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    Polymer Films of Poly-3-hydroxybutyrate Synthesized byCupriavidus necatorfrom Different Carbon Sources / E. Shishatskaya, I. Nemtsev, A. Lukyanenko [et al.] // J. Polym. Environ. - 2021. - Vol. 29. - P. 837-850, DOI 10.1007/s10924-020-01924-3. - Cited References: 54. - The reported study was funded by RFBR and KKRF Grant No. 19-43-240012 "Biological and physical principles of production of new generation biomaterials". The work was carried out as part of the State Assignment of the Ministry of Education and Science of the Russian Federation No. FSRZ-2020-0006. The authors would like to express their special thanks to Krasnoyarsk Regional Center of Research Equipment of Federal Research Center "Krasnoyarsk Science Center SB RAS" for providing equipment to ensure the accomplishment of this project . - ISSN 1566-2543. - ISSN 1572-8919
   Перевод заглавия: Полимерные пленки Поли-3-гидроксибутирата, синтезированные некатором Cupriavidus из различных источников углерода

РУБ Engineering, Environmental + Polymer Science
Рубрики:
CHEMOMECHANICAL PROPERTIES
RALSTONIA-EUTROPHA
SURFACE-ROUGHNESS
Кл.слова (ненормированные):
Degradable P(3HB) -- Various carbon substrates -- Films -- Structure -- Properties -- NIH 3T3 fibroblasts
Аннотация: Films were prepared from 2% solutions of biodegradable poly-3-hydroxybutyrate [P(3HB)] and investigated. The polymer was synthesized by the Cupriavidus necator B-10646 bacterium cultivated using various carbon sources (glucose and glycerol of different degrees of purity, containing 0.3 to 17.93% impurities). Glycerol as the substrate influenced molecular-weight properties and crystallinity of the polymer without affecting its temperature characteristics. The P(3HB) specimens synthesized from glycerol had reduced Mw (300–400 kDa) and degree of crystallinity (50–55%) compared to the specimens synthesized from glucose (860 kDa and 76%, respectively). The low-crystallinity P(3HB) specimens, regardless of the degree of purity of glycerol, produced a beneficial effect on the properties of polymer films, which had a better developed folded surface and increased hydrophilicity. The values of the highest roughness (Ra) of the films synthesized from glycerol were 1.8 to 4.0 times lower and the water angles 1.4–1.6 times smaller compared to the films synthesized from glucose (71.75 nm and 87.4°, respectively). Those films performed better as cell scaffolds: the number of viable NIH fibroblasts was 1.7–1.9 times higher than on polystyrene (control) or films of P(3HB) synthesized from glucose.

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Держатели документа:
Siberian Fed Univ, 79 Svobodnyi Av, Krasnoyarsk 660041, Russia.
RAS, Krasnoyarsk Sci Ctr SB, Fed Res Ctr, Inst Biophys, Krasnoyarsk, Russia.
RAS, Krasnoyarsk Sci Ctr SB, Fed Res Ctr, LV Kirenskii Inst Phys, Krasnoyarsk, Russia.

Доп.точки доступа:
Shishatskaya, Ekaterina; Nemtsev, I. V.; Немцев, Иван Васильевич; Lukyanenko, A. V.; Лукьяненко, Анна Витальевна; Vasiliev, A. D.; Васильев, Александр Дмитриевич; Kiselev, Evgeniy; Sukovatyi, Aleksey; Volova, Tatiana; RFBRRussian Foundation for Basic Research (RFBR); KKRF [19-43-240012]; Ministry of Education and Science of the Russian FederationMinistry of Education and Science, Russian Federation [FSRZ-2020-0006]
}
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The effect of the initial microstructure of the X70 low-carbon microalloyed steel on the heat affected zone formation and the mechanical properties of laser welded joints / A. I. Gordienko, L. S. Derevyagina, A. G. Malikov [et al.] // Mater. Sci. Eng. A. - 2020. - Vol. 797. - Ст. 140075, DOI 10.1016/j.msea.2020.140075. - Cited References: 32. - Microstructural studies and mechanical tests of laser welds were performed within the frame of the Fundamental Research Program of the State Academies of Sciences for 2013?2020, line of research III.23.1.1. Part of the research related to the selection of optimal laser welding parameters for low carbon steels was carried out within Basic State Project No. AAAA-A17-117030610122-6. TEM studies were carried out in Center of Federal Research Center of Kirensky Institute of Physics SB RAS. The authors are grateful to I.P. Mishin. for assistance in cross-helical rolling of the steel . - ISSN 0921-5093
Кл.слова (ненормированные):
Low-carbon steel -- Cross-helical rolling -- Laser welding -- Heat affected zone -- Bainite -- Microhardness
Аннотация: In this paper, the heat affected zone (HAZ) of laser welded joints of the X70 steel were studied by the transmission electron microscopy method. The effect of the initial microstructure (coarse-grained hot-rolled and fine-grained after cross-helical rolling) on the HAZ formation and the mechanical characteristics of the welded joints were shown. It was found that the microstructure in the inter-critical HAZ of the steel after cross-helical rolling was more dispersed, homogeneous, and uniform compared to that of the coarse-grained hot-rolled one due to the initial fine-grained ferrite-bainitic-pearlite microstructure and the absence of pronounced ferrite-pearlite banding in the base metal. The character of the microhardness value distribution in the HAZ of the steel after cross-helical rolling was smooth with the gradual decrease from 370 down to 185 HV as shifted towards the base metal. In the HAZ of the coarse-grained hot-rolled steel, the heterogeneous microhardness value (up to 640–670 НV) distribution was revealed. The reason was the upper degenerate bainite microstructure with high residual stresses, characterized by laths up to 2.0–2.5 μm long and a high martensitic-austenitic constituent fraction (10–16%) of a slender shape along the boundaries of bainite laths. The conclusion was drawn that one of the ways to reduce the brittleness of the laser welded joints could be using the initially fine-grained steels possessing the homogeneous (mainly bainitic) microstructure.

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Держатели документа:
Institute of Strength Physics and Materials Science of Siberian Branch Russian Academy of Sciences, 2/4, Pr. Akademicheskii, Tomsk, 634055, Russian Federation
Khristianovich Institute of Theoretical and Applied Mechanics of the Siberian Branch of the Russian Academy of Sciences, 4/1, Institutskaya str., Novosibirsk, 630090, Russian Federation
Kirensky Institute of Physics of the Siberian Branch of the Russian Academy of Sciences (SB RAS), Akademgorodok 50, bld. 38, Krasnoyarsk, 660036, Russian Federation
Reshetnev Siberian State University of Science and Technology, 31, Pr. Krasnoyarsk worker, Krasnoyarsk, 660037, Russian Federation

Доп.точки доступа:
Gordienko, A. I.; Derevyagina, L. S.; Malikov, A. G.; Orishich, A. M.; Surikova, N. S.; Volochaev, M. N.; Волочаев, Михаил Николаевич
}
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    Simulation of fullerene formation in a carbon-helium plasma / P. V. Novikov, I. V. Osipova, G. N. Churilov, A. I. Dudnik // Fuller. Nanotub. Carbon Nanostruct. - 2021. - Vol. 29, Is. 5. - P. 337-342, DOI 10.1080/1536383X.2020.1842738. - Cited References: 22 . - ISSN 1536-383X
   Перевод заглавия: Моделирование образования фуллерена в углеродно-гелиевой плазме
Кл.слова (ненормированные):
Fullerene formation -- kinetic model -- carbon clusters -- Kinetic modeling -- Fullerenes
Аннотация: A kinetic model of fullerene formation in the carbon-helium plasma of an arc discharge was proposed. In the model, in addition to the coagulation of carbon clusters, the cluster isomerization and their cooling with a buffer gas were taken into account. The simulation results of the fullerene formation are in qualitatively agreement with the experimental data, i.e., the fraction of higher fullerenes increases at high pressures in the fullerene mixture.

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Держатели документа:
Krasnoyarsk Institute of Railway Transport, Krasnoyarsk, Russian Federation
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, Russian Federation
Siberian Federal University, Krasnoyarsk, Russian Federation

Доп.точки доступа:
Novikov, P. V.; Osipova, I. V.; Осипова, Ирина Владимировна; Churilov, G. N.; Чурилов, Григорий Николаевич; Dudnik, A. I.; Дудник, Александр Иванович
}
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Spin state crossover in Co3BO5 / N. V. Kazak, M. S. Platunov, Y. V. Knyazev [et al.] // Phys. Rev. B. - 2021. - Vol. 103, Is. 9. - Ст. 094445, DOI 10.1103/PhysRevB.103.094445. - Cited References: 71. - We acknowledge many inspirational discussions on the topic of this paper with the late Natalia Ivanova and Leonard Bezmaternykh. The authors acknowledge A. Ney for allowing us to use the XANES spectrum of film. We are grateful to the Russian Foundation for Basic Research (Project No. 20-02-00559) and President Council on Grants (Project No. МК-2339.2020.2) for supporting this paper. This paper was carried out within the state assignment of the Russian Ministry of Science and High Education via program “Quantum”' (No. AAAA-A18-118020190095-4). We also acknowledge support by Russian Ministry of Education and Science via Contract No. 02.A03.21.0006. We acknowledge financial support from the Spanish Ministry of Economy, Industry and Competitiveness (MINECO, Grant No. MAT2017-83468-R) and from the regional Government of Aragon (E12-20R RASMIA project) . - ISSN 2469-9950
Кл.слова (ненормированные):
Carbon dioxide -- Crystal structure -- Dichroism -- Energy gap -- Hydraulic structures -- Ions -- Iron compounds -- Magnetic moments -- Magnetic susceptibility -- Single crystals -- DC magnetic susceptibility -- Effective magnetic moments -- Electronic configuration -- Generalized gradient approximations -- Magnetic sublattices -- Octahedral environment -- Paramagnetic susceptibility -- X-ray magnetic circular dichroism -- Cobalt
Аннотация: We have investigated the spin and oxidation states of Co in Co3BO5 using x-ray magnetic circular dichroism (XMCD) and dc magnetic susceptibility measurements. At low temperatures, XMCD experiments have been performed at the Co K-edge in Co3BO5 and Co2FeBO5 single crystals in the fully ferrimagnetically ordered phase. The Co (K-edge) XMCD signal is found to be related to the Co2+ magnetic sublattices in both compounds, providing strong experimental support for the low-spin (LS) Co3+ scenario. The paramagnetic susceptibility is highly anisotropic. An estimation of the effective magnetic moment in the temperature range 100–250 K correlates well with two Co2+ ions in the high-spin (HS) state and some orbital contribution, while Co3+ remains in the LS state. The crystal structure of the Co3BO5 single crystal has been solved in detail at the T range 296–703 K. The unit cell parameters and volume show anomalies at 500 and 700 K. The octahedral environment of the Co4 site strongly changes with heating. The generalized gradient approximation with Hubbard U correction calculations have revealed that, at low-temperatures, the system is insulating with a band gap of 1.4 eV, and the Co2+ ions are in the HS state, while Co3+ are in the LS state. At high temperatures (T > 700 K), the charge ordering disappears, and the system becomes metallic with all Co ions in 3d7 electronic configuration and HS state.

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Держатели документа:
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
M.N. Miheev Institute of Metal Physics UB RAS, Ekaterinburg, 620137, Russian Federation
Ural Federal University, Ekaterinburg, 620002, Russian Federation
Instituto de Nanociencia y Materiales de Aragon (INMA), CSIC-Universidad de Zaragoza, Departamento de Fisica de la Materia Condensada, Zaragoza, 50009, Spain
Servicio de Medidas Fisicas, Universidad de Zaragoza, Zaragoza, 50009, Spain
Institute of Chemistry and Chemical Technology, Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
P.N. Lebedev Physical Institute of RAS, Moscow, 119991, Russian Federation
ESRF-The European Synchrotron, 71 Avenue des Martyrs CS40220, Grenoble Cedex 9, F-38043, France

Доп.точки доступа:
Kazak, N. V.; Казак, Наталья Валерьевна; Platunov, M. S.; Платунов, Михаил Сергеевич; Knyazev, Yu. V.; Князев, Юрий Владимирович; Molokeev, M. S.; Молокеев, Максим Сергеевич; Gorev, M. V.; Горев, Михаил Васильевич; Ovchinnikov, S. G.; Овчинников, Сергей Геннадьевич; Pchelkina, Z. V.; Gapontsev, V. V.; Streltsov, S. V.; Bartolome, J.; Arauzo, A.; Yumashev, V. V.; Gavrilkin, S. Y.; Wilhelm, F.; Rogalev, A.
}
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Co/multi-walled carbon nanotubes/polyethylene composites for microwave absorption: Tuning the effectiveness of electromagnetic shielding by varying the components ratio / M. A. Kazakova, N. V. Semikolenova, E. Y. Korovin [et al.] // Compos. Sci. Technol. - 2021. - Vol. 207. - Ст. 108731, DOI 10.1016/j.compscitech.2021.108731. - Cited References: 45. - This work was supported by the Ministry of Science and Higher Education of the Russian Federation within the state assignment for Boreskov Institute of Catalysis (project # АААА-А21-121011390054-1) . - ISSN 0266-3538
Кл.слова (ненормированные):
Polymer composites -- Multi-walled carbon nanotubes -- Co nanoparticles -- Hybrid structures -- Electromagnetic interference shielding
Аннотация: We present novel polyethylene (PE) composites for electromagnetic interference (EMI) shielding application. They are based on cobalt modified multi-walled carbon nanotubes (MWCNTs) produced via in situ polymerization of ethylene, with the Ti-Ziegler–Natta catalyst preliminarily immobilized on Co/MWCNT hybrids. The electromagnetic properties of the composites were tuned by varying the filler loading and Co:MWCNT ratio. The microstructure of the composites and electromagnetic absorption process were carefully characterized by transmission and scanning electron microscopy, X-ray diffraction, vibrating sample magnetometry, ferromagnetic resonance and vector network analysis. The electromagnetic wave absorbing properties of the nanocomposite were investigated in the 10 MHz−18 GHz frequency range revealing that the EMI absorption properties can be tuned by varying the Co:MWCNT weight ratio in the filler. Interestingly, the Co/MWCNT-PE composite with a total filler and Co loading of only 12 and 1.7 wt%, respectively, showed extremely high reflection loss (RL) of −55 dB. More importantly, an effective bandwidth of 12.8–17.8 GHz (RL below −10 dB) was achieved for a matching thickness of only 1.5 mm. The specific RL value (RL/filler loading) of the composite was superior in comparison with the previously reported nanostructured carbon materials. The highly effective absorbing properties of Co/MWCNT-PE composites are explained primarily by the unprecedented uniform filler distribution in the polyethylene as well as by the synergistic effect of MWCNTs and Co nanoparticles. This approach thus offered an effective strategy to design cost-effective, lightweight and flexible EMI shielding materials with tunable dielectric and magnetic performance.

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Держатели документа:
Boreskov Institute of Catalysis, SB RAS, Lavrentieva 5, Novosibirsk, 630090, Russian Federation
National Research Tomsk State University, Lenin Ave. 36, Tomsk, 634050, Russian Federation
Kirensky Institute of Physics, SB RAS, Akademgorodok St. 50, Krasnoyarsk, 660036, Russian Federation
TOTAL Research and Technology Feluy (TRTF), Zone Industrielle C, Feluy, 7181, Belgium
Soft Matter Science and Engineering (SIMM), UMR CNRS 7615, ESPCI Paris, Universite PSL, Sorbonne Universite, Paris, 75005, France

Доп.точки доступа:
Kazakova, M. A.; Semikolenova, N. V.; Korovin, E. Y.; Zhuravlev, V. A.; Selyutin, A. G.; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Moseenkov, S. I.; Andreev, A. S.; Lapina, O. B.; Suslyaev, V. I.; Matsko, M. A.; Zakharov, V. A.; Lacaillerie, J. -B.D.D.
}
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Electrical and mechanical properties of the high-permittivity ultra-high-molecular-weight polyethylene-based composite modified by carbon nanotubes / I. A. Markevich, G. E. Selyutin, N. A. Drokin, A. G. Selyutin // Tech. Phys. - 2020. - Vol. 65, Is. 7. - P. 1106-1113, DOI 10.1134/S1063784220070129. - Cited References: 39 . - ISSN 1063-7842
Аннотация: A composite based on ultra-high-molecular-weight polyethylene (UHMWPE) added with 1 wt % of multiwalled carbon nanotubes (MWCNTs) with a high permittivity (ε = 4.5) and a low dielectric loss (tanδ = 10–2) in the frequency range from 100 Hz to 100 MHz has been synthesized, and its main mechanical characteristics have been studied. The material has a low (22 MPa) breaking strength, a high (700%) tensile elongation, and an abrasion resistance higher than that of pure UHMWPE by 37%. It is shown using the X-ray diffraction and differential scanning calorimetry data that the changes in the mechanical properties of the composite are related to the changes in the polymer matrix structure under the action of the high-intensity ultrasonic radiation used for embedding MWCNTs into the polymer.

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Публикация на русском языке Электрофизические и механические свойства композита с повышенной диэлектрической проницаемостью на основе сверхвысокомолекулярного полиэтилена, модифицированного углеродными нанотрубками [Текст] / И. А. Маркевич, Г. Е. Селютин, Н. А. Дрокин, А. Г. Селютин // Журн. техн. физ. - 2020. - Т. 90 Вып. 7. - С. 1151-1158

Держатели документа:
Institute of Chemistry and Chemical Technology, Krasnoyarsk Scientific Center, Siberian Branch, Russian Academy of Sciences, Krasnoyarsk, 660036, Russian Federation
Kirensky Institute of Physics, Krasnoyarsk Scientific Center, Siberian Branch, Russian Academy of Sciences, Krasnoyarsk, 660036, Russian Federation
Boreskov Institute of Catalysis, Siberian Branch, Russian Academy of Sciences, Novosibirsk, 630090, Russian Federation

Доп.точки доступа:
Markevich, I. A.; Selyutin, G. E.; Drokin, N. A.; Дрокин, Николай Александрович; Selyutin, A. G.
}
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Influence of ultrasonic treatment on mechanical and electro-physical characteristics of UHMWPE/MWCNT composites / I. A. Markevich, G. Y. Selyutin, V. A. Poluboyarov [et al.] // Mater. Today: Proc. - 2020. - Vol. 25. - P. 532-535, DOI 10.1016/j.matpr.2020.02.746. - Cited References: 20 . - ISSN 2214-7853
Рубрики:
NANOCOMPOSITE
Кл.слова (ненормированные):
Multi-walled carbon nanotubes -- Ultra-high molecular weight polyethylene -- Composite -- Ultrasonic treatment -- Polymer structure
Аннотация: The influence of ultrasonic treatment on the strength and dielectric properties of composites based on ultra-high molecular weight polyethylene (UHMWPE) and multi-walled carbon nanotubes (MWCNT) is studied. It is revealed that the ultrasonic treatment of composite melt at 130 °C results in the uniform distribution of nanotubes in the UHMWPE matrix, an increase in the degree of composite crystallinity by 10%, an increase in abrasion resistance by 37%, an increase in elongation at rupture by a factor of 2. The change in the physical and mechanical properties of the composite is caused by the change in the polymer matrix structure, taking place as a result of ultrasonic action, and does not depend on the presence of nanotubes in the polymer matrix.

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Держатели документа:
RAS, SB, Inst Chem & Chem Technol, Res Ctr,Krasnoyarsk Sci Ctr, 50,Bil 24, Krasnoyarsk 660036, Russia.
RAS, SB, Inst Solid State Chem & Mechanochem, Kutateladze,18, Novosibirsk 630128, Russia.
RAS, Siberian Branch, Kirensky Inst Phys, 50,Bil 38, Krasnoyarsk 660036, Russia.
RAS, SB, Boreskov Inst Catalysis, Fed Res Ctr, Novosibirsk 630090, Russia.

Доп.точки доступа:
Markevich, I. A.; Selyutin, G. Ye.; Poluboyarov, V. A.; Drokin, N. A.; Дрокин, Николай Александрович; Selyutin, A. G.; Matzko, M. A.; All-Russian Conference (with International Participation) "Hot Topics of Solid State Chemistry : From New Ideas to New Materials"(3rd ; Oct. 01-05, 2019 ; Novosibirsk, Russia)
}
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Electrophysical properties of composites based on polyethylene modified with multi-walled carbon nanotubes with high content of Fe-Co-catalyst / S. I. Moseenkov, V. L. Kuznetsov, A. V. Zavorin [et al.] // Russ. J. Appl. Chem. - 2020. - Vol. 93, Is. 4. - P. 586-594, DOI 10.1134/S107042722004014X. - Cited References: 30. - This work was financially supported by the Russian Science Foundation, project no. 17-73-20293. . - ISSN 1070-4272. - ISSN 1608-3296

РУБ Chemistry, Applied
Рубрики:
POLYMER COMPOSITES
   NANOPARTICLES
   ACTIVATION
   NANOCOMPOSITES
Кл.слова (ненормированные):
multi-walled carbon nanotubes -- ferromagnetic catalyst particles -- polymer composites -- mechanical mixing in the melt -- gigahertz range -- electromagnetic absorption
Аннотация: The effect of the residual catalyst for the synthesis of multi-walled carbon nanotubes (MWCNTs) on the electrophysical properties of MWCNT-polyethylene composites produced by melt mechanical mixing was studied. The residual catalyst content was varied by changing the MWCNTs synthesis time. The nanotubes used in the work were characterized using transmission and scanning electron microscopy, atomic emission analysis, X-ray phase analysis, and magnetic permeability measurements. The structure of the synthesized composites was studied using optical and scanning electron microscopy. The dependences of the specific magnetization on the applied magnetic field, bulk electrical conductivity on the volumetric content of the filler in the composite, and the frequency dependences of the reflection, transmission, and absorption of electromagnetic radiation in the range 0.01-18 GHz were obtained. It was established that the obtained composites are characterized by a uniform distribution of nanotubes in the polymer matrix, and the dependence of the bulk electrical conductivity on the content of MWCNTs in the composite has a percolation character. Variation in the synthesis time of nanotubes allows producing MWCNTs with a high content of ferromagnetic particles, which are an alloy close in stoichiometry to the composition of the active component of the catalyst. It was shown that the use of composites modified with MWCNTs with a high content of residual catalyst is more effective for absorbing electromagnetic radiation due to an increase in their magnetic losses.

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Публикация на русском языке Электрофизические свойства композитов на основе полиэтилена, модифицированного многослойными углеродными нанотрубками с высоким содержанием Fe-Co-катализатора [Текст] / С. И. Мосеенков, В. Л. Кузнецов, А. В. Заворин [и др.] // Журн. прикл. химии. - 2020. - Т. 93 № 4. - С. 581-590

Держатели документа:
Russian Acad Sci, Siberian Branch, Boreskov Inst Catalysis, Novosibirsk 630090, Russia.
Novosibirsk Natl Res State Univ, Novosibirsk 630090, Russia.
Natl Res Tomsk State Univ, Tomsk 634050, Russia.
Russian Acad Sci, Kirensky Inst Phys, Siberian Branch, Krasnoyarsk 660036, Russia.

Доп.точки доступа:
Moseenkov, S. I.; Kuznetsov, V. L.; Zavorin, A. V.; Golubtsov, G. V.; Korovin, E. Yu.; Suslyaev, V. I.; Ishchenko, A. V.; Serkova, A. N.; Sergeenko, D. I.; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Russian Science FoundationRussian Science Foundation (RSF) [17-73-20293]
}
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Nonequilibrium carbon black suspensions used in synthesis of polymer composite material / O. P. Stebeleva, L. V. Kashkina, E. A. Petrakovskaya [et al.] // Journal of Physics: Conference Series. - 2020. - Vol. 1515, Is. 2. - Ст. 022003, DOI 10.1088/1742-6596/1515/2/022003. - Cited References: 9
Кл.слова (ненормированные):
Carbon black -- Carbon nanotubes -- Composite coatings -- Embedded systems -- Fillers -- Foams -- Polymer matrix composites -- Polyurethanes
Аннотация: Nowadays polymer matrix-based composite material with various carbon fillers are widely used to protect radioequipment from different interference, to improve characteristics of radar absorbing coatings. Current synthesis processes are sophisticated and rather costly. The challenge is to develop new methods of producing composite materials by efficient knowledge intensive technologies to reduce the cost of products. The paper studies possibility of producing composite material on the basis of elastic polyurethane foam with carbon fillers using polyurethane impregnation in nonequilibrium black carbon suspension. Suspension composition: running water and carbon-bearing powders of nanometer range: fullerene black carbon, Taunite (multi-layer carbon nano tube material), technical carbon T900, wood soot. Nonequilibrium suspension was produced by treatment in hydrodynamic generator of rotor type (cavitation mode). Angular rotation speed of the rotor ω = 10000 rpm.

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Держатели документа:
Siberian Federal University, Svobodnyy Ave 79, Krasnoyarsk, 660049, Russian Federation
Federal Research Center, Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of Sciences, L.V. Kirensky Institute of Physics Sb Ras, Akademgorodok, 50, Krasnoyarsk, 660036, Russian Federation
Fed. Res. Ctr. krasnoyarsk Sci. Ctr. of the Siberian Branch of the Russian Academy of Sciences, Akademgorodok, 50, Krasnoyarsk, 660036, Russian Federation

Доп.точки доступа:
Stebeleva, O. P.; Kashkina, L. V.; Petrakovskaya, E. A.; Петраковская, Элеонора Анатольевна; Rubleva, T. V.; Nikitin, S. L.; Vshivkova, O. A.; International Scientific Conference on Metrological Support of Innovative Technologies(2 ; 2020 ; 4 March ; Krasnoyarsk)
}
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10.

    Characterization of the iron oxide phases formed during the synthesis of core-shell FexOy@C nanoparticles modified with Ag / D. A. Petrov, C. R. Lin, R. D. Ivantsov [et al.] // Nanotechnology. - 2020. - Vol. 31, Is. 39. - Ст. 395703, DOI 10.1088/1361-6528/ab9af2. - Cited References: 46. - The reported study was funded by Joint Research Project of Russian Foundation for Basic Research № 19-52-52002 and Ministry of Science and Technology, Taiwan MOST № 108-2923-M-153-001-MY3 and № 106-2112-M-153-001-MY3. The samples of series 1 were studied with the support of the Ministry of Science and Higher Education of the Russian Federation within the State assignment FSRC «Crystallography and Photonics» RAS. The electron microscopy investigations were conducted in the SFU Joint Scientific Center supported by the State assignment (#FSRZ-2020-0011) of the Ministry of Science and Higher Education of the Russian Federation . - ISSN 1361-6528
   Перевод заглавия: Идентификация фаз оксида железа, формирующихся в процессе синтеза наночастиц FexOy@C с морфологией ядро-оболочка, модифицированных Ag
Кл.слова (ненормированные):
core–shell nanoparticles -- iron oxides -- carbon shell -- Ag nanoparticles
Аннотация: Core–shell FexOy@C nanoparticles (NPs) modified with Ag were studied with x-ray diffraction, transmission electron microscopy, energy dispersive elemental mapping, Mössbauer spectroscopy, static magnetic measurements, and optical magnetic circular dichroism (MCD). FexOy@C NPs synthesized by the pyrolysis process of the mixture of Fe(NO3)3 centerdot 9H2O with oleylamine and oleic acid were added to a heated mixture of oleylamine and AgNO3 in different concentrations. The final product was a mixture of iron oxide crystalline NPs in an amorphous carbon shell and Ag crystalline NPs. The iron oxide NPs were presented by two magnetic phases with extremely close crystal structures: Fe3O4 and γ-Fe2O3. Ag is shown to form crystalline NPs located very close to the iron oxide NPs. An assumption is made about the formation of hybrid FexOy@C-Ag NPs. Correlations were obtained between the Ag concentration in the fabricated samples, their magnetic properties and the MCD spectrum shape. Introducing Ag led to a approximately linear decrease of the NPs saturation magnetization depending upon the Ag concentration, it also resulted into the MCD spectrum shift to the lower light wave energies. MCD was also studied for the Fe3O4@C NPs synthesized earlier with the same one-step process using different heat treatment temperatures, and MCD spectra were compared for two series of NPs. A possible contribution of the surface plasmon excitation in Ag NPs to the MCD spectrum of the FexOy@C-Ag NPs is discussed.

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Держатели документа:
Kirensky Institute of Physics, FRC, KSC, SB RAS, Krasnoyarsk 660036, Russia
National Pingtung University, Pingtung City, Pingtung County 90003, Taiwan
Siberian Federal University, Svobodny Av., 79, Krasnoyarsk 660041, Russia
Shubnikov Institute of Crystallography of FSRC 'Crystallography and Photonics' RAS, Moscow 119333, Russia

Доп.точки доступа:
Petrov, D. A.; Петров, Дмитрий Анатольевич; Lin, C. R.; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Ovchinnikov, S. G.; Овчинников, Сергей Геннадьевич; Zharkov, S. M.; Жарков, Сергей Михайлович; Yurkin, G. Yu.; Юркин, Глеб Юрьевич; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Knyazev, Yu. V.; Князев, Юрий Владимирович; Molokeev, M. S.; Молокеев, Максим Сергеевич; Tseng, Y. T.; Lin, E. S.; Edelman, I. S.; Эдельман, Ирина Самсоновна; Baskakov, A. O.; Starchikov, S. S.; Lyubutin, I. S.
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