordeaux, 1-CNRS UMR 5798, 33405 Talence Cedex, France
Kirensky Institute of Physics, Siberian Branch of RAS, 660036 Krasnoyarsk, Russian Federation
Boreskov Institute of Catalysis, Siberian Branch, RAS, 630090 Novosibirsk, Russian Federation
Department of Physics, Bar-Ilan University, Ramat-Gan 52900, Israel
S. I. Vavilov State Optical Institute, St. Petersburg 199034, Russian Federation

Доп.точки доступа:
Kliava, J.; Edelman, I. S.; Эдельман, Ирина Самсоновна; Ivanova, O. S.; Иванова, Оксана Станиславовна; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Bayukov, O. A.; Баюков, Олег Артемьевич; Petrakovskaja, E. A.; Петраковская, Элеонора Анатольевна; Zaikovskiy, V.; Bruckental, I.; Yeshurun, Y.; Stepanov, S.
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Velikanov, D. A.
Magnetic properties of Ba2Cu3O4Cl2 / D. A. Velikanov, K. S. Rabinovich, L. L. Samoilenko // VI Euro-Asian Symposium "Trends in MAGnetism" (EASTMAG-2016) : abstracts / ed.: O. A. Maksimova, R. D. Ivantsov. - Krasnoyarsk : KIP RAS SB, 2016. - Ст. P2.16. - P. 158. - References: 4 . - ISBN 978-5-904603-06-9
Кл.слова (ненормированные):
layered cuprate -- magnetic moment -- coercivity -- remanence -- weak ferromagnet

Доп.точки доступа:
Rabinovich, K. S.; Рабинович, К. С.; Samoilenko, L. L.; Самойленко, Л. Л.; Великанов, Дмитрий Анатольевич; Euro-Asian Symposium "Trends in MAGnetism"(6 ; 2016 ; Aug. ; 15-19 ; Krasnoyarsk); "Trends in MAGnetism", Euro-Asian Symposium(6 ; 2016 ; Aug. ; 15-19 ; Krasnoyarsk); Институт физики им. Л.В. Киренского Сибирского отделения РАН

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Magnetic properties and L1 0 phase formation in CoPt nanoparticles / S. V. Komogortsev [et al.] // Diffusion and Defect Data Pt.B: Solid State Phenomena. - 2012. - Vol. 190. - P. 159-162, DOI 10.4028/www.scientific.net/SSP.190.159 . - ISBN 1012-0394. - ISBN 9783037854365
Кл.слова (ненормированные):
Hard magnetic -- Magnetic anisotropy -- Magnetic nanoparticles -- Remnant magnetization -- Annealing time -- CoPt nanoparticles -- Disorder-order -- Domain formation -- Hard magnetic -- Magnetic anisotropy energy -- Magnetic nanoparticles -- Phase formations -- Remnant magnetization -- Decomposition -- Magnetic anisotropy -- Magnetic materials -- Remanence -- Nanoparticles
Аннотация: The effect of the atomic disorder-order transformation on remanence, coercivity and magnetic anisotropy energy in CoPt nanoparticles prepared by thermal decomposition and annealed at 400oC for 4 and 16 hours has been studied. The observed remanence and magnetic anisotropy energy enhancement versus annealing time are discussed in the terms of ordering domain formation inside nanoparticles. В© (2012) Trans Tech Publications.

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Доп.точки доступа:
Komogortsev, S. V.; Комогорцев, Сергей Викторович; Chizhik, N. A.; Чижик Н.А.; Filatov, E. Yu.; Филатов Е.Ю.; Korenev, S. V.; Коренев С.В.; Shubin, Yu.V.; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Iskhakov, R. S.; Исхаков, Рауф Садыкович; Yurkin, G.Yu.; Юркин, Глеб Юрьевич; Moscow International Symposium on Magnetism(5 ; 2011 ; Aug. ; 21-25 ; Moscow)
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    The exchange interaction effects on magnetic properties of the nanostructured CoPt particles / S. V. Komogortsev [et al.] // J. Magn. Magn. Mater. - 2016. - Vol. 401. - P. 236-241, DOI 10.1016/j.jmmm.2015.10.041. - Cited References: 55. - The work has been partially supported by RFBR Grants 15-08-06673, 14-03-00411, 14-03-00129, 15-42-0417115 and it is partly performed in Siberian Federal University within the state contract of the Russian Federation Ministry of Education and Science for 2014-2016 (project number 1792) . - ISSN 0304-8853
   Перевод заглавия: Влияния обменного взаимодействия на магнитные свойства наноструктурированных частиц CoPt

РУБ Materials Science, Multidisciplinary + Physics, Condensed Matter
Рубрики:
CLUSTER BEAM DEPOSITION
   BULK MAGNETS
   NANOCRYSTALLINE FERROMAGNETS
   REMANENCE ENHANCEMENT
   THIN-FILMS
   COERCIVITY
   MICROSTRUCTURE
   NANOPARTICLES
   IRON
   SYSTEM
Аннотация: Various manifestations of the exchange interaction effects in magnetization curves of the CoPt nanostructured particles are demonstrated and discussed. The inter-grain exchange constant A in the sponge-like agglomerates of crystallites is estimated as A=(7±1) pJ/m from the approach magnetization to saturation curves that is in good agreement with A=(6.6±0.5) pJ/m obtained from Bloch T 3/2 law. The fractal dimensionality of the exchange coupled crystallite system in the porous media of the disordered CoPt alloy d=(2.60±0.18) was estimated from the approach magnetization to saturation curve. Coercive force decreases with temperature as Hc~T 3/2 which is assumed to be a consequence of the magnetic anisotropy energy reduction due to the thermal spin wave excitations in the investigated CoPt particles. © 2015 Elsevier B.V. All rightsreserved.
Демонстрируются и обсуждаются различные проявления эффектов обменного взаимодействия в кривых намагниченности наноструктуированных частиц CoPt. Межзеренная обменная константа А в агломератах губчатой структуры кристаллитов оценивается как /A/=(7±1) pJ/m из кривых приближения намагниченности к насыщению, это значение находится в хорошем согласии с /A/=(6.6±0.5) pJ/m, полученным из закона /T/. /2 Блоха. Размерность фрактала обменно-соединенных кристаллических систем в пористой среды неупорядоченного сплава CoPt /d/=(2.60±0.18) оценивалась из кривых приближения намагниченности к насыщению. Коэрцитивная сила уменьшается с температурой по закону /H_c /~/T/. /2 , который, как предполагается, есть следствие уменьшения энергии магнитной анизотропии из-за теплового возбуждения спиновых волн в изучаемых частицах CoPt.

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Держатели документа:
Kirensky Institute of Physics, SB RAS, Krasnoyarsk, Russian Federation
Nikolaev Institute of Inorganic Chemistry, SB RAS, Novosibirsk, Russian Federation
Novosibirsk State University, Novosibirsk, Russian Federation
Siberian Federal University, Krasnoyarsk, Russian Federation

Доп.точки доступа:
Komogortsev, S. V.; Комогорцев, Сергей Викторович; Iskhakov, R. S.; Исхаков, Рауф Садыкович; Zimin, A. A.; Зимин, А. А.; Filatov, E. Y.; Korenev, S. V.; Shubin, Yu. V.; Chizhik, N. A.; Yurkin, G. Yu.; Юркин, Глеб Юрьевич; Eremin, E. V.; Еремин, Евгений Владимирович
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