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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Deich L. I.
Заглавие : Far-infrared attenuation in glasses
Разночтения заглавия :авие SCOPUS: Far-infrared attenuation in glasses
Место публикации : Phys. Rev. B. - 1994. - Vol. 49, Is. 1. - P.109-113. - ISSN 0163-1829, DOI 10.1103/PhysRevB.49.109
Примечания : Cited References: 29
Предметные рубрики: VITREOUS SILICA
TEMPERATURE
MODEL
LOCALIZATION
ABSORPTION
SOLIDS
STATES
Аннотация: The influence of quasilocal vibrations on the far-infrared spectra of glasses is investigated under the supposition that the quasilocal vibrations are directly inactive in the attenuation. It is shown that taking into account phonon-quasilocal-vibration coupling and both medium- and short-range structure of the inhomogeneities of a photon-phonon coupling parameter can give rise to an attenuation curve similar to one observed for a-SiO2 and related materials.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Deich L. I.
Заглавие : Low-frequency raman-scattering in glasses
Разночтения заглавия :авие SCOPUS: Low-frequency Raman scattering in glasses
Место публикации : Phys. Rev. B. - 1995. - Vol. 51, Is. 13. - P.8131-8139. - ISSN 0163-1829, DOI 10.1103/PhysRevB.51.8131
Примечания : Cited References: 32
Предметные рубрики: AMORPHOUS SOLIDS
VITREOUS SILICA
THERMAL-CONDUCTIVITY
LIGHT-SCATTERING
TEMPERATURE
STATES
MODES
HEAT
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Belyaev B. A., Drokin N. A., Kumakhov M. A., Shabanov V. F.
Заглавие : Dielectric properties of liquid crystals in polycapillary matrices
Коллективы :
Место публикации : Phys. Solid State: MAIK NAUKA/INTERPERIODICA/SPRINGER, 2010. - Vol. 52, Is. 6. - P1315-1322. - ISSN 1063-7834, DOI 10.1134/S1063783410060314
Примечания : Cited References: 24. - This study was supported by the Council on Grants from the President of the Russian Federation (grant no. 3818.2008.3) and the Siberian Branch of the Russian Academy of Sciences (Integration Project no. 5) and performed within the framework of the State Contract (no. 02.740.11.0220).
Предметные рубрики: MOLECULAR-SIEVES
SILICA AEROGEL
POROUS-GLASS
MEMBRANES
NMR
8CB
Аннотация: This paper reports on the results of investigations into the dielectric properties of liquid crystals embedded in polycapillary matrices and describes a technique for their measurement. It has been revealed that the chemical structure of the rigid core and the length of mobile alkyl groups of liquid-crystal molecules of the alkylcyanobiphenyl group substantially affect the equilibrium configuration of the liquid-crystal director in capillaries. The reorientation of liquid-crystal molecules embedded in capillaries in the nematic phase under the influence of an external magnetic field has been investigated.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Babkina I. V., Volochaev M. N., Zhilova O. V., Kalinin Y. E., Kashirin M. A., Sitnikov A. V., Chehonadskih M. V., Yanchenko L. I.
Заглавие : Effect of Heat Treatment on the Stability of Nanosized (Co40Fe40B20)34(SiO2)66/ZnO/In2O3 Multilayers
Место публикации : Bull. Russ. Acad. Sci. Phys. - 2020. - Vol. 84, Is. 9. - P.1100-1103. - ISSN 10628738 (ISSN), DOI 10.3103/S1062873820090051
Примечания : Cited References: 11. - This work was supported by the RF Ministry of Science and Higher Education as part of State Task no. FZGM-2020-0007
Аннотация: An investigation is performed of the thermal stability and phase transformations of thin-film heterogeneous [(Co40Fe40B20)34(SiO2)66/ZnO/In2O3]85 multilayers obtained via ion beam sputtering. The system contains 85 layers, each consisting of a (Co40Fe40B20)34(SiO2)66 composite layer and ZnO and In2O3 semiconductor spacers. The sample structure in the initial state and after heat treatment is studied by means of X-ray diffraction. It is shown that the samples are stable at temperatures of up to 500°С. Zn2SiO4, InBO3, CoFe, and In2O3 phases form during annealing.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Bondarenko L. S., Kovel E. S., Kydralieva K. A., Dzhardimalieva G. I., Illes E., Tombacz E., Kicheeva A. G., Kudryasheva N. S.
Заглавие : Effects of modified magnetite nanoparticles on bacterial cells and enzyme reactions
Место публикации : Nanomaterials. - 2020. - Vol. 10, Is. 8. - Ст.1499. - P.1-20. - ISSN 20794991 (ISSN), DOI 10.3390/nano10081499
Примечания : Cited References: 83. - This research was funded by the Russian Foundation for Basic Research (#19-315-50048, #19-33-90149, and #18-29-19003)
Аннотация: Current paper presents biological effects of magnetite nanoparticles (MNPs). Analyzing effects of MNP’ characteristics (zeta-potential and hydrodynamic diameters) on bacteria and their enzyme reactions was the main focus. Photobacterium phosphoreum and bacterial enzymatic reactions were chosen as bioassays. Three types of MNPs were under study: bare Fe3O4, Fe3O4 modified with 3-aminopropyltriethoxysilane (Fe3O4/APTES), and humic acids (Fe3O4/HA). Effects of the MNPs were studied at a low concentration range (< 2 mg/L) and attributed to availability and oxidative activity of Fe3+, high negative surface charge, and low hydrodynamic diameter of Fe3O4/HA, as well as higher Fe3+ content in suspensions of Fe3O4/HA. Low-concentration suspensions of bare Fe3O4 provided inhibitory effects in both bacterial and enzymatic bioassays, whereas the MNPs with modified surface (Fe3O4/APTES and Fe3O4/HA) did not affect the enzymatic activity. Under oxidative stress (i.e., in the solutions of model oxidizer, 1,4-benzoquinone), MNPs did not reveal antioxidant activity, moreover, Fe3O4/HA demonstrated additional inhibitory activity. The study contributes to the deeper understanding of a role of humic substances and silica in biogeochemical cycling of iron. Bioluminescence assays, cellular and enzymatic, can serve as convenient tools to evaluate bioavailability of Fe3+ in natural dispersions of iron-containing nanoparticles, e.g., magnetite, ferrihydrite, etc.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Buktiyarova G.A., Shuvaeva М.А., Bayukov O. A., Yakushkin S.S., Martyanov O.N.
Заглавие : Facile synthesis of nanosized е-РегОз particles on the silica support
Место публикации : J. Nanopart. Res. - 2011. - Vol. 13, Is. 10. - Ст.5527-5534. - DOI 10.1007/sl 1051-011-0542-5
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Edelman I. S., Petrakovskaja E. A., Petrov D. A., Zharkov S. M., Khaibullin R. I., Nuzhdin V. I., Stepanov A. L.
Заглавие : FMR and TEM Studies of Co and Ni Nanoparticles Implanted in the SiO2 Matrix
Место публикации : Appl. Magn. Reson. - WIEN: SPRINGER WIEN, 2011. - Vol. 40, Is. 3. - С. 363-375. - MAY. - ISSN 0937-9347, DOI 10.1007/s00723-011-0218-4. - ISSN 1613-7507
Примечания : Cited Reference Count: 51. - Гранты: The work was supported in part by the Russian Foundation for Basic Research, grant no. 11-02-00972-a, Ministry of Education and Science of the Russian Federation, Federal Target Program "Scientific and scientific-pedagogical personnel of innovative Russia'', contract no. 02.740.11.0797, and State Program "Development of the Scientific Potential of the Higher Education School'', project no. 2.1.1/6038. S.M. Zharkov acknowledges the financial support of the Russian government contract no. 02.740.11.0568. The electron microscopy investigations were carried out at the Joint Center of the Siberian Federal University.Финансирующая организация: Russian Foundation for Basic Research [11-02-00972-a]; Ministry of Education and Science of the Russian Federation [02.740.11.0797]; State Program "Development of the Scientific Potential of the Higher Education School'' [2.1.1/6038]; Russian government [02.740.11.0568]
Предметные рубрики: FERROMAGNETIC-RESONANCE
MAGNETIC-PROPERTIES
THIN-FILMS
COBALT NANOPARTICLES
ION-IMPLANTATION
FINE PARTICLES
GRANULAR FILMS
ANISOTROPY
POLYIMIDES
RUTILE
Ключевые слова (''Своб.индексиров.''): energy dispersive x ray spectroscopy--face-centered cubic structure--fused silica plates--g factors--hexagonal close packing--high dose--high-dose implantation--implantation dose--implanted samples--line shape--magnetic parameters--matrix--metal nanoparticles--ni nanoparticles--nonsymmetric--out-of-plane--room temperature--spherical shape--subsurface layer--tem--temperature dependence--thin magnetic films--uniaxial magnetic anisotropy--cobalt--fused silica--magnetic anisotropy--nanoparticles--silica--silicon compounds--transmission electron microscopy--x ray spectroscopy--ferromagnetic resonance
Аннотация: Fused silica plates have been implanted with 40 keV Co+ or Ni+ ions to high doses in the range of (0.25-1.0) x 10(17) ions/cm(2), and magnetic properties of the implanted samples have been studied with ferromagnetic resonance (FMR) technique supplemented by transmission electron microscopy, electron diffraction and energy dispersive X-ray spectroscopy. The high-dose implantation with 3d-ions results in the formation of cobalt and nickel metal nanoparticles in the irradiated subsurface layer of the SiO2 matrix. Co and Ni nanocrystals with hexagonal close packing and face-centered cubic structures have a spherical shape and the sizes of 4-5 nm (for cobalt) and 6-14 nm (for nickel) in diameter. Room-temperature FMR signals from ensembles of Co and Ni nanoparticles implanted in the SiO2 matrix exhibit an out-of-plane uniaxial magnetic anisotropy that is typical for thin magnetic films. The dose and temperature dependences of FMR spectra have been analyzed using the Kittel formalism, and the effective magnetization and g-factor values have been obtained for Co- and Ni-implanted samples. Nonsymmetric FMR line shapes have been fitted by a sum of two symmetrical curves. The dependences of the magnetic parameters of each curve on the implantation dose and temperature are presented.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Kirik S. D., Parfenov V. A., Zharkov S. M.
Заглавие : Monitoring MCM-41 synthesis by X-ray mesostructure analysis
Место публикации : Micropor. Mesopor. Mater.: Elsevier Science, 2014. - Vol. 195. - P.21-30. - ISSN 1387-1811, DOI 10.1016/j.micromeso.2014.04.012. - ISSN 1873-3093
Примечания : Cited References: 70. - The investigation was made with financial support of the Program of Presidium RAS (Project 24.37), RF State contracts No 02.740.11.0629, RFBR Grants: 11-03-00610a and 11-03-12161-ofi, RSF 14-13-000025.
Предметные рубрики: ORDERED MESOPOROUS MATERIALS
ORDERED MESOPOROUS MATERIALS
IN-SITU
POWDER DIFFRACTION
SILICA/SURFACTANT COMPOSITES
ELECTRON-MICROSCOPY
MOLECULAR-SIEVES
STABLE MCM-41
SILICA
ADSORPTION
Ключевые слова (''Своб.индексиров.''): hydrothermal stability--mcm-41--mesostructure--tem--x-ray diffraction
Аннотация: The electron density maps calculated from X-ray diffraction patterns of the mesoporous silica material MCM-41 present averaged mesostructure images which in contrast to transmission electron microscopy (TEM) images are exceptionally repeating and represent the whole sample. It was shown that the averaged mesostructure parameters such as a unit cell parameter, a pore diameter, a wall width, a pore shape estimated from the X-ray powder diffraction data in combination with the continuous electron density function approach allow monitoring continuous set of the silica framework states at different stages of the material synthesis. The mentioned technique supplemented by N 2-adsorption measurements and transmission electron microscopy was applied for consideration of the MCM-41 hydrothermal stability. Attention has been given to the variations of the synthesis conditions affecting the hydrothermal stability, in particular the maintaining the basicity of the synthesis solution as well the substitution of the synthesis solution with water or a salt solution at hydrothermal treatment. The averaged pore shape was observed to be changed from cylindrical to hexagonal-prismatic form. The observed wall thickness was in the range from 0.75 to 1.25 nm. The competition of silica polycondensation and surface hydrolysis was shown to be responsible for the variety of framework geometry and hydrothermal stability. It has been established that the pore diameter increases generally due to the osmotic pressure of water. If the pores acquire the average prismatic hexagonal shape, the sample has low hydrothermal stability. Under the conditions favorable for the polycondensation the pores have averaged cylindrical shape and material demonstrates higher hydrothermal stability. Cooperative mechanism of mesostructure destruction under hydrothermal conditions was observed using TEM data and was discussed in connection with irregular polycondensation. © 2014 Elsevier Inc. All rights reserved.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Denisova E. A., Komogortsev S. V., Li O. A., Chekanova L. A., Patrusheva T. N., Eremin E. V.
Заглавие : Magnetic particles in mesoporous silica MCM-41
Коллективы : Euro-Asian Symposium "Trends in MAGnetism": Nanomagnetism
Место публикации : V Euro-Asian simposium "Trend in MAGnetism": Nanomagnetism: abstracts. - Vladivostok: FEFU, 2013. - С. 176. - ISBN 978-5-7444-3124-2
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Yakushkin S. S., Dubrovskiy A. A., Balaev A. D., Shaykhutdinov K. A., Bukhtiyarova G. A., Martyanov O. N.
Заглавие : Magnetic properties of few nanometers ɛ-Fe2O3 nanoparticles supported on the silica
Место публикации : J. Appl. Phys.: American Institute of Physics, 2012. - Vol. 111, Is. 4. - Ст.44312. - ISSN 0021-8979, DOI 10.1063/1.3686647
Примечания : Cited References: 27. - authors thank A. D. Balaev and N. V. Volkov for fruitful discussions and comments. This work was supported by Program of RAS No. 27.46.
Предметные рубрики: HIGH-TEMPERATURE
IRON
STABILIZATION
OXIDE
GEL
Аннотация: Magnetic properties of ɛ-Fe2O3nanoparticles supported on silica with the average size of few nanometers, narrow size distribution and no admixture of any other iron oxide polymorphs are investigated. The investigation of the temperature behavior of magnetization within the temperature range from 4.2 to 1000 K revealed the presence of several magnetic subsystems in the species under study. The temperatures’ behavior of the magnetic moment value indicates ferrimagnetic ordering in the ɛ-Fe2O3nanoparticles with a Curie temperature of about 800 K and points to the existence of a significant paramagnetic contribution becoming apparent at low temperatures. According to the electron spin resonance data, the particles possess superparamagnetic behavior at temperature higher ∼120 K. The model of the magnetic structure of monophase system of few nanometers ɛ-Fe2O3nanoparticles supported on silica is proposed.
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