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Каталог книг и брошюр библиотеки ИФ СО РАН

Каталог журналов библиотеки ИФ СО РАН

Труды сотрудников ИФ СО РАН

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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Volova T., Goncharov D., Sukovatyi A. G., Shabanov A. V., Nikolaeva E., Shishatskaya E.
Заглавие : Electrospinning of polyhydroxyalkanoate fibrous scaffolds: effects on electrospinning parameters on structure and properties
Коллективы : Project 'Biotechnologies of novel biomaterials: innovative biopolymers and devices for biomedicine' [1, 11.G34.31.0013]; Government of the Russian Federation [220]; RF President for supporting young Doctors of Sciences [MD-3112.2012.4]
Место публикации : J. Biomater. Sci.-Polym. Ed.: Taylor & Francis, 2014. - Vol. 25, Is. 4. - P.370-393. - ISSN 0920-5063, DOI 10.1080/09205063.2013.862400. - ISSN 1568-5624
Примечания : Cited References: 52. - This study was financially supported by Project 'Biotechnologies of novel biomaterials: innovative biopolymers and devices for biomedicine' (Agreement No. 1 of 15.02.2013 to Agreement No. 11.G34.31.0013) in accordance with Resolution No. 220 of the Government of the Russian Federation of April 9, 2010, 'On measures designed to attract leading scientists to the Russian institutions of higher learning' and Grant of the RF President for supporting young Doctors of Sciences No. MD-3112.2012.4.
Предметные рубрики: TISSUE ENGINEERING APPLICATIONS
FIBER MATS
POLY 3-HYDROXYBUTYRATE
POLY(3-HYDROXYBUTYRATE-CO-3-HYDROXYVALERATE)
BIOCOMPATIBILITY
PROLIFERATION
FABRICATION
NANOFIBERS
COPOLYMERS
MEMBRANES
Ключевые слова (''Своб.индексиров.''): electrospinning--polyhydroxyalkanoates--ultrafine fibers--physical-mechanical properties--fibroblast cells
Аннотация: IIn this study, electrospinning was used to prepare ultrafine fibers from PHAs with different chemical compositions: P(3HB) and copolymers: P(3HB-co-4HB), P(3HB-co-3HV), and P(3HB-co-3HHx). The main process parameters that influence ultrafine fiber diameter and properties (polymer concentration, solution feeding rate, working distance, and applied voltage) have been investigated and their effects evaluated. The study revealed electrospinning parameters for the production of high-quality ultrafine fibers and determined which parameters should be varied to tailor the properties of the products. This study is the first to compare biological and physical-mechanical parameters of PHAs with different chemical compositions as dependent upon the fractions of monomers constituting the polymers and ultrafine fiber orientation. Mechanical strength of aligned ultrafine fibers prepared from different PHAs is higher than that of randomly oriented ones; no significant effect of ultrafine fiber orientation on surface properties has been found. None of the fibrous scaffolds produced by electrospinning from PHAs had any adverse effects on attachment, growth, and viability of NIH 3T3 mouse fibroblast cells, and all of them were found to be suitable for tissue engineering applications.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Edelman I. S., Zharkov S. M., Pankrats A. I., Vorotynov A. M., Tugarinov V. I., Ivantsov R. D., Petrov D. A., Velikanov D. A., Lin C. -R., Chen C. -C., Tseng Y. -T., Hsu H. -S.
Заглавие : Electron spin resonance in Cu1−xFexCr2Se4 nanoparticles synthesized with the thermal decomposition method
Место публикации : J. Magn. Magn. Mater.: Elsevier, 2017. - Vol. 436. - P.21-30. - ISSN 03048853 (ISSN), DOI 10.1016/j.jmmm.2017.04.006
Примечания : Cited References: 34. - The paper was partially supported by the President of Russia (Grant #NSh-7559.2016.2). We also thank the Ministry of Science and Technology of Taiwan, Taiwan, and the Siberian Branch of RAS, Russian Federation (MOST 102-2112-M-153-002-MY3) for the financial support.
Ключевые слова (''Своб.индексиров.''): anisotropy--association reactions--chromium compounds--decomposition--electrospinning--inorganic compounds--magnetic moments--magnetocrystalline anisotropy--nanoparticles--plates (structural components)--resonance--spin dynamics--synthesis (chemical)--temperature distribution--thermolysis--inter-particle interaction--nanoparticle (nps)--resonance spectrum--single-crystalline--temperature behavior--temperature decrease--temperature dependence--thermal decomposition methods--electron spin resonance spectroscopy
Аннотация: IIn this paper, we present a study of the electron spin resonance (ESR) of nanoparticles (NPs) of Cu1−xFexCr2Se4 chalcogenides with x = 0, 0.2, and 0.4. NPs were synthesized via the thermal decomposition of metal chloride salts and selenium powder in a high-temperature organic solvent. According to the XRD and HRTEM data, the NPs were single crystalline nearly hexagonal plates with the structure close to CuCr2Se4 (Fd-3m, a = 10.337 Å). For x = 0 and 0.2, the NPs tend to form long stacks consisting of the plates “face to face” attached to each other due to the magnetostatic interparticle interaction. Only separate NPs were observed in the case of x = 0.4. Peculiarities were revealed in the ESR temperature behavior for the NPs with x = 0 and 0.2 consistent with the features in the temperature dependences of the NPs magnetization. The non-monotonous dependence of the resonance field Hres on the temperature with a kink near 130 K and the energy gap in the resonance spectrum depending on the type of nanoparticle compacting are the distinct peculiarities. One of the main factors is discussed in order to explain the peculiarities: the coexistence of two types of anisotropy in the Cu1−xFexCr2Se4 NPs, in-plain shape anisotropy and magnetocrystalline anisotropy with four easy axes, which increases strongly with the temperature decrease.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Koblischka M. R., Gokhfeld D. M., Chang C., Hauet T., Hartmann U.
Заглавие : Pinning force scaling of electrospun Bi-2212 nanowire networks
Место публикации : Solid State Commun.: Elsevier, 2017. - Vol. 264. - P.16-18. - ISSN 00381098 (ISSN), DOI 10.1016/j.ssc.2017.07.002
Примечания : Cited References: 24. - This work is supported by the DFG project Ko2323/8, which is gratefully acknowledged
Ключевые слова (''Своб.индексиров.''): electrospinning--bi-2212 superconductors--flux pinning--pinning force scaling
Аннотация: Flux pinning forces were determined on different network samples of superconducting Bi2Sr2CaCu2O8 (Bi-2212) nanowires prepared by the electrospinning technique. We employed magnetization data determined by SQUID magnetometry in a wide temperature range 10 K T 35 K, where a strong superconducting signal prevails. The scaling analysis of the pinning forces was applied to interprete the data obtained. Both pure and Li-doped Bi2212 nanowire networks exhibit a peak position of h0∼ 0.11, which is smaller than the expected value of h0
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Bolbasov E. N., Buznik V. M., Stankevich K. S., Goreninskii S. I., Ivanov Y. N., Kondrasenko A. A., Gryaznov V. I., Matsulev A. N., Tverdokhlebov S. I.
Заглавие : Composite materials obtained via two-nozzle electrospinning from polycarbonate and vinylidene fluoride/tetrafluoroethylene copolymer
Место публикации : Inorg. Mater.: Appl. Res. - 2018. - Vol. 9, Is. 2. - P.184-191. - ISSN 20751133 (ISSN), DOI 10.1134/S2075113318020065
Примечания : Cited References: 36. - The membranes were prepared and studied by means of scanning electron microscopy and X-ray diffraction at the Tomsk National Research Polytechnic University under financial support of the Russian Science Foundation (project no. 16-13-10239). NMR studies were financially supported by the Russian Foundation for Basic Research (project no. 14-29-10178 ofi_m) and performed at the Kirensky Institute of Physics, Siberian Branch, Russian Academy of Sciences.
Ключевые слова (''Своб.индексиров.''): electrospinning--two-nozzle electrospinning--nonwoven composite materials--vinylidene fluoride/tetrafluoroethylene copolymer--polycarbonate--fluoropolymers
Аннотация: Nonwoven composite membranes based on polycarbonate (PC) and vinylidene fluoride/tetrafluoroethylene copolymer were obtained via the two-channel electrospinning method with a common collector. Three groups of materials were studied: the first one was a polymer membrane made of a vinylidene fluoride/tetrafluoroethylene copolymer, the second one was a polymer membrane based on PC, and the third one involved a composite polymer membrane. Scanning electron microscopy studies of morphology of the polymeric membranes showed that a composite material with a variable pore area could be obtained, which allows selection of this parameter depending on the purpose. The resulting composite material and its constituents are studied with nuclear magnetic resonance, IR spectroscopy, X-ray diffraction, and differential scanning calorimetry. There are electrically active crystalline phases in the composite membranes. The obtained nonwoven composite membrane formed is presented as a two-phase system without any chemical interactions between the phases. © A.V. Alekseev, D.Yu. Dubov, M.R. Predtechenskiy, 2017 and Pleiades Publishing, Ltd., 2018.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Морозов, Евгений Владимирович, Больбасов Е. Н., Горенинский С. И., Юрков Г. Ю., Бузник, Вячеслав Михайлович
Заглавие : МРТ исследование процессов замерзания воды и таяния льда в полимерных композиционных мембранах
Место публикации : Полимер. матер. и технол. - 2020. - Т. 6, № 4. - С. 20-29. - ISSN 2415-7260, DOI 10.32864/polymmattech-2020-6-4-20-29
Примечания : Библиогр.: 23
Аннотация: Полимерные композиционные мембраны, полученные методом электроформования, находят широкое применение в различных отраслях промышленности благодаря своей структуре и уникальным свойствам. Однако, вследствие высокой сорбционной активности изделия на основе таких мембран подвержены негативному влиянию атмосферной влаги в условиях знакопеременного температурного воздействия. В данной работе представлены новые полимерные композиционные мембраны с улучшенными водоотталкивающими свойствами, сочетающие слои гидрофобных и гидрофильных волокнистых материалов. Впервые проведены МРТ исследования процессов замерзания воды и таяния льда в них. Детально изучены качественная и количественная стороны протекающих процессов. Обнаружено, что водопоглощение в композиционных мембранах осуществляется исключительно за счет слоев гидрофильного материала. Исследование также показало, что скорость протекания процессов замерзания/таяния оказалась чувствительна к присутствию гидрофобных слоев: обнаружено, что введение слоев гидрофобных волокон в композит приводит к существенному снижению скорости замерзания и таяния. Полученный результат демонстрирует возможности метода МРТ для исследования и диагностики полимерных волокнистых материалов и процессов замерзания/таяния в них, а также показывает пути оптимизации свойств готовых полимерных материалов для арктических и иных практических приложений.Electrospun polymer composite membranes are very attractive for many industrial applications due to their special structure and properties. However, high sorption capacity of fibrous material results in noticeable moisture content in the membranes which then, being exposed to natural environment, suffer from the freeze/thawing cycling. In this work, the new polymer composite membranes with advanced water resistance due to a layered hydrophobic/hydrophilic structure were manufactured via electrospinning. Using these membranes the NMR imaging study of water freezing and ice thawing were carried out for the first time. In result, the qualitative and quantitative character of the processes was elucidated. Thus, it was found out that the water uptake in membranes occurs solely due to the hydrophilic layers. From the other hand, the hydrophobic layers play a major role, affecting the rate of freeze/thawing: introduction the hydrophobic material into membranes structure makes the freeze/thawing front propagation slow down. The results obtained demonstrate the advantages of the NMR imaging as a tool for studying and control of the polymer fibrous materials, processes of water sorption and water freezing/thawing occurring under the natural environment conditions. New results also show the routes of polymer materials optimization for arctic and other practical applications.
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