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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Bogdanov E. V., Kartashev A. V., Pogoreltsev E. I., Gorev M. V., Laptash N. M., Flerov I. N.
Заглавие : Anomalous behaviour of thermodynamic properties at successive phase transitions in (NH4)3GeF7
Место публикации : J. Solid State Chem. - 2017. - Vol. 256. - P.162-167. - ISSN 00224596 (ISSN), DOI 10.1016/j.jssc.2017.09.010
Примечания : Cited References: 23. - The reported study was partially supported by the Russian Foundation for Basic Research, research project no. 15-02-02009 a.
Ключевые слова (''Своб.индексиров.''): phase transition--fluorides--heat capacity--entropy--thermal expansion--high pressure
Аннотация: Heat capacity, thermal dilatation, susceptibility to hydrostatic pressure and dielectric properties associated with succession of three phase transitions below room temperature in double fluoride salt (NH4)3GeF7 were studied. A possible transformation into the parent Pm-3m cubic phase was not observed up to the decomposition of compound. Nonferroelectric nature of structural distortions was confirmed. The DTA under pressure studies revealed a high temperature stability of two phases: P4/mbm and Pbam. The entropies of the phase transitions agree well with the model of structural distortions. Analysis of the thermal properties associated with the individual phase transitions in the framework of thermodynamic equations has shown a high reliability of the data obtained. © 2017 Elsevier Inc.
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Вид документа : Однотомное издание
Шифр издания :
Автор(ы) : Flerov I. N., Bogdanov E. V., Gorev M. V.
Заглавие : Barocaloric effect in ferroelastic fluorides and oxyfluorides
Колич.характеристики :23 pp.
Место публикации : Barocaloric effects in the solid-state. Materials and methods/ ed. P. Lloveras: IOP Publishing, 2023. - Chapt. 4. - P.4-1-4-23. - , DOI 10.1088/978-0-7503-4690-0ch4
Примечания : Cited References: 68
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Flerov I. N., Gorev M. V., Bogdanov E. V., Laptash N. M.
Заглавие : Barocaloric effect in ferroelastic fluorides and oxyfluorides
Место публикации : Ferroelectrics: Taylor and Francis, 2016. - Vol. 500, Is. 1. - P.153-163. - ISSN 00150193 (ISSN), DOI 10.1080/00150193.2016.1214525
Примечания : Библиогр.: 33. - The reported study was partially supported by the Russian Foundation for Basic Research (RFBR), research project No. 15-02-02009 a.
Ключевые слова (''Своб.индексиров.''): phase transition--fluorides--oxyfluorides--thermal properties--barocaloric effect
Аннотация: Using the data about the temperature - pressure phase diagram and the phase transition entropy at ambient and high pressure, intensive and extensive barocaloric effects were analyzed in the region of single and successive order-disorder phase transitions in fluorides and oxyfluorides with the elpasolites-cryolite structure. It was found that hydrostatic as well as chemical pressure are the effective tools to change the entropy of compounds with disordered ionic groups or atoms in structure and to realize the significant intensive and extensive barocaloric effects comparable with the values of baro- and magnetocaloric effects, characteristic for materials, considered as promising solid refrigerants. © 2016 Taylor & Francis Group, LLC.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Flerov I. N., Gorev M. V., Mikhaleva E. A., Kartashev A. V., Bondarev V. S.
Заглавие : Caloric Effects in Some Ferroelectric and Ferroelastic Fluorides, Oxyfluorides and Oxides
Коллективы : Russia/CIS/Baltic/Japan Symposium on Ferroelectricity, International Workshop on Relaxor Ferroelectrics
Место публикации : Joint 13th Russia/CIS/Baltic/Japan Symp. on Ferroelectricity and Int. Workshop on Relaxor Ferroelectrics (RCBJSF-IWRF 2016): book of abstracts. - 2016. - Ст.Invite-6
Примечания : References: 4. - The reported study was partially supported by RFBR, research project No. 15-02-02009 a
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Gorev M. V., Kartashev A. V., Bogdanov E. V., Flerov I. N., Laptash N. M.
Заглавие : Calorimetric, dilatometric and DTA under pressure studies of the phase transitions in elpasolite (NH4)2KZrF7
Место публикации : J. Fluor. Chem. - 2020. - Vol. 235. - Ст.109523. - ISSN 00221139 (ISSN), DOI 10.1016/j.jfluchem.2020.109523
Примечания : Cited References: 45. - The reported study was funded by RFBR according to the research project No. 18-02-00269 a. X-ray and dilatometric data were obtained using the equipment of Krasnoyarsk Regional Center of Research Equipment of Federal Research Center "Krasnoyarsk Science Center SB RAS"
Аннотация: Heat capacity, thermal expansion, and sensitivity to the hydrostatic pressure of (NH4)2KZrF7 elpasolite are studied in a wide temperature range. The changes in deformation and entropy during successive phase transitions are determined: Δ(ΔV/V) = 3·10−4; ΔS = 8 J/mol K The temperatures and entropies of phase transitions turned out to be slightly sensitive to pressure changes. An analysis of the entropy of phase transformations was performed in the framework of the model of the cubic phase structure Fm-3 m. In the low temperature phase, an anomalous behavior of thermodynamic properties, which is not characteristic of phase transitions, was observed, accompanied by a significant change in the crystal lattice entropy.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Flerov I. N., Gorev M. V., Bogdanov E. V., Laptash N. M.
Заглавие : Chemical pressure as an effective tool for tuning the structural disordering and barocaloric efficiency of complex fluorides (NH4)3MF7 (M: Sn, Ti, Ge, Si)
Колич.характеристики :18 с
Место публикации : J. Phys. D: Appl. Phys. - 2024. - Vol. 57, Is. 17. - Ст.175301. - ISSN 00223727 (ISSN), DOI 10.1088/1361-6463/ad211b. - ISSN 13616463 (eISSN)
Примечания : Cited References: 39. - The study was supported by a Grant from the Russian Science Foundation No. 23-22-00115, https://rscf.ru/project/23-22-00115/
Аннотация: Double fluoride salts (NH4)3M4+F7 (M4+: Sn, Ti, Ge, Si) demonstrate a high efficiency of using chemical pressure as a tool for control and tuning structural ordering/disordering, sensitivity to hydrostatic pressure, successions of the phase transitions, etc and, as a result, for purposeful variation within a wide range of parameters of barocaloric effect (BCE). The conventional and inverse BCEs near the triple points were found on the T − p phase diagrams, combination of which can be used to construct original cooling cycle in narrow temperature and pressure ranges. Reconstructive transformation between two cubic phases, Pm3-m ↔ Pa3-, realized in (NH4)3SnF7 at atmospheric pressure and in (NH4)3TiF7 at p ˃ 0.4 GPa are characterized by rather low thermal hysteresis, δT0 = 1 K, and a great entropy change, ΔSBCE = 110–152 J (kg · K)−1, depending on the size of the central atom. At above 300–350 K, a contribution to BCE associated with the regular thermal expansion of the crystal lattice becomes comparable to entropy and temperature changes under pressure in the region of the phase transitions. An analysis of the absolute, relative and integral barocaloric characteristics of (NH4)3M4+F7 compounds showed their high competitiveness with respect to other barocaloric materials considered as promising solid-state refrigerants.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Flerov I. N., Gorev M. V., Bogdanov E. V.
Заглавие : Complex fluorides and oxyfluorides: successive ferroelastic phase transitions and barocaloric effect
Коллективы : International Symposium on Solid State Chemistry for Applications and Sustainable Development, Sustainable Industrial Processing Summit and Exhibition, FLOGEN Stars Outreach
Место публикации : Tressaud Int. Symp. on Solid State Chem. for Applications and Sustainable Dev.: program. - 2019. - Ст.ChemistryFriPM106. - P.103
Примечания : Cited References: 4
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Xia, Zhiguo, Molokeev M. S., Oreshonkov A. S., Atuchin V. V., Liu R. S., Dong C.
Заглавие : Crystal and local structure refinement in Ca2Al3O6F explored by X-ray diffraction and Raman spectroscopy
Место публикации : Phys. Chem. Chem. Phys.: Royal Society of Chemistry, 2014. - Vol. 16, Is. 13. - P.5952-5957. - ISSN 1463-9076, DOI 10.1039/c3cp53816h. - ISSN 1463-9084
Примечания : Cover illustration: Graphical abstract from this article. - Cited References: 34. - This present work was supported by the National Natural Science Foundations of China (Grant No. 51002146, 51272242), Natural Science Foundations of Beijing (2132050), the Program for New Century Excellent Talents in University of Ministry of Education of China (NCET-12-0950), Beijing Nova Program (Z131103000413047) and Beijing Youth Excellent Talent Program (YETP0635), and this study was also partially supported by SB RAS, Grant 28.13. Part of the work was supported by the National Science Council of Taiwan under contract No. NSC 101-2113-M-002-014-MY3.
Предметные рубрики: EMITTING OXYFLUORIDE PHOSPHOR
PHASE-TRANSITIONS
SOLID-STATE
FLUORIDES
DIODES
Аннотация: We present a combined structural analysis on the powder of the Ca2Al3O6F phase using X-ray diffraction (XRD) and Raman spectroscopy techniques. The crystal structure of Ca2Al3O6F has been refined in the rhombohedral system, R space group, a = 17.3237(7) Å, c = 7.00017(4) Å, V = 1819.38(2) Å3, Z = 6. The Ca2Al3O6F phase consists of almost ideal AlO4 tetrahedrons linked through corners, Ca2+ ions in voids, and F− ions disordered over 6 sites around the Ca2 ion. The two different Ca sites have also been verified by the photoluminescence spectrum and decay curves using Eu2+ as the probe ion substituted onto the Ca2+ sites. A lattice dynamics simulation based on the simplified version of the Born–Karman potential model has been produced. Calculated Raman phonon modes agree qualitatively well with the experimental data. The calculations show that the strong line at 538 cm−1 (Ag) corresponds to the vibrational mode of a six-membered AlO4 tetrahedrons ring, and the line at 572 cm−1 (Ag) corresponds to the full symmetric vibration of fluorine atoms in the ab crystal plane.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Molokeev M. S., Vasiliev A. D., Voronov V. N., Laptash N. M., Aleksandrov K. S., Flerov I. N., Tressaud A.
Заглавие : Crystal structures of room and low temperature phases in RBKTiOF5 and RB2KFeF6
Коллективы : "Advanced inorganic fluorides", International Siberian workshop
Место публикации : Advanced inorganic fluorides: the Third International Siberian workshop Intersibfluorine - 2008, September 01-06, 2008, Vladivostok, Russia : proceedings of ISIF-2008. - 2008. - С. 69-70. - ISBN 978-5-98128-036-8
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10.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Voronov V. N., Nikolayeva T. V.
Заглавие : Crystallization and studies of A+B3+F4 compounds
Коллективы : "Advanced inorganic fluorides", International Siberian workshop
Место публикации : Advanced inorganic fluorides: the Third International Siberian workshop Intersibfluorine - 2008, September 01-06, 2008, Vladivostok, Russia : proceedings of ISIF-2008. - Vladivostok, 2008. - p.200-203. - ISBN 978-5-98128-036-8
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11.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Flerov I. N., Gorev M. V., Fokina V. D., Bovina A. F., Bogdanov E. V., Pogoreltsev E. I., Laptash N. M.
Заглавие : Disorder and phase transitions in oxyfluoride (NH4)(3)Ta(O-2)(2)F-4
Место публикации : J. Fluor. Chem. - 2011. - Vol. 132, Is. 10. - P.713-718. - ISSN 0022-1139, DOI 10.1016/j.jfluchem.2011.05.012
Примечания : Cited Reference Count: 19. - Гранты: This work was supported by the Council on Grants from the President of the Russian Federation for the Support of Leading Scientific Schools of the Russian Federation (NSh-4645.2010.2).Финансирующая организация: Council on Grants from the President of the Russian Federation for the Support of Leading Scientific Schools of the Russian Federation [NSh-4645.2010.2]
Предметные рубрики: HEAT-CAPACITY
COMPLEXES
RB2KTIOF5
FLUORIDES
CRYOLITE
Ключевые слова (''Своб.индексиров.''): cubic oxyfluorides--structural disorder--phase transitions--entropy--permittivity--pressure effect--cubic oxyfluorides--entropy--permittivity--phase transitions--pressure effect--structural disorder
Аннотация: Calorimetric, X-ray, dielectric and DTA under pressure measurements have been performed on oxyfluoride (NH4)(3)Ta(O-2)(2)F-4. The succession of nonferroelectric phase transitions was found associated with the order-disorder processes. The comparative analysis tantalate with related niobate has revealed the important role of the central atom in the physical properties behavior, mechanism of structural distortions and barocaloric effect in oxyfluorides with the eight-coordinated anionic polyhedra. (C) 2011 Elsevier By. All rights reserved.
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12.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Bogdanov E. V., Gorev M. V., Flerov I. N.
Заглавие : Effect of deuteration on the barocaloric properties of complex vanadates (NH4)3VOxF6−x (x: 1, 2)
Место публикации : Solid State Sci. - 2022. - Vol. 133. - Ст.107022. - ISSN 12932558 (ISSN), DOI 10.1016/j.solidstatesciences.2022.107022
Примечания : Cited References: 28
Аннотация: We report on the analysis of intensive and extensive barocaloric properties and their sensitivity to deuteration of complex oxyfluorides (NH4)3VOxF6−x (x: 1, 2) undergoing a similar sequence of structural phase transitions. Due to the high sensitivity to hydrostatic pressure and the strong disordering of six-coordinated anionic fluoro-oxygen species, (NH4)3VO2F4 and (ND4)3VO2F4 crystals demonstrate the highest barocaloric efficiency at low pressure, p = 0.1 GPa, during the phase transition from the initial cubic phase: barocaloric coefficients reach large values |ΔSBCE|/p ≈ 400 J/(kg K GPa) and ΔTAD/p ≈ 80 K/GPa. Anionic, [VOF5] → [VO2F4], and cationic, [ND4] → [NH4] substitutions are accompanied by a decrease in the disorder of structural units in the cubic phase, which leads to a decrease in changes in entropy and temperature under pressure. The contribution of thermal expansion of the crystal lattice to the total intensive and extensive barocaloric effects is large and amounts to about 30–40%.
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13.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Bogdanov E. V., Pogoreltsev E. I., Gorev M. V., Mel'nikova S. V., Molokeev M. S., Laptash N. M., Flerov I. N.
Заглавие : Effect of the size of the central atom on the stability of crystalline phases in solid solutions (NH4)3TixSn1-xF7
Колич.характеристики :8 с
Место публикации : J. Solid State Chem. - 2023. - Vol. 328. - Ст.124373. - ISSN 00224596 (ISSN), DOI 10.1016/j.jssc.2023.124373. - ISSN 1095726X (eISSN)
Примечания : Cited References: 20. - The study was supported by a grant from the Russian Science Foundation № 23-22-00115, https://rscf.ru/project/23-22-00115/X-ray and dilatometric data and SEM images were obtained using the equipment of the Krasnoyarsk Regional Center for Collective Use of the Federal Research Center — Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of Sciences. We are grateful to Dr. A.V. Shabanov for examination of the SEM images
Аннотация: The effect of a change in internal pressure as a result of partial substitution of the central atom on the realization and stability of the initial and distorted crystalline phases in (NH4)3TixSn1-xF7 solid solutions has been studied. It was found that at a Ti concentration in the range of x = 0.15–0.40, the reconstructive transition Pm-3m ↔ Pa-3 is transformed into a sequence of phase transitions Pm-3m ↔ P4/mbm ↔ P4/mnc ↔ Pa-3. In the (NH4)3Ti0.15Sn0.85F7 solid solution, the first-order phase transition between two cubic phases at T0 = 352 K is characterized by a significant volume jump δ(ΔV/V0) ≈ 1 %, comparable with that in (NH4)3SnF7. An increase of the Ti concentration leads to a strong decrease in the stability of the Pm-3m cubic phase: the first tetragonal P4/mbm phase appears in (NH4)3Ti0.4Sn0.6F7 at T0 = 400 K, which proves the existence of the predicted high-temperature cubic phase in (NH4)3TiF7. In solid solutions, a decrease in birefringence and entropy of phase transitions was observed in comparison with the initial compounds with Sn and Ti as central atoms. The role of critical parameters (unit cell volume, temperature, external pressure) in the formation of cubic and distorted phases is discussed.
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14.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Gerasimova Y. V., Krylov A. S., Vtyurin A. N., Laptash N. M.
Заглавие : Ferroelastic phase transition in the family of crystals of double salts of fluorides according to vibrational spectroscopy data
Коллективы : IEEE International Symposium on Applications of Ferroelectrics, International Conference on ElectroCeramics, European Meeting on Ferroelectricity, International Workshop on PiezoMEMS, Piezoresponse Force Microscopy Workshop
Место публикации : Joint Conference of the IEEE ISAF, EMF, ICE, IWPM and PFM: Abstract book. - 2019. - P.174
Примечания : Cited References: 3. - The study was carried out with the financial support of the Russian Foundation for Basic Research №17-02-00920
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15.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Gerasimova Yu. V., Krylov A. S., Vtyurin A. N., Laptash N. M., Krylova S. N.
Заглавие : Ferroelastic phase transition in the family of double fluoride crystals by Raman spectroscopy
Коллективы : European Meeting on Ferroelectricity
Место публикации : Ferroelectrics. - 2020. - Vol. 568, Is. 1. - P.185-190. - DOI 10.1080/00150193.2020.1713348
Примечания : Cited References: 14. - This research is supported by Russian Foundation for Basic Research under Grant No. 17-02-00920
Аннотация: In order to clarify ordering mechanisms of ferroic phase transitions in double fluoride salts (NH4)3SnF7, (NH4)3GeF7 and (NH4)3TiF7, their Raman scattering spectra have been studied in wide ranges of frequencies (20–3400 cm−1) and temperatures (8–410 K). Substitution of the central ion in the octahedron groups was found to change not only the phase transition types and sequences, but to modify the types of structural disorder as well, which is a special feature of these high-symmetry fluoride crystals.
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16.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Flerov I. N., Gorev M. V., Aleksandrov K. S., Tressaud A., Fokina V. D.
Заглавие : Ferroelastic phase transitions in fluorides with cryolite and elpasolite structures
Место публикации : Crystallogr. Rep. - 2004. - Vol. 49, Is. 1. - P.100-107. - ISSN 1063-7745, DOI 10.1134/1.1643969
Примечания : Cited References: 43
Предметные рубрики: NUCLEAR MAGNETIC-RESONANCE
THERMODYNAMIC PROPERTIES
RB2KMIIIF6 ELPASOLITES
NEUTRON-DIFFRACTION
CRYSTALS
PEROVSKITES
DIAGRAM
SC
RB2KGAXSC1-XF6
SCATTERING
Аннотация: The ferroelastic phase transitions are investigated in several series of fluoride crystals belonging to the elpasolite and cryolite families (space group Fm (3) over barm) with the general formula A(2)BB'F-6. The influence of the size and shape of cations and anions on the entropy and the mechanism of structural distortions is discussed. (C) 2004 MAIK "Nauka/Interperiodica".
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18.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Flerov I. N., Gorev M. V.
Заглавие : Fluorides and Oxyfluorides with Elpasolite-Cryolite Structure: Order-Disorder Phase Transitions and Barocaloric Efficiency
Коллективы : Functional Materials and Nanotechnologies
Место публикации : International Conference “Functional materials and nanotechnologies” FM&NT 2012. - 2012. - P.65
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19.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Gorev M. V., Bogdanov E. V., Flerov I. N.
Заглавие : Fluorides and oxyfluorides: successive ferroelastic phase transitions and barocaloric effect
Коллективы : Fall Meeting, European Materials Research Society, European Materials Research Society, Warsaw University of Technology
Место публикации : E-MRS fall meeting: conference programme. - 2019. - С. E.P.2
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20.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Pogoreltsev E. I., Flerov I. N., Kartashev A. V., Bogdanov E. V., Laptash N. M.
Заглавие : Heat capacity, entropy, dielectric properties and T–p phase diagram of (NH4)3TiF7
Коллективы : Russian Foundation for Basic Research [15-02-02009]; Council on Grants from the President of the Russian Federation for the Support of Leading Scientific Schools of the Russian Federation [NSh-924.2014.2]
Место публикации : J. Fluor. Chem.: Elsevier Science, 2014. - Vol. 168. - P.247-250. - ISSN 0022-1139, DOI 10.1016/j.jfluchem.2014.10.016. - ISSN 1873-3328
Примечания : Cited References: 16. - This work was supported by the Russian Foundation for Basic Research (Grant no. 15-02-02009), and the Council on Grants from the President of the Russian Federation for the Support of Leading Scientific Schools of the Russian Federation (Grant no. NSh-924.2014.2).
Предметные рубрики: CRYSTAL-STRUCTURE
TRANSITIONS
FLUORIDES
NH4F
Ключевые слова (''Своб.индексиров.''): cubic fluorides--phase transitions--dielectric--phase diagram--calorimetry
Аннотация: Successive phase transitions G1 -- G2 -- G3 in the double salt (NH4)(3)TiF7 have been studied by detailed calorimetric, DTA under hydrostatic pressure and dielectric measurements. Rather large entropy jumps at phase transition points were found to be followed by large additional contributions associated with the temperature dependence of the excess heat capacity. The permittivity behaviour and the tangent of the dielectric losses proved the nonferroelectric nature of both transformations. Two triple-points were found on the temperature-pressure phase diagram, suggesting the existence of a hypothetical parent G0 = Pm-3m cubic phase. A direct transformation between high (G0) and low (G3) temperature cubic phases takes place at p 0.41 GPa with a baric coefficient dT(G0) -- (G3)/dp = -40 K/GPa. (C) 2014 Elsevier B.V. All rights reserved.
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