Библиотека института физики им. Л.В. Киренского СО РАН

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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Ruseikina A. V., Solovyov L. A., Chernyshev V. А., Aleksandrovsky A. S., Andreev O. V., Krylova S. N., Krylov A. S., Velikanov D. A., Molokeev M. S., Maximov N. G., Grigoriev M. V., Garmonov A. A., Matigorov A. V.
Заглавие : Synthesis, structure, and properties of EuErCuS3
Место публикации : J. Alloys Compd. - 2019. - Vol. 805. - P.779-788. - ISSN 09258388 (ISSN), DOI 10.1016/j.jallcom.2019.07.059
Примечания : Cited References: 54. - The work was supported by the State budget allocated to the fundamental research in the Ministry of Science and Education, Russian Federation of (Project No. V.45.3.3); by RFBR Grant 17-02-00754 ; by the Ministry of Science and Higher Education of the Russian Federation under Project No 3.9534.2017/8.9.
Аннотация: The crystal structure of the first-synthesized compound EuErCuS3 was determined from X-ray powder diffraction data: orthorhombic crystal system, space group Pnma, structural type Eu2CuS3: a = 10.1005(2) Å, b = 3.91255(4)Å, c = 12.8480(2) Å; V = 507.737(14) Å3, Z = 4, and ρx = 6.266 g/cm3. The temperatures and enthalpies of reversible polymorphic transitions and incongruent melting of the compound were determined by DSC: Tα↔β = 1524 K, ΔНα↔β = 2.3 ± 0.2 kJ∙mol−1; Tβ↔γ = 1575 K, ΔНβ↔γ = 0.7 ± 0.1 kJ∙mol−1; Tγ↔δ = 1602 K; ΔНγ↔δ = 1.3 ± 0.1 kJ∙mol−1 and Tcr = 1735 ± 10 K, ΔНcr = −3.5 ± 0.3 kJ∙mol−1. IR spectra were recorded in the range from 50 to 400 cm−1. The compound was found to be IR-transparent in the range 4000–400 cm−1. The compound was characterized by Raman spectroscopy. The observed spectra featured both Raman lines and luminescence. Ab initio calculations of the EuErCuS3 crystal structure and phonon spectrum were performed, the frequencies and types of fundamental modes were determined, and the involvement of constituent ions in the IR and Raman modes was assessed from an analysis of the ab initio displacement vectors. The vibrational spectra were interpreted. EuErCuS3 manifests a ferrimagnetic transition at 4.8 K. Its microhardness is 2850 MPa. The obtained data can serve as the basis for predicting the properties of EuLnCuS3 compounds. Valence states for Eu (2+) and Er (3+) are proved both by the XRD and optical methods. Optical band gap was found to be 1.934 eV from diffuse reflectance spectrum.
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Вид документа : Статья из сборника (выпуск продолж. издания)
Шифр издания :
Автор(ы) : Tripathy A., Gautam K., Dey K., Ahad A., Gudim I. A., Sathe V. G., Shukla D. K.
Заглавие : Dielectric and Raman spectroscopy measurements across structural phase transition in multiferroic HoFe3(BO3)4 single crystal
Коллективы : International Conference on Advanced Materials
Место публикации : AIP Conf. Proc. - 2019. - Vol. 2162: International Conference on Advanced Materials, ICAM 2019. - Ст.020062. - , DOI 10.1063/1.5130272
Примечания : Cited References: 10. - DKS acknowledges support from the DST, New Delhi, India through the grant no INI/RUS/RFBR/P-269 (Indo Russian project). K.G. thanks, Council of Scientific and Industrial Research, New Delhi, India, for support in the form of SRF.
Аннотация: We report on findings in the HoFe3(BO3)4 single crystal across structural phase transition by the dielectric and Raman spectroscopic measurements. In most of the compounds of RFe3(BO3)4 (R=La-Lu) family low temperature P3121 structure is introduced through structural phase transition (from space group R32). Temperature dependent dielectric measurements on the HoFe3(BO3)4 crystal depicts a step like feature at the structural phase transition at ?366 K. The Raman spectroscopy study also confirms the structural transition around this temperature. A clear signature of structural transition is reflected in the Raman spectra, mainly in the frequency range (200-400 cm-1). Appearance of new Raman modes below the transition temperature also indicates that the transition is from a high symmetry phase to a low symmetry phase.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Knyazev Yu. V., Tarasov A. S., Platunov M. S., Trigub A. L., Bayukov O. A., Boronin A. I., Solovyov L. A., Rabchevskii E. V., Shishkina N. N., Anshits A. G.
Заглавие : Structural and electron transport properties of CaFe2O4 synthesized in air and in helium atmosphere
Место публикации : J. Alloys Compd. - 2020. - Vol. 820. - Ст.153073. - ISSN 0925-8388, DOI 10.1016/j.jallcom.2019.153073. - ISSN 1873-4669 (eISSN)
Примечания : Cited References: 37. - The reported study was partially supported by the Russian Foundation for Basic Research, Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund of Science (grant #18-42-243011) and the UMNIK Program.
Аннотация: The samples with the CaFe2O4-type crystal structure were obtained by the solid-state reaction method at 1000 °C in the air and the helium atmosphere for the first time. We investigated the modification of the structural and electronic properties of the obtained samples. Mössbauer, XAFS-, XPS-spectroscopies, and dc-, ac-conductivity measurements were carried out. Mössbauer and XAFS-spectroscopies showed that the local environment of Fe and Ca cations does not change in the case of the inert atmosphere synthesis. Nevertheless, a sharp six-order increase in the electrical resistance observed at room temperature for the sample obtained in the in the helium atmosphere. Moreover, calculated from dc-conductivity data activation energy rises from 0.327 for the air-synthesized sample to 0.585 eV for helium-obtained one. This behavior indicates significant modification of in-band-gap energy structure, which correlated with thermally activated charge carriers. Our ac-conductivity measurements in the frequency range of 1 kHz–2 MHz for the CaFe2O4 obtained in the air showed the presence of defect levels in the energy band structure. Oxygen pressure reduction during the synthesis results in levels vanishing. Therefore, we suppose the key role of oxygen atoms in the transport properties of the material, which is indirectly confirmed by XPS data. In prospect, CaFe2O4 can be used in promising gas analyzers.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Lyashchenko S. A., Maximova O. A., Shevtsov D. V., Yakovlev I. A., Tarasov I. A., Varnakov S. N., Ovchinnikov S. G.
Заглавие : Measurements of the optical and magneto-optical properties of Fe-Si layer structures at different temperatures
Коллективы : Asian School-Conference on Physics and Technology of Nanostructured Materials, Азиатская школа-конференция по физике и технологии наноструктурированных материалов, Институт автоматики и процессов управления ДВО РАН, Дальневосточный федеральный университет
Место публикации : Fourth Asian school-conference on physics and technology of nanostructured materials (ASCO-NANOMAT 2018): proceedings/ progr. com. S. G. Ovchinnikov [et al.]. - 2018. - Ст.III.24.05p. - P.139. - ISBN 978-5-7444-4368-9
Аннотация: The temperature boundaries of phase stability, stability of surface morphology and optical properties of synthesized iron silicides are determined. In the spectral range 1.5ч3.5 eV, the temperature dependences of the optical and magneto-optical properties of Fe, Fe3Si, β-FeSi2 and Fe5Si3 were measured. A significant effect of Fe and Si impurity atoms on the temperature dependences of the optical properties of iron silicides was observed.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Maximova O. A., Lyashchenko S. A., Shevtsov D. V., Yakovlev I. A., Ovchinnikov S. G.
Заглавие : Development of techniques for processing data from magneto-ellipsometry measurements
Коллективы : Asian School-Conference on Physics and Technology of Nanostructured Materials, Азиатская школа-конференция по физике и технологии наноструктурированных материалов, Институт автоматики и процессов управления ДВО РАН, Дальневосточный федеральный университет
Место публикации : Fourth Asian school-conference on physics and technology of nanostructured materials (ASCO-NANOMAT 2018): proceedings/ progr. com. S. G. Ovchinnikov [et al.]. - 2018. - Ст.IV.25.05p. - P.180. - ISBN 978-5-7444-4368-9
Аннотация: The approach to data processing for layered thin films with a ferromagnet layer is proposed for studying optical and magneto- optical properties. The scope and applicability of models which describe reflective layered structures are studied in order to recommend the best model choice for each case. A significant effect of penetration depth on this choice was observed.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Popkov S. I., Krasikov A. A., Velikanov D. A., Kirillov V. L., Martyanov O. N., Balaev D. A.
Заглавие : Formation of the magnetic subsystems in antiferromagnetic NiO nanoparticles using the data of magnetic measurements in fields up to 250 kOe
Место публикации : J. Magn. Magn. Mater. - 2019. - Vol. 483. - P.21-26. - ISSN 03048853 (ISSN) , DOI 10.1016/j.jmmm.2019.03.004
Примечания : Cited References: 76. - We are grateful S.V. Semenov and A.A. Dubrovskiy for their help, S.V. Komogortsev and A.D. Balaev for fruitful discussions, and M.N. Volochaev for the TEM measurements. The TEM investigations were carried out on the equipment of the Center of Collective Use of the Federal Research Center “Krasnoyarsk Scientific Center, Siberian Branch, Russian Academy of Sciences”.The reported study was funded by Russian Foundation for Basic Research, Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund of Science, to the research project: «Magnetic reversal of magnetic nanoparticles in strong pulsed magnetic fields - a new approach to the study of dynamic effects associated with the magnetization of magnetic nanoparticles» (project no. 18-42-240012).
Ключевые слова (''Своб.индексиров.''): antiferromagnetic nanoparticle--external magnetic field--low temperature regions--magnetic subsystems--magnetically actives--magnetization curves--paramagnetic subsystems--pulsed magnetic fields--magnetic bubbles
Аннотация: It is well-known that the fraction of surface atoms and the number of defects in an antiferromagnetic particle increase with a decrease in the particle size to tens of nanometers, which qualitatively changes the properties of the particle. Specifically, in antiferromagnetic nanoparticles, spins in the ferromagnetically ordered planes can partially decompensate; as a result, an antiferromagnetic particle acquires a magnetic moment. As a rule, uncompensated chemical bonds of the surface atoms significantly weaken the exchange coupling with the antiferromagnetic particle core, which can lead to the formation of an additional magnetic subsystem paramagnetic at high temperatures and spin-glass-like in the low-temperature region. The existence of several magnetic subsystems makes it difficult to interpret the magnetic properties of antiferromagnetic nanoparticles. It is shown by the example of NiO nanoparticles with an average size of 8 nm that the correct determination of the contributions of the magnetic subsystems forming in antiferromagnetic nanoparticles requires magnetic measurements in much stronger external magnetic fields than those commonly used in standard experiments (up to 60–90 kOe). An analysis of the magnetization curves obtained in pulsed magnetic fields up to 250 kOe allows one to establish the contributions of the uncompensated particle magnetic moment μun, paramagnetic subsystem, and antiferromagnetic particle core. The μun value obtained for the investigated NiO particles is consistent with the Néel model, in which μun ∼ N1/2 (N is the number of magnetically active atoms in a particle), and thereby points out the existence of defects on the surface and in the bulk of a particle. It is demonstrated that the anomalous behavior of the high-field susceptibility dM/dH of antiferromagnetic NiO nanoparticles, which was observed by many authors, is caused by the existence of a paramagnetic subsystem, rather than by the superantiferromagnetism effect.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Maximova O. A., Ovchinnikov S. G.
Заглавие : Possibility of using analytical method to calculate magneto-optical parameter from magneto-ellipsometry measurements data
Коллективы : Asian School-Conference on Physics and Technology of Nanostructured Materials, Азиатская школа-конференция по физике и технологии наноструктурированных материалов
Место публикации : The Fifth Asian School-Conference on Physics and Technology of Nanostructured Materials: Proceedings. - VLadivostok: Dalnauka Publishing, 2020. - Ст.IV.31.13p. - P.122. - ISBN 978-5-8044-1698-1
Примечания : This study was supported by the Research Grant No. 075-15-2019-1886 from the Government of the Russian Federation.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Maksimova O. A., Lyashchenko S. A., Ovchinnikov S. G.
Заглавие : How to obtain the dielectric tensor from spectral magneto-optical ellipsometry measurements data
Коллективы : International Online Workshop on the properties of Functional MAX-materials, Институт физики им. Л.В. Киренского Сибирского отделения РАН
Место публикации : 1st FunMAX Workshop 2020: Book of Abstracts/ , Ин-т физики им. Л.В. Киренского. - 2020. - P18
Примечания : Cited References: 6. - This study was supported by the Research Grant No. 075-15-2019-1886 from the Government of the Russian Federation.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Maximova O. A., Lyashchenko S. A., Ovchinnikov S. G.
Заглавие : How to obtain the dielectric tensor from spectral magneto-optical ellipsometry measurements data
Коллективы : International workshop on functional MAX-materials, Kirensky Institute of Physics
Место публикации : International workshop on functional MAX-materials (1st FunMax). - 2020. - P.18
Примечания : Cited references: 6. - This study was supported by the Research Grant No. 075-15-2019-1886 from the Government of the Russian Federation
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Turchin P. P., Turchin V. I., Yurkevich S. V., Sukhodaev P. O., Raikova I. S.
Заглавие : Application of DMA 242 C for quasi-static measurements of piezoelectric properties of solids
Место публикации : J. Sib. Fed. Univ. Math. Phys. - 2020. - Vol. 13, Is. 1. - P.97-103. - ISSN 19971397 (ISSN), DOI 10.17516/1997-1397-2020-13-1-97-103; Журн. СФУ. Матем. и физика
Примечания : Cited References: 26. - The reported study was funded by Russian Foundation for Basic Research project no. 18-42-240016, Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund of Science, to the research project: "Electromechanical Properties and Anisotropy of Acoustic Wave Propagation in Yttrium Aluminoborates Single Crystals"
Аннотация: An experimental device for quasi-static measurements of piezoelectric moduli dijk, based on the possibilities of precision variations in mechanical stresses with the device DMA 242 C in the frequency range 0-100 Hz has been developed. A special sample holder and a charge amplifier are used in the measuring scheme. The measurements of piezoelectric moduli values of trigonal piezoelectric single crystalls La3Ga5SiO14 (P321) and YAl3(BO3)4 (R32), as well as hexagonal ZnO (P63mc) have been carried out.
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