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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Ivantsov R. D., Lin C. -R., Chen Y. -Z., Ivanova O. S., Altunin R. R., Knyazev Yu. V., Molokeev M. S., Zharkov S. M., Shestakov N. P., Sukhachev A. L., Edelman I. S.
Заглавие : Effect of surfactants on the structure, phase composition, and magnetic properties of FexSy nanoparticles synthesized by thermal decomposition
Место публикации : Nanobiotechnol. Rep. - 2022. - Vol. 17, Is. 3. - P.336-344. - ISSN 26351676 (ISSN), DOI 10.1134/S2635167622030089
Примечания : Cited References: 27. - This study was supported by the Russian Foundation for Basic Research with Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund of Science, the research project no. 19-42-240005: “Features of the Electronic Structure, Magnetic Properties, and Optical Excitations in Nanocrystals of Multifunctional Magnetic Chalcogenides Fe3S4 and FeSe” and the Russian Foundation for Basic Research and the Ministry of Science and Technology of Taiwan, joint projects nos. 19-52-52002 and 109-2112-M-153-003 and 108-2923-M-153-001-MY3The electron-microscopy study was carried out at the Laboratory of Electron Microscopy of the Center for Collective Use of the Siberian Federal University within the state assignment of the Ministry of Science and Higher Education of the Russian Federation (research code FSRZ-2020-0011). The magnetic measurements were carried out on a vibrating sample magnetometer at the Krasnoyarsk Regional Center for Collective Use, Krasnoyarsk Scientific Center, Siberian Branch, Russian Academy of Sciences
Аннотация: The effect of surfactants on the structure, morphology, and magnetic properties of FexSy iron-sulfide nanoparticles synthesized by thermal decomposition is studied. Oleylamine, hexadecylamine, and octadecylamine are used as surfactants. It is established by X-ray and electron-diffraction analysis combined with Mossbauer spectroscopy that, in samples 1 and 2 prepared using oleylamine and hexadecylamine, respectively, the Fe3S4 greigite phase dominates, with an inverse spinel structure isostructural to the iron oxide Fe3O4 magnetite with minor Fe9S11 impurities. Deviations in the distribution of iron cations over the tetrahedral and octahedral sites relative to the bulk greigite crystals are observed. The nanoparticles synthesized using octadecylamine (sample 3) are found to be multiphase with a greigite fraction of ~20%. In all three cases, as showed the results of transmission electron microscopy and Fourier transform infrared spectroscopy together with thermogravimetry analysis, the magnetic nanoparticles have an organic shell chemically bonded to their magnetic core, which prevents the agglomeration of the particles. This shell is much more massive in samples 2 and 3. The magnetization values for samples 1 and 2 are similar to those of greigite nanoparticles reported in publications, while the magnetization of sample 3 is several times lower, in accordance with the greigite fraction in it. The combination of fairly high magnetization with a massive organic shell allows one to consider hexadecylamine to be a promising surfactant for the synthesis of iron-sulfide nanoparticles protected from external impact and agglomeration.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Sutormin V. S., Krakhalev M. N., Prishchepa O. O., Gardymova A. P., Shabanov A. V., Kuz’menok N., Bezborodov V., Zyryanov V. Ya.
Заглавие : Electrically controlled anchoring transitions induced by ionic surfactants in liquid crystals
Коллективы : International Liquid Crystal Conference
Место публикации : Abstracts of 27th International Liquid Crystal Conference (ILCC 2018). - 2018. - Ст.2-B1-16
Примечания : Cited References: 3
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Belyaev B. A., Drokin N. A., Maslennikov A. N.
Заглавие : Impedance spectroscopy investigation of liquid crystals doped with ionic surfactants
Коллективы : Siberian Branch of the Russian Academy of Sciences [109]
Место публикации : Phys. Solid State: MAIK Nauka-Interperiodica / Springer, 2014. - Vol. 56, Is. 7. - P.1455-1462. - ISSN 1063-7834, DOI 10.1134/S106378341407004X. - ISSN 1090-6460
Примечания : Cited References: 20. - This study was supported by the Siberian Branch of the Russian Academy of Sciences (integration project no. 109).
Аннотация: The effect of a direct-current (dc) electric field on the electrophysical characteristics of nematic liquid crystals of the alkyl cyanobiphenyl series nCB (n = 6-8) and the multicomponent liquid-crystal mixture MB-1, which are doped with ionic surfactants, has been investigated using impedance spectroscopy. It has been found that the impedance spectra depend substantially on the dc bias voltage applied to the sample. The approximation of the measured spectra with specially developed equivalent circuits of the measuring cell with a sample has made it possible to determine the capacitance of the electric double layer and the electrical conductivity of the samples, as well as the mobility, concentration, and diffusion coefficient of the ions. It has been shown that a region of the space charge is formed in the frequency range f ˂ 100 Hz near the electrodes of the measuring cell with a liquid-crystal sample, which leads to an increase in the active (resistive) and reactive (capacitive) components of the impedance.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Krakhalev M. N., Prishchepa O. O., Zyryanov V. Ya.
Заглавие : Inverse mode of ion-surfactant method of director reorientation inside nematic droplets
Место публикации : Mol. Cryst. Liquid Cryst. - 2009. - Vol. 512, Is. 1. - P.1998-2003. - ISSN 1542-1406, DOI 10.1080/15421400903050814
Примечания : Cited Reference Count: 8. - Гранты: This work was partially supported by the grants Nos. NSh-3818.2008.3; 02.740.11.0220, and No. 08-03-01007 of RFBR, and Nos. 27.1; 110; 144 of SB RAS. M. Krakhalev acknowledges the financial support from K. I. Zamaraev MBN Foundation. O. Prishchepa acknowledges the financial support from Russian Science Support Foundation.Финансирующая организация: RFBR [NSh-3818.2008.3, 02.740.11.0220, 08-03-01007]; SB RAS [27.1; 110; 144]; Zamaraev MBN Foundation; Russian Science Support Foundation
Ключевые слова (''Своб.индексиров.''): electrically commanded surfaces--ion surfactant--nematic--polymer dispersed liquid crystals--surface anchoring--electrically commanded surfaces--ion surfactant--nematic--polymer dispersed liquid crystals--surface anchoring--applied voltages--crossed polarizers--director fields--director reorientation--droplet structure--electrically commanded surfaces--high concentration--homeotropic--initial state--ionic modification--liquid-crystal droplets--nematic droplets--nematic polymer--surface-active cations--surface-anchoring--trimethyl--ammonium compounds--cationic surfactants--crystals--drop formation--dyes--ionization of liquids--ions--liquid crystal displays--liquid crystals--liquids--nematic liquid crystals
Аннотация: Inverse mode of a novel electrooptical effect caused by the ionic modification of boundary conditions has been studied for liquid crystal droplets. We have considered the droplets of nematic 5CB doped with cationic surfactant cetyl-trimethyl-ammonium-bromide and dispersed in polyvinyl alcohol. In the initial state the surface anchoring was normal on the whole interface due to the high concentration of homeotropic surfactant. Applied voltage results in the purification of a section of the interface from the surface-active cations thereby restoring here a tangential anchoring and stimulating the significant transformation of droplet structure. At that three different types of director field distribution can be realized within the same droplet. The proper textures of the droplet both in the crossed polarizers and without analyzer are considered.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Krakhalev M. N., Sutormin V. S., Prishchepa O. O., Gardymova A. P., Zyryanov V. Ya.
Заглавие : Ionic surfactants for the development of new method to control liquid crystals
Коллективы : International conference on colloid chemistry and physicochemical mechanics, Российская академия наук, Московский государственный университет им. М.В. Ломоносова
Место публикации : IV International conference on colloid chemistry and physicochemical mechanics. (CCPCM-13): book of abstracts. - 2013. - P.332-333
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Zyryanov V. Ya., Sutormin V. S., Krakhalev M. N., Gardymova A. P., Prishchepa O. O., Shabanov A. V.
Заглавие : Liquid crystal materials with ionic-surfactant operation
Место публикации : Bull. Russ. Acad. Sci. Phys.: Allerton Press, 2017. - Vol. 81, Is. 5. - P.594-597. - ISSN 10628738 (ISSN), DOI 10.3103/S1062873817050288
Примечания : Cited References: 15
Ключевые слова (''Своб.индексиров.''): crystalline materials--liquid crystals--surface active agents--b-y ions--ionic surfactants--liquid crystal materials--liquid crystalline materials--new approaches--surface-active compounds--surface-anchoring--liquids
Аннотация: A conceptually new approach for developing methods of control of liquid crystals is discussed. The approach is based on modifying surface anchoring. A brief review of the authors’ research on developing ionic-surfactant control of liquid crystalline materials is described. This approach is based on the effect of electrically induced modification of the boundary conditions by ions of surface-active compounds. © 2017, Allerton Press, Inc.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Krakhalev M. N., Sutormin V. S., Prishchepa O. O., Gardymova A. P., Shabanov A. V., Wei Lee, Zyryanov V. Ya.
Заглавие : Liquid crystals doped with ionic surfactants for electrically induced anchoring transitions
Место публикации : Unconventional liquid crystals and their applications/ ed.: Wei Lee, S. Kumar. - Berlin et al.: De Gruyter, 2021. - Chap. 7. - P.279-330. - DOI 10.1515/9783110584370-007
Примечания : Cited References: P. 327-330
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Ivantsov R. D., Chun-Rong Lin, Knyazev Yu. V., Ying Zhen Chen, Zharkov S. M., Lin E. S., Chen B.Y., Yaw-Teng Tseng, Edelman I. S.
Заглавие : Morphology and magnetic properties of iron sulphides nanoparticles synthesized by the thermal decomposition method with different surfactants
Коллективы : "Новое в магнетизме и магнитных материалах", международная конференция, Научный совет по физике конденсированных сред РАН, МИРЭА - Российский технологический университет, Московский государственный университет им. М.В. Ломоносова, Магнитное общество России
Место публикации : Новое в магнетизме и магнитных материалах: сборник трудов XXIV международной конференции/ прогр. ком.: Р. С. Исхаков, С. Г. Овчинников [и др.]. - 2021. - Секция 11: Магнитные наноструктуры. - Ст.11-25-28
Примечания : Библиогр.: 4
Аннотация: Morphology, magnetic, and structural properties were investigated of the iron sulphides (FexSy) nanoparticles fabricated by the thermal decomposition method using oleylamine, 1-hexadecylamine and octadecylamine surfactants. The presence of surfactant layer is confirmed by FT-IR spectroscopy and thermo-gravimetric analysis. The structural analysis and Mцssbauer spectroscopy of synthesized nanoparticles showed in main Fe3S4 phase with inclusions of Fe9S11 in cases of OLA and HDA surfactants and significant admixture of FeS2 and even Fe2O3 in case of ODA surfactant. Deviations of iron ions distribution among crystal positions from that in bulk pure greigite and the pronounce changes in the magnetic circular dichroism (MCD) spectra are explained with the influence of surfactants on the particles formation process as well with the role of the boundary between magnetic core and organic shell.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Ivantsov R. D., Lin C. -R., Ivanova O. S., Altunin R. R., Knyazev Yu. V., Molokeev M. S., Zharkov S. M., Chen Y. -Z., Lin E. -S., Chen B. -Y., Shestakov N. P., Edelman I. S.
Заглавие : Mossbauer and MCD spectroscopy of the Fe3S4 nanoparticles synthesized by the thermal decomposition method with two different surfactants
Место публикации : Curr. Appl. Phys. - 2021. - Vol. 25. - P.55-61. - ISSN 15671739 (ISSN), DOI 10.1016/j.cap.2021.02.013
Примечания : Cited References: 30. - The reported study was funded by Joint Research Project of Russian Foundation for Basic Research № 19-52-52002 and Ministry of Science and Technology, Taiwan MOST № 108-2923-M-153-001-MY3 and № 106-2112-M-153-001-MY3 , and by Russian Foundation for Basic Research with Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund of Science , the research project number 19-42-240005 : “Features of the electronic structure, magnetic properties and optical excitations in nanocrystals of the multifunctional magnetic chalcogenides Fe3S4 and FeSe”. The electron microscopy and electron diffraction investigations were conducted in the SFU Joint Scientific Center supported by the State assignment (#FSRZ-2020-0011) of the Ministry of Science and Higher Education of the Russian Federation. The thermal-gravity measurements were carried out with the differential Scanning Calorimeter DSC 204 F-1 Phoenix (NETZSCH) in the Krasnoyarsk Regional Center of Research Equipment of Federal Research Center «Krasnoyarsk Science Center SB RAS»
Аннотация: Greigite (Fe3S4) nanoparticles (NPs) were fabricated by the thermal decomposition method using two different surfactants: oleylamine (OLA) and 1-hexadecylamine (HDA). In both cases, the synthesized NPs were characterized as the Fe3S4 nanocrystals with minor inclusions of Fe9S11 phase. FT-IR spectroscopy and thermo-gravimetric analysis allow concluding about OLA or HDA shells covering magnetic core of NPs. Mossbauer spectra has revealed deviations of iron ions distribution among crystal positions from that presented in literature for pure greigite. In accordance with these deviations, the pronounce changes are observed in the magnetic circular dichroism (MCD) spectra which manifest themselves as the spectrum shift to higher energies of electromagnetic waves and redistribution of the MCD maximum intensities. These effects are associated with a change in the density of electronic states in the samples due to the redistribution of iron ions between octahedral and tetrahedral positions in nanocrystals under the influence of surfactants.
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Кузьменок Н. М., Михалёнок С. Г., Орёл А. С., Безбородов В. С., Крахалев, Михаил Николаевич, Сутормин, Виталий Сергеевич, Прищепа, Оксана Олеговна, Зырянов, Виктор Яковлевич
Заглавие : Синтез и исследование анизотропных солей аммония для создания жидкокристаллических материалов и устройств с варьируемым поверхностным сцеплением
Место публикации : Жидк. кристаллы и их практич. использ. - 2018. - Т. 18, № 4. - С. 27-39. - ISSN 1991-3966, DOI 10.18083/LCAppl.2018.4.27; Liq. Cryst. Appl.
Примечания : Библиогр.: 13. - Работа выполнена частично при поддержке БРФФИ (грант № X16P-110) и РФФИ (грант № 16-53-00073).
Ключевые слова (''Своб.индексиров.''): жидкокристаллические материалы--ионные сурфактанты--амины--кватернизация--электрооптические устройства--дисплеи--liquid crystals--ionic surfactants--amines--quaternization--electro-optical devices--displays
Аннотация: Получены разнообразные анизотропные четвертичные соли аммония, характеризующиеся специфическим взаимодействием с границей раздела и способные к формированию различных ориентационных структур жидкокристаллического слоя. Показано, что данные соли перспективны для создания более совершенных ЖК-композиций с поверхностным сцеплением, обусловленным ионными сурфактантами, а результаты исследований представляют несомненный интерес для разработчиков новых жидкокристаллических материалов и электрооптических устройств на их основе.Various anisotropic quaternary ammonium salts characterized by a specific interaction with the interface and capable to form various orientational structures of liquid crystal layer, have been prepared. It has been shown that these salts are promising materials for creation of advanced LC compositions with surface anchoring caused by ionic surfactants. The obtained results are of undoubted interest for the developers of new liquid crystal materials and electro-optical devices based on them.
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