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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Eftifeeva, Anna S., Panchenko, Elena Y., Fatkullin, Ilya D., Volochaev M. N., Tagiltsev, Anton I., Chumlyakov, Yuriy I.
Заглавие : The cyclic stability of superelasticity in aged Ti49.3Ni50.7 single crystals with oxide surface
Место публикации : Metals. - 2022. - Vol. 12, Is. 12. - Ст.2113. - ISSN 20754701 (eISSN), DOI 10.3390/met12122113
Примечания : Cited References: 30. - This research was funded by grant under the Decree of the Government of the Russian Federation No. 220 of 9 April 2010 (Agreement No. 075-15-2021-612 of 4 June 2021)
Аннотация: The cyclic stability of superelasticity in compression in [001]B2-oriented Ti49.3Ni50.7 single crystals is considered in this paper. The crystals were aged at 823 K for 1.0 h in air and helium. It has been experimentally shown that a two-layered surface thin film, consisting of a Ni-free oxide layer and a Ni-rich sublayer, appears after the oxidation at 823 K in air. The surface layers have a weak effect on the forward B2-R-B19’ martensitic transformation temperatures: TR temperature increases by 4 K; Ms and Mf temperatures decrease by 6 K. The oxide layer does not affect either the superelasticity response during fatigue tests or the temperatures of reverse B19’-B2 martensitic transformation. The cracking of the surface oxide layer during fatigue tests was not found in [001]B2-oriented single crystals aged in air. This is contributed by the relaxation of internal stresses. Such internal stresses are caused by both the formation of an oxide layer during aging and the matrix deformation at the stress-induced martensitic transformation. The main relaxation mechanisms of the internal stresses are the oriented growth of Ti3Ni4 precipitation near a thin surface film at aging in air, the formation of dislocations near the precipitation-matrix interface and a fine twinned B19’-martensite at fatigue tests.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Гаврилюк А. П., Исаев, Иван Леонидович, Карпов, Сергей Васильевич, Герасимов, Валерий Сергеевич
Заглавие : Фотостимулированная агрегация электростатически стабилизированных гидрозолей металлов
Место публикации : Инженерная физика. - 2008. - № 6. - С. 18-19. - ISSN 2072-9995
Предметные рубрики:
Аннотация: В работе впервые предложено объяснение причин ускорения (до 105 раз) агрегации электростатически стабилизированных гидрозолей металлов под действием оптического излучения в условиях проявления электронного фотоэффекта. Явление объясняется изменением структуры диффузной частиц двойного электрического слоя в процессе электронной фотоэмиссии из металлического ядра наночастиц и снижением фактора агрегативной устойчивости.In work, explaining reasons of acceleration (to 105 times) of agregation of electrostatic of the stabilized hidrozole metals is first offered under the action of optical radiation in the conditions of display of electronic photoeffect. The phenomenon is explained the change of structure diffuse particles of double electric layer in the process of electronic photoemission from the metal kernel of nanoparticles and by the decline of factor of aggregate stability.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Petrakovskaya E. A., Isakova V. G., Velikanov D. A., Isakov V.
Заглавие : Electron Magnetic Resonance in nanoparticles of 3-d and 5-d metals formation in nanocarbon powders
Коллективы : "Магнитный резонанс для будущего", Международный конгресс, "Euromar", International Conference
Место публикации : EUROMAR 2008 Conference: St.Peterbsburg, 2008, [6-11 July]. - 2008. - p224
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Narkevich N. A., Volochaev M. N., Shulepov I. A., Gomorova Yu. F.
Заглавие : Surface hardening of high-nitrogen austenitic steel by severe deformation–heat treatment
Место публикации : Phys. Metals Metallogr. - 2022. - Vol. 123, Is. 10. - P.1024-1030. - ISSN 0031918X (ISSN), DOI 10.1134/S0031918X22601007. - ISSN 15556190 (eISSN)
Примечания : Cited References: 28. - This work was performed within the state assignment of the Institute of Strength Physics and Materials Science, Siberian Branch, Russian Academy of Sciences (theme no. FWRW-2021-0009)
Аннотация: The structure and mechanical properties of austenitic high-nitrogen steel (16.5 Cr, 18.8 Mn, 0.07 C, 0.53 N, 0.52 wt % Si, Fe for balance) have been investigated after severe deformation–heat treatment, which has involved shock surface forging at the ultrasonic frequency (USF) and electron-beam heat treatment (EBT). A subgrain structure hardened by CrN nanoparticles has been shown to form in the surface layer as a result of deformation–heat treatment. No discontinuous decomposition of austenite with the formation of Cr2N nitrides takes place. This structure modification in the surface layer enhances the strength properties of the steel, namely, σ0.2 increases to 712 MPa and σu to 923 MPa at a plasticity of 25%. The yield strength increases by 50% compared to the state after quenching.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Aleksandrovsky A. S., Zaitsev A. I., Shakhura I. E. , Zamkov A. V., Vyunishev A. M.
Заглавие : Random quasi-phase-matching in a nonlinear photonic crystal structure of strontium tetraborate
Место публикации : Phys. Rev. A. - 2008. - Vol. 78, Is. 3. - Ст.031802. - ISSN 1050-2947, DOI 10.1103/PhysRevA.78.031802
Примечания : Cited Reference Count: 20. - Гранты: This work was supported by RFBR Grant No. 02-0700497, Grants of the President of the Russian Federation for the support of leading scientific schools (No. SS-1011.2008.2 and No. SS-3818.2008.3), Grant No. RNP.2.1.1.1814, and the Interdisciplinary Integration project of SB RAS 33.Финансирующая организация: RFBR [02-0700497]; Russian Federation [SS-1011.2008.2, SS-3818.2008.3, RNP.2.1.1.1814]; SB RAS 33
Предметные рубрики: HARMONIC-GENERATION
DOMAIN-STRUCTURE
Ключевые слова (''Своб.индексиров.''): alkaline earth metals--crystal atomic structure--experiments--harmonic generation--photonic crystals--powders--random processes--strontium--angular dependences--enhancement factors--near ultraviolet--photonic crystal structures--quasi phase-matching--second-harmonic generation--spectral dependences--tetra borate--crystal structure
Аннотация: Random quasi-phase-matching (RQPM) of the second-harmonic generation process is investigated experimentally and theoretically in a strongly randomized spontaneously grown nonlinear photonic crystal structure of strontium tetraborate. The thickness of domains in the structure is measured and employed in calculations of angular and spectral dependences of random quasi-phase-matching. Despite the great scale of randomness, the RQPM effect is preserved. The calculated enhancement factor due to RQPM is in excellent agreement with experiment, and good agreement between calculations and experiment is obtained for the shape of the angular dependence of RQPM. The calculated spectral dependence of RQPM consists of a number of narrow peaks, and a maximum enhancement factor is attained in the near ultraviolet. The band structure of randomized nonlinear photonic crystal is calculated.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Tomilin F. N., Shubin A. A., Kozak V. V., Ivanova D. A., Fedorova N. A., Ol’shevskaya Y. S., Kovaleva A. V., Avramov P. V., Ovchinnikov S. G.
Заглавие : Effect of substitution on magnetic moments of iron and chromium atoms in MAX phases of type (Cr4 – xFex)0.5SiC: Theoretical calculation
Место публикации : Phys. Met. Metallogr. - 2022. - Vol. 123, Is. 7. - P.640-644. - ISSN 0031918X (ISSN), DOI 10.1134/S0031918X22070195
Примечания : Cited References: 25. - The study is supported by the Russian Science Foundation (project no. 21-12-00226) and by the Interagency Supercomputer Center of the Russian Academy of Sciences (MVS-100K and MVS-10P)
Аннотация: MAX phases are a family of ternary layered compounds with formal stoichiometry M2AX and have a layered hexagonal structure. Calculations with the B3LYP density functional show that, by varying the ratio between the chromium and iron in the MAX phase (Cr4 – xFex)0.5SiC, it is possible to change the lattice parameters and the magnetic moment on metal atoms. In this phase, a partial substitution of one metal for the other can be considered a technique of intended variation of their magnetic properties.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Гаврилюк А.П., Исаев И.Л., Карпов С.В., Герасимов, Валерий Сергеевич
Заглавие : Электростатические взаимодействия наночастиц с двойным электрическим слоем в золях металлов: исследования методом броуновской динамики
Место публикации : Инженерная физика. - 2008. - № 6. - С. 14-17. - ISSN 2072-9995
Предметные рубрики:
Аннотация: Методом численного моделирования решается важная методическая задача, состоящая в проверке степени адекватности классической теории Дерягина-Ландау-Фервея-Овербека (ДЛФО) электростатического взаимодействия двух наночастиц в лиозолях металлов. Исследуется зависимость от межчастичного расстояния энергии электростатического взаимодействия двух контактирующих наночастиц с перекрывающимися двойными электрическими слоями, образованным ионами электролита, в процессе контакта этих слоев. Проводится сравнение результатов с полученными с помощью теории ДЛФО.An important methodical task, co-standing in verification of degree of adequacy of classic theory of Deryagina-Landau-Ferveya-Overbeka (DLFO) of electrostatic co-operation of two nano particles in liozol of metals, decides in working as the method of numeral design. Dependence is explored on interpartial distance of energy of electrostatic co-operation of two contacting nano particles with the blocked double electric layers, formed the ions of electrolyte, in the process of contact of these layers. A comparison of results with DLFO got by a theory is made.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Гаврилюк А.П., Исаев, Иван Леонидович, Карпов, Сергей Васильевич, Герасимов, Валерий Сергеевич
Заглавие : Применение метода броуновской динамики для исследования формирования двойного электрического слоя наночастиц в гидрозолях металлов
Место публикации : Инженерная физика. - 2008. - № 4. - С. 70-72. - ISSN 2072-9995
Предметные рубрики:
Аннотация: Впервые методом броуновской динамики исследуется образование двойного электрического слоя наночастиц гидрозолей металлов при адсорбции ионов электролита из окружающей среды с целью сопоставления с классическими теориями Штерна, Гуи-Чэпмена, Гельмгольца. При этом исследуется влияние на структуру слоя кулоновских сил, включая и силы изображения, ван-дер-ваальсовых, диссипативных и случайных сил, а также степени гидратации адсорбируемых ионов. Полученные результаты позволяют уточнить форму потенциала межчастичного взаимодействия в данном типе золей - одного из фундаментальных параметров, определяющих процесс структурообразования в дисперсных системах с электростатическим механизмом стабилизации.For the first time the method of Brown dynamics investigates formation of a double electric layer nanoparticles hidrozole metals at adsorption of ions of electrolit from an environment with the purpose of comparison to Stern's, Gui-Chepmen's and Gelmgolt's theories. Thus influence on structure of a layer Kulon's forsec, including and forces of the image, Van der Vals's, and casual forces, and also a degree of hydration of adsorbed ions is investigated. The received results allow to specify the form of potential of interpartial interaction in the given type ofzole - one of the fundamental parameters defining process of structurization in disperse systems with the electrostatic mechanism of stabilization.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Narkevich N., Vlasov I., Volochaev M. N., Gomorova Y., Mironov Y., Panin S., Berto F., Maksimov P., Deryugin E.
Заглавие : Low-temperature deformation and fracture of Cr-Mn-N stainless steel: Tensile and impact bending tests
Место публикации : Metals. - 2023. - Vol. 13, Is. 1. - Ст.95. - ISSN 20754701 (eISSN), DOI 10.3390/met13010095
Примечания : Cited References: 41. - The research was funded by RSF, project No. 22-29-00438. The low-temperature tensile tests were carried out in accordance with the state assignment for the ISPMS SB RAS, project No. FWRW-2021-0009
Аннотация: The paper presents the results of tensile and impact bending tests of 17%Cr-19%Mn-0.53%N high-nitrogen austenitic stainless steel in temperatures ranging from −196 to 20 °C. The steel microstructure and fracture surfaces were investigated using transmission and scanning electron microscopes, as well as X-ray diffraction analysis. The steel experiences a ductile-to-brittle transition (DBT); however, it possessed high tensile and impact strength characteristics, as well as the ductile fracture behavior at temperatures down to −114 °C. The correspondence between γ–ε microstructure and fracture surface morphologies was revealed after the tensile test at the temperature of −196 °C. In this case, the transgranular brittle and layered fracture surface was induced by ε-martensite formation. Under the impact bending test at −196 °C, the brittle intergranular fracture occurred at the elastic deflection stage without significant plastic strains, which preceded a failure due to the high internal stresses localized at the boundaries of the austenite grains. The stresses were induced by: (i) segregation of nitrogen atoms at the grain boundaries and in the near-boundary regions, (ii) quenching stresses, and (iii) reducing fcc lattice volume with the test temperature decrease and incorporation of nitrogen atoms into fcc austenite lattice. Anisotropy of residual stresses was revealed. This was manifested in the localization of elastic deformations of the fcc lattice and, consequently, the stress localization in 100-oriented grains; this is suggested to be the reason of brittle cleavage fracture.
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Orlov V. A., Rudenko R. Yu., Luk'yanenko A. V., Yakovchuk V. Yu., Komarov V. A., Prokopenko V. S., Orlova I. N.
Заглавие : Features of the magnetic state of an ordered array of ferromagnetic ribbons
Место публикации : Phys. Met. Metallogr. - 2023. - Vol. 124, Is. 2. - P.109-117. - ISSN 0031918X (ISSN), DOI 10.1134/S0031918X22601780. - ISSN 15556190 (eISSN)
Примечания : Cited References: 35. - In the part of sample preparations, this study was supported by the Russian Foundation for Basic Research within research project no. 20-02-00696. The magnetic measurements and theoretical calculations were performed within the framework of State assignment from the Ministry of Science and Higher Education of the Russian Federation (topic no. FSRZ-2020-0011)
Аннотация: The features of the magnetic state of an array of parallel oriented permalloy ribbons are discussed. The arrays are made by explosive lithography. The ribbons have a thickness of 180 nm, a width of 2.8 µm, and a length of about 4 mm. The distance between ribbons in different samples varies in the range from 300 nm to 4 μm. It is found that the ribbons in the regions far from the end faces are in a single-domain state with small-angle ripples, the magnetization distribution of which correlates with inhomogeneities of the ribbon side surfaces. Moreover, there is a distinct relationship in the spatial distribution of the ripples between adjacent ribbons with a relatively small distance between them. This makes it possible to evaluate the role of the magnetostatic coupling of magnetic subsystems of array elements and to estimate the characteristic value of the random stray field that pins the magnetization.
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11.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Stolyar S. V., Li O. A., Nikolaeva E. D., Vorotynov A. M., Velikanov D. A., Knyazev Yu. V., Bayukov O. A., Iskhakov R. S., P’yankov V. F., Volochaev M. N.
Заглавие : An effective method of magnetic hyperthermia based on the ferromagnetic resonance phenomenon
Место публикации : Phys. Met. Metallogr. - 2023. - Vol. 124, Is. 2. - P.174-180. - ISSN 0031918X (ISSN), DOI 10.1134/S0031918X22601834. - ISSN 15556190 (eISSN)
Примечания : Cited References: 15. - This study was supported by grant no. 22-14-20020 from the Russian Science Foundation and the Krasnoyarsk Regional Fund for Support of Scientific and Technological Activities. The authors are grateful to the Krasnoyarsk Regional Center for Collective Use at Federal Research Center Krasnoyarsk Scientific Center, Siberian Branch, Russian Academy of Sciences, for providing their research facilities
Аннотация: Nickel and cobalt ferrite nanoparticles have been synthesized using the chemical precipitation method; the nanoparticle sizes were found to be 63 ± 22 and 26 ± 4 nm, respectively. The static hysteresis loops and Mossbauer spectra have been measured. It is shown that cobalt ferrite powders are magnetically harder than nickel ferrite powders. Ferromagnetic resonance (FMR) curves have been studied. It is found that the FMR absorption for cobalt ferrite is observed at room temperature and above. The time dependences of the nanoparticle warm-up under FMR conditions have been measured. The maximum temperature changes for nickel ferrite and cobalt ferrite particles are 8 and 11 K, respectively. Using the example of cobalt ferrite powder, the possibility of effectively heating of particles in the FMR mode in their own field without using a DC magnetic field source is shown. The observed effect can be used in magnetic hyperthermia.
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12.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Bayukov O. A., Balaev A. D., Petrov M. I., Anshits A. G., Sharonova O. M., Rabchevskii E. V.
Заглавие : Mossbauer and magnetic study of microspheres extracted from fly ashes of power stations
Место публикации : The Physics of Metals and Metallography. - 2006. - Т. 102, SUPPL. 1. - ISSN 0031-918X, DOI 10.1134/S0031918X06140134. - ISSN 1531-8672(eissn)
ГРНТИ : 29.19
MeSH-главная:
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13.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Volkova I. R., Tyryshkina L. E., Volochaev M. N., Zaloga A. N., Shabanova K. A., Ovchinnikov A. V., Lyamkin A. I.
Заглавие : The effect of aluminum-oxide powders on the structure and properties of copper electrodeposited composite coatings
Место публикации : Prot. Met. Phys. Chem. Surf. - 2023. - Vol. 59, Is. 1. - P.71-75. - ISSN 20702051 (ISSN), DOI 10.1134/S2070205122700022. - ISSN 2070206X (eISSN)
Примечания : Cited References: 9
Аннотация: Copper electrodeposited composite coatings containing two types of aluminum-oxide powders with different dispersities (alumina Al2O3-1 and electroexplosive aluminum-oxide nanopowder Al2O3-2) are obtained during the work. The studies show that introducing the powders leads to a change in the microstructure of the composites and a change in the grain growth principles during the formation of the coatings. Refinement and ordering of the grain structure of the coatings occurs and twinning defects and texture are formed. The change in the formation of the microstructure of the composites leads to a change in some operational characteristics: an increase in the microhardness (by 10% in the composites with the addition of alumina and by more than 30% in the coatings with electroexplosive aluminum oxide) and ultimate tensile strength (by 20% in the composites with Al2O3-1 and almost 1.5-fold in the samples with Al2O3-2).
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14.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Vazhenina I. G., Iskhakov R. S., Yakovchuk V. Yu.
Заглавие : Characteristics of angular dependences of parameters of ferromagnetic and spin-wave resonance spectra of magnetic films
Место публикации : Phys. Met. Metallogr. - 2022. - Vol. 123, Is. 11. - P.1084-1090. - ISSN 0031918X (ISSN), DOI 10.1134/S0031918X2260124X. - ISSN 15556190 (eISSN)
Примечания : Cited References: 36
Аннотация: This paper presents the results of measuring the main parameters of the ferromagnetic and spin-wave resonance spectra (resonant field, linewidth, and intensity) of single-layer permalloy films at various angles in the out-of-plane orientation. The effect of the type of surface conditions on the angular dependence of the intensity ratio of adjacent modes is studied. A correspondence is established between the angle of the applied constant magnetic field with respect to the normal to the film and the change in the oscillation type from uniform to nonuniform. The revealed features of the angular dependences of the resonant field and the intensity of the spectral peak can be successfully used in the identification of microwave spectra. The fundamental magnetic parameters (effective magnetization, exchange interaction constant, surface anisotropy constant, and perpendicular anisotropy field) were determined.
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15.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Dubrovskiy A. A., Knyazev Yu. V., Gerasimova Yu. V., Udovenko A. A., Laptash N. M.
Заглавие : Influence of the Jahn-Teller effect on magnetic anisotropy in single crystals of fluorine hexahydrates of transition metals
Место публикации : Phys. Solid State. - 2022. - Vol. 64, Is. 11. - P.1709-1712. - ISSN 10637834 (ISSN), DOI 10.21883/PSS.2022.11.54194.406. - ISSN 10906460 (eISSN)
Примечания : Cited References: 16. - The work was done with financial support from the Russian Foundation for Basic Research, Government of Krasnoyarsk Krai and the Krasnoyarsk Krai Foundation of Science within the research project No. 20-42-240014
Аннотация: The magnetic properties of fluorine hexahydrates of transition metals have been studied. It was found that the presence of spin-orbit interaction of the transition metal ion has a significant effect on anisotropy of magnetic properties. Depending on the direction of interaction of the orbital magnetic moment of a transition metal cation with a crystal field easy direction of magnetization changes from the crystallographic b-axis to the c-axis.
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16.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Moshkina E. M., Seryotkin, Yurii, Bayukov O. A., Molokeev M. S., Kokh, Dieter, Smorodina, Ekaterina, Krylov A. S., Bezmaternykh L. N.
Заглавие : Flux growth and phase diversity of the triple oxides of transition metals (Mn,Fe,Ga)2O3 in multicomponent fluxes based on Bi2O3–MoO3–B2O3–Na2O
Колич.характеристики :11 с
Место публикации : CrystEngComm. - 2023. - Vol. 25, Is. 18. - P.2824-2834. - ISSN 14668033 (eISSN), DOI 10.1039/D3CE00147D
Примечания : Cited References: 38. - The study was supported by the Russian Science Foundation (grant no. 21-72-00130)
Аннотация: To determine the mutual influence of the solvent and soluble in multicomponent fluxes based on Bi2O3–MoO3–B2O3–Na2O, the crystallization of the triple oxides of the transition metals (Mn,Fe,Ga)2O3 is investigated, namely the phases based on orthorhombic FeGaO3 and bixbyite FeMnO3. Simultaneously, a set of fluxes is studied based on the variation in the component ratio with regard to the solvent and soluble. The crucial role of various components of the flux system is considered at the intersection of the phase boundaries. Fluxes for the stable growth of (Mn,Fe,Ga)2O3 single crystals of the studied phases (based on orthorhombic FeGaO3 and bixbyite FeMnO3) are determined. A set of single crystal samples (9 samples) with different Fe/Mn/Ga ratios is obtained. The actual composition of the samples is studied using the EDX technique. The partition coefficients of Fe2O3, Mn2O3 and Ga2O3 in the studied fluxes are analyzed. The structure of the obtained samples is characterized using X-ray diffraction methods, including the phase composition, space group and lattice parameters. The room temperature Raman spectra of the obtained samples are presented. The distribution of iron cations over the crystal positions in the obtained phases is studied using Mossbauer spectroscopy.
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17.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mikhailov A. G., Vashlaev I. I., Morozov E. V.
Заглавие : Mass transfer of base metals in upward penetration of solutions in tailing dumps
Место публикации : J. Min. Sci. - 2022. - Vol. 58, Is. 6. - P.1033-1039. - ISSN 10627391 (ISSN), DOI 10.1134/S1062739122060187. - ISSN 15738736 (eISSN)
Примечания : Cited References: 20. - This study was performed within the State Assignment of the Institute of Chemistry and Chemical Technology, SB RAS, project no. 0287-2021-0014 using the equipment provided by Krasnoyarsk Regional Center for Collective Use, FRC KSC SB RAS
Аннотация: The article describes the studies into the process of upward mass transfer in flotation tailings with water solutions. The swift-flowing geological process is investigated using the magnetic resonance imaging. The kinetics of water-soluble minerals as well as the structure and substance transformations in the body of tailings are studied for substantiating in-situ formation of the target concentration zones at the tailings surface.
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18.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Sinyakova E. F., Vasilyeva I. G., Oreshonkov A. S., Goryainov S. V., Karmanov N. S.
Заглавие : Formation of noble metal phases (Pt, Pd, Rh, Ru, Ir, Au, Ag) in the process of fractional crystallization of the CuFeS2 melt
Место публикации : Minerals. - 2022. - Vol. 12, Is. 9. - Ст.1136. - ISSN 2075163X (ISSN), DOI 10.3390/min12091136
Примечания : Cited References: 61. - This work was supported by the Russian Federation state assignment of Sobolev Institute of Geology and Mineralogy of SB RAS, Nikolaev Institute of Inorganic Chemistry SB RAS, and Kirensky Institute of Physics of Federal Research Center KSC SB RAS. The grant number is projects II.1.64. and 40330-2016-0001
Аннотация: The quasi-equilibrium directional crystallization of the melt composition (at. %): Cu 24.998, Fe 25.001, S 49.983, with Ag 0.002, Pd 0.003, Ru 0.004, Rh 0.006, and Au, Pt, Ir (each as 0.001) was carried out. The crystallized cylindrical ingot consisted of two primary zones and three secondary zones with different chemical and phase compositions. The compositions of the primary zones corresponded to high-temperature intermediate solid solution (zone I) and liquid enriched in sulfur (zone II). The compositions of the secondary zones corresponded to low-temperature intermediate solid solution and chalcopyrite (zone Ia), the same intermediate solid solution with chalcopyrite and bornite (zone Ib), and again with bornite, chalcocite, and idaite (zone II). We plotted the distribution curves of Fe, Cu, and S along the ingot, calculated the distribution coefficients of the components during directional crystallization, and clearly showed that, from the initial stoichiometric composition CuFeS2, the intermediate solid solution enriched in Fe and depleted in S is crystallized. Based on the data of directional crystallization and thermal analysis, a cross section was constructed in the intermediate solid solution-sulfide melt region of the Cu-Fe-S system. With solubility in the solid Cu-Fe sulfides lying below detection limit of scanning electron microscopy/energy-dispersive X-ray spectrometry (SEM/EDS), noble elements occurred as individual phases of a size more often <10 µm. They were identified as Ag, RuS2, PdS, Au* (an Au based alloy), (Rh, Ir, Ru)3S8, (Rh, Ir)3S8, Rh3S8, and (Cu, Fe)~2(Pt, Rh)1S~5 phases by electron microprobe. Based on ab initio calculations of crystal structure, electronic band structure, and lattice dynamics of idealized laurite RuS2 phase and the idealized Ir3S8, Rh3S8, and Ru3S8 phases, the interpretation of Raman spectrum of the cation-mixed (Ru, Rh, Ir)S2 sulfide was presented for the first time.
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19.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Edel'man I. S.
Заглавие : Magneto-optics of ferromagnetic metals nanoparticles fabricated by ion implantation in dielectric matrix
Коллективы : International Conference Functional Materials
Место публикации : International Conference Functional Materials (ICFM-2011): Book of abstracts. - 2011. - С. 163
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20.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Iskhakov R.S., Komogortsev S.V.
Заглавие : Magnetic microstructure of amorphous, nanocrystalline, and nanophase ferromagnets
Место публикации : Phys. Metals Metallogr. - 2011. - Vol. 112, Is. 7. - С. 666-681. - DEC. - ISSN 0031-918X, DOI 10.1134/S0031918X11070064
Примечания : Cited Reference Count: 40. - Federal Program Development of the Scientific Potential of Higher Education [RNP. 2.1.1/11470], This work was supported in part by the Federal Program Development of the Scientific Potential of Higher Education ( project no. RNP. 2.1.1/11470), Federal Target Program Research and Research-Pedogogical Personnel of Innovative Russia for 2009-2014.
Предметные рубрики: Metallurgy & Metallurgical Engineering
Аннотация: The magnetic microstructure of nanostructured ferromagnets is represented by an ensemble of stochastic magnetic domains-regions with dimensions of the length of magnetic orientation coherency. It is shown that the curves displaying the approach of magnetization to saturation make it possible to determine the dimension of the element of the micromagnetic structure, i.e., the size of the stochastic domain and the constant of the effective anisotropy in this element, the size of the element of the nanostructure and the constant its local anisotropy, as well as the dimensionality of the exchange-coupled ferromagnetic nanoparticles.
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