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Вид документа : Статья из сборника (выпуск продолж. издания)
Шифр издания :
Автор(ы) : Mironov V. L., Kosolapova L. G., Lukin Y. I., Karavaysky A. Yu., Molostov I. P.
Заглавие : A dielectric model at a frequency of 1.4GHz for frozen mineral soils in the temperature range −1 to −30°C
Коллективы : Progress in Electromagnetics Research Symposium
Место публикации : Progr. Electromag. Res. Symp. (PIERS): Proceedings. - 2016. - P.2518-2522. - , DOI 10.1109/PIERS.2016.7735031
Примечания : References: 5. - The study was supported by a grant from the Russian Foundation for Basic Research (project No. 16-05-00572)
Аннотация: A single-frequency dielectric model at 1.4 GHz for frozen mineral soils was developed, with the temperature and clay content varying from -1 to -30°C and 9.1 to 41.3%, respectively. The model is based on dielectric measurements of three typical soils (sandy loam, silt loam, and silty clay) collected in the Yamal peninsular. The refractive mixing model was applied to fit the data aggregates consisting of measured complex refractive indexes (CRI) for the three soils as a function of soil moisture at a fixed temperature. As a result, there were derived the parameters of the refractive mixing dielectric model as a function of temperature and texture. These parameters involve the maximum allowed gravimetric fraction of bound water and the CRIs of soil solids, bound soil water, and free soil water components, the latter being represented by capillary ice. The error of the dielectric model was evaluated by correlating the predicted complex relative permittivity (CRP) values of the soil samples with the measured ones. The coefficient of determination, R2, and the root mean square error, RMSE, were estimated to be R2 = 0.994, RMSE = 0.22 and R2 = 0.988, RMSE = 0.07 for the real and imaginary parts of the CRP, respectively. These values are on the order of the dielectric measurement error itself. The proposed dielectric model can be applied in active and passive remote sensing techniques used in the Arctic areas, mainly for the SMOS, SMAP and Aquarius missions.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Grishina, Svetlana, Kodera, Peter, Goryainov, Sergey, Oreshonkov A. S., Seryotkin, Yurii, Simko, Frantisek, Polozov, Alexander G.
Заглавие : Application of Raman spectroscopy for identification of rinneite (K3NaFeCl6) in inclusions in minerals
Коллективы : Russian Foundation for Basic ResearchRussian Foundation for Basic Research (RFBR) [18-05-00682]; European Regional Development FundEuropean Union (EU) [ITMS 26240220086]; Vedecka Grantova Agentura MSVVaS SR a SAV [1/0313/20]
Место публикации : J. Raman Spectrosc. - 2020. - Vol. 51, Is. 12. - P.2505-2516. - ISSN 0377-0486, DOI 10.1002/jrs.6005. - ISSN 1097-4555(eISSN)
Примечания : Cited References: 55. - Russian Foundation for Basic Research, Grant/Award Numbers: 18-05-00682, 18-05-00682; European Regional Development Fund, Grant/Award Number: ITMS 26240220086; Vedecka Grantova Agentura MSVVaS SR a SAV, Grant/Award Number: 1/0313/20
Предметные рубрики: SALT MELT
IRON
DEPOSIT
FLUIDS
TRANSFORMATIONS
FERRIHYDRITE
Аннотация: Solid daughter phases in fluid and salt melt inclusions in minerals provide important clues to characterization of mineral‐forming processes. The analysis of the fluid inclusions often requires the exposure of the daughter minerals. Rinneite (K3NaFeCl6), which is a hygroscopic mineral, decomposes in air and cannot thus be identified by conventional methods. A combined approach has been applied for investigation of synthetic and natural rinneite to acquire its diagnostic Raman spectrum for a nondestructive identification. We used natural rinneite inclusions in halite, suitable for applying a complex of methods, to clear up the reference spectrum. Improved high‐resolution X‐ray diffraction (XRD) data obtained from natural rinneite inclusion are comparable with that of previously published, with similar unit cell dimensions. Polarized Raman spectra of natural inclusions were obtained using different geometries and polarization of the incident and scattered light. Interpretation of experimental Raman spectra was performed within the framework of lattice dynamics simulations and group analysis. Individual spectral bands are interpreted in terms of Raman‐active vibrational modes of K3NaFeCl6 structural units. Raman spectrum of synthetic rinneite with main peaks at 75, 91, 103, 143, 167, 171, 187, and 239 cm−1 agrees well with the spectra of rinneite inclusions in halite from the Nepa potash deposit and rinneite daughter minerals in salt melt inclusions hosted by quartz veinlets from the porphyry gold systems in the Central Slovakia Volcanic Field. This provides a firm basis for any future identification of this mineral worldwide, using nondestructive Raman spectroscopy.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Bataleva, Yu. V., Palyanov, Yu. N., Borzdov, Yu. M., Bayukov O. A., Sobolev N. V.
Заглавие : Conditions for diamond and graphite formation from iron carbide at the P-T parameters of lithospheric mantle
Коллективы : Russian Science Foundation [14-27-00054]
Место публикации : Russ. Geol. Geophys.: Elsevier Science, 2016. - Vol. 57, Is. 1: Tectonics, geodynamics, and petrology of earth’s lithosphere and mantle (to the 80th birthday of Academician Nikolai Leontievich Dobretsov). - P.176-189. - ISSN 1068-7971, DOI 10.1016/j.rgg.2016.01.012. - ISSN 1878-030X(eISSN)
Примечания : Cited References:55. - This work was supported by the Russian Science Foundation under Grant No. 14-27-00054.
Предметные рубрики: DEEP CARBON-CYCLE
EARTHS MANTLE
MINERAL INCLUSIONS
HIGH-PRESSURE
KOKCHETAV MASSI
SUBDUCTION ZONES
REDOX BUDGET
FERRIC IRON
MOSSBAUER
METAL
Ключевые слова (''Своб.индексиров.''): iron carbide--wusite--graphite--diamond--oxides--olivine--subduction--redox interaction--lithospheric mantle--high-pressure experiment
Аннотация: To estimate conditions for the stability of iron carbide under oxidation conditions and to assess the possibility of formation of elemental carbon by interaction between iron carbide and oxides, experimental modeling of redox interaction in the systems Fe3C-Fe2O3 and Fe3C-Fe2O3-MgO-SiO2 was carried out on a split-sphere high-pressure multianvil apparatus at 6.3 GPa and 900-1600 degrees C for 18-20 h. During carbide-oxide interaction in the system Fe3C-Fe2O3, graphite crystallizes in assemblage with Fe3+-containing wusite. Graphite forms from carbide carbon mainly by cohenite oxidation: Fe3C + 3Fe(2)O(3) - 9FeO + C-0 and FeO + Fe3C - (Fe2+, Fe3+)O + C-0. At above-solidus temperatures (= 1400 degrees C), when metal-carbon melt is oxidized by wusite, graphite and diamond crystallize by the redox mechanism and form the Fe3+-containing wstite + graphite/diamond assemblage. Interaction in the system Fe3C-Fe2O3-MgO-SiO2 results in the formation of Fe3+-containing mannesiowusite-olivine-graphite assemblage. At = 1500 degrees C, two melts with contrasting f(O2) values are generated: metal-carbon and silicate-oxide; their redox interaction leads to graphite crystallization and diamond growth. Under oxidation conditions, iron carbide is unstable in the presence of iron, silicon, and magnesium oxides, even at low temperatures. Iron carbide-oxide interaction at the mantle temperatures and pressures leads to the formation of elemental carbon; graphite is produced from carbide carbon mainly by redox reactions of cohenite (or metal-carbon melt) with Fe2O3 and FeO as well as by interaction between metal-carbon and silicate-oxide melts. The results obtained suggest that cohenite can be a potential source of carbon during graphite (diamond) formation in the lithospheric mantle and the interaction of iron carbide with iron, silicon, and magnesium oxides, during which carbon is extracted can be regarded as a process of the global carbon cycle. (C) 2016, V.S. Sobolev IGM, Siberian Branch of the RAS. Published by Elsevier B.V. All rights reserved.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Fomin S. V., Muzalevskiy K. V.
Заглавие : A dielectric model for frozen mineral soils at a frequency of 435 MHz
Место публикации : Remote Sens. Lett. - 2021. - Vol. 12, Is. 9. - P.944-950. - ISSN 2150704X (ISSN), DOI 10.1080/2150704X.2021.1947537
Примечания : Cited References: 16. - This work was supported by the state assignment of the Ministry of Science and Higher Education of the Russian Federation [project No. 0287-2021-0034]
Аннотация: A single frequency refractive mixing dielectric model at 435 MHz for frozen mineral soils is proposed. The model was created based on the laboratory dielectric measurements of three soil samples in the ranges of soil moisture from 0.01cm3 cm−3 to 0.42cm3 cm−3, temperature from– 30°C to– 1°C, clay content (by weight) from 9.1% to 41.3%. Coefficient of determination R2 and root mean square error (RMSE) predicted by the model and measured values for real () and imaginary () part of the complex relative permittivity (CRP) are = 0.988 (= 0.323) and = 0.987 (= 0.100). Compared to well-known spectroscopic models, this model is simpler in practical engineering use. The input parameters of the model are the volumetric soil moisture, temperature and the content of the clay fraction. The output parameters are the real and imaginary parts of the CRP. The created model may be used to develop new remote sensing retrieval algorithms of temperature, the content of unfrozen water and ice in the root zone of frozen soils for northern regions.ε 'ε ''R2ε 'RMSEε 'R2ε ''RMSEε ''
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Fomin S. V., Muzalevskiy K. V.
Заглавие : Dielectric Model for Thawed Mineral Soils at a Frequency of 435 MHz
Место публикации : IEEE Geosci. Remote Sens. Lett. - 2021. - Vol. 18, Is. 2. - P.222-225. - ISSN 1545-598X (ISSN), DOI 10.1109/LGRS.2020.2972559. - ISSN 1558-0571 (eISSN)
Примечания : Cited References: 20. - This work was supported by the Program of SB RAS, project №0356-2019-0004
Аннотация: A single-frequency dielectric model at 435 MHz for mineral soils is proposed. The dielectric model was created on the basis of the laboratory dielectric measurements of three soil samples with clay content in the range of 9.1%-41.3%. The input parameters of the dielectric model are volumetric soil moisture and clay content. The output parameter of the dielectric model is complex permittivity (CP). The model prediction errors are comparable with the errors of instrumental measurements of the CP for refractive index and normalized attenuation 0.1-0.3 and 0.06-0.12, respectively, in terms of root-mean-square error (RMSE). The comparative analysis of dielectric predictions in the case of the developed model proved to obtain a better accuracy than the existing dielectric models. The created model may be recommended for practical use in the algorithms of soil-moisture retrieval in the P-band.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Mironov V. L., Molostov I. P., Lukin Y. I., Karavaysky A. Yu., Fomin S. V.
Заглавие : Frequency-, temperature-, and texture-dependent dielectric model for frozen and thawed arctic mineral soi
Коллективы : Progress in Electromagnetics Research Symposium
Место публикации : Progr. Electromag. Res. Symp. (PIERS): Proceedings. - 2017. - P.2546-2553. - DOI 10.1109/PIERS.2017.8262181
Примечания : Cited References: 15. - Present research was supported in the frame of project No. 16-45-242162 in the corporative program of the Russian foundation for basic research and Krasnoyarsk region government foundation for science and technology. It was also supported by the RAS Presidium Program “Arctika”, 2015– 2017 and program II.12.1. of the SB RAS basic researches.
Аннотация: A simple single-frequency dielectric model for the set of frequencies which are 0.45, 1.26, 1.4, 1.6, 5.4, 6.9, 9.6, and 10.7 GHz for frozen mineral soils is developed. The model is based on the dielectric measurements of three typical soils (sandy loam, silt loam, and silty clay) at the temperature range from -1°C to -30°C. The measured data as a function of moisture were fitted with the refractive mixing dielectric model. The model parameters are maximum bound water fraction, and refractive indexes of soil solid, unfrozen bound water, and wet ice. In the result of fitting measured data, the model parameters were determined as a functions of soil type (clay content), and soil temperature. The error of the predicted values of the complex relative permittivity (CRP) of frozen soils relative to the measured ones was evaluated through determination coefficients, and root mean square error (RMSE). The values of RMSE are on the order of the dielectric measurement error itself. The proposed dielectric model can be applied in active and passive remote sensing techniques used in the cold regions.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Golovnev N. N., Vasil'ev A. D.
Заглавие : Structure of two new compounds of fluoroquinolone antibiotics with mineral acids
Место публикации : Russ. J. Inorg. Chem.: Maik Nauka-Interperiodica Publishing, 2016. - Vol. 61, Is. 11. - P.1419-1422. - ISSN 00360236 (ISSN), DOI 10.1134/S0036023616110073
Примечания : Cited References: 19
Ключевые слова (''Своб.индексиров.''): single crystals--x ray diffraction--crystallographic data--fluoroquinolone antibiotics--intra- and intermolecular hydrogen bonds--levofloxacin--mineral acid--pi interactions--space groups--sparfloxacin--hydrogen bonds
Аннотация: New compounds of sparfloxacin (C19H22F2N4O3, SfH) and levofloxacin (C18H20FN3O4, LevoH) with mineral acids, namely, sparfloxacinium bromide (SfH · HBr, I) and levofloxacindium diperchlorate (LevoH · 2HClO4, II), have been synthesized and characterized by X-ray diffraction. Crystallographic data are a = 7.7151(7) Å, , b = 26.109(3) Å,с = 10.008(1) Å, β = 103.556(1)°, V = 1959.7(3) Å3, space group P21/n, Z = 4 for I and a = 9.727(6) Å, b = 20.440(12) Å, с = 12.286(7) Å, β = 104.327(8)°, V = 2367(2)Å3, space group P21, Z = 4 for II. The structures of these compounds are stabilized by intra- and intermolecular hydrogen bonds and π–π interaction between SfH2 + or LevoH3 2+ ions. © 2016, Pleiades Publishing, Ltd.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Grishina S., Kodera P., Uriarte L. M., Dubessy J., Oreshonkov A. S., Goryainov S., Simko F., Yakovlev I., Roginskii E. M.
Заглавие : Identification of anhydrous CaCl2 and KCaCl3 in natural inclusions by Raman spectroscopy
Место публикации : Chem. Geol. - 2018. - Vol. 493. - P.532-543. - ISSN 00092541 (ISSN), DOI 10.1016/j.chemgeo.2018.07.017
Примечания : Cited References: 52. - The manuscript was greatly benefited from revisions of Dr. Matthew Steele-MacInnis and anonymous Reviewer. The authors are grateful to Dr. Sharigin V. for providing the sample and photograph of the chloride segregation from Udachnaya-East pipe, Dr. Mazurov M.P. for providing apatite and forsterite samples and Dr. Polozov A. for drawing the map. The computations were performed using facilities of the Computational Centre of the Research Park of St. Petersburg State University. This work is financially supported by the Russian Foundation for Basic Research (grants 15-05-09345 , 18-05-00682 ) and VEGA grant 1/0560/15.
Ключевые слова (''Своб.индексиров.''): polymorphs cacl2--raman spectra--magma-salt interaction--chlorocalcite--daughter mineral--ab initio calculations
Аннотация: Anhydrous chlorides - CaCl2, and KCaCl3 (chlorocalcite) were identified as mineral inclusions in halite from the Siberian Large Igneous Province at the contact of magmatic intrusions and evaporates. Chlorocalcite was also found as daughter mineral in polyphase hypersaline inclusions. While Raman spectra of KCaCl3 (chlorocalcite) in natural inclusions are similar to spectra of synthetic analogue, the Raman spectra of natural CaCl2 do not correspond to the published Raman spectra of synthetic CaCl2. Simulations of Raman spectra using ab initio density-functional theory (DFT) allowed us to calculate the spectra of individual polymorphs of CaCl2 and to discriminate anhydrous CaCl2 phases in natural inclusions and synthetic CaCl2. In the spectrum of the Pbcn polymorph of CaCl2 twelve different peaks could be identified at 74, 95, 99, 107, 124, 158, 164, 179, 212, 236, 244, 256 cm−1 in contrast to five peaks in the spectrum of the Pnnm polymorph of CaCl2 at 115, 157, 160, 211 and 252 cm−1. Naturally occurring CaCl2 in inclusions in halite consist of Pbcn polymorph only, which probably results from a mechanical stress on cooling from magmatic to ambient temperatures. However, the Raman spectra of the synthetic CaCl2 corresponds to the Pnnm phase with small contributions of the Pbcn phase. Raman spectra of synthetic KCaCl3 with main peaks at 58, 67, 90, 97, 133, 139, 147, 193 cm−1 agrees well with the spectra of chlorocalcite in the natural inclusions. Positions of each atom in the KCaCl3 structure were refined using the density-functional theory. There are no imaginary phonon modes for the optimized structure, indicating that the structure of KCaCl3 is stable. Calculated Raman spectrum is in a good agreement with the Raman spectrum of synthetic and natural KCaCl3 samples.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Bataleva, Yu. V., Palyanov, Yu. N., Borzdov, Yu. M., Bayukov O. A., Sobolev N. V.
Заглавие : Interaction of iron carbide and sulfur under P–T conditions of the lithospheric mantle
Коллективы : Russian Foundation for Basic Research [14-05-31061], Council for Grants and Support of the Leading Scientific Schools of the President of the Russian Federation [NSh 2024.2014.5]
Место публикации : Dokl. Earth Sci.: MAIK Nauka-Interperiodica / Springer, 2015. - Vol. 463, Is. 1. - P.707-711. - ISSN 1028-334X, DOI 10.1134/S1028334X15070077
Примечания : This study was supported by the Russian Foundation for Basic Research (project no. 14-05-31061) and by the Council for Grants and Support of the Leading Scientific Schools of the President of the Russian Federation (NSh 2024.2014.5).
Предметные рубрики: MINERAL INCLUSIONS
DIAMOND
CARBON
EVOLUTION
CORES
Аннотация: Experimental studies were performed in the Fe3C–S system at P = 6.3 GPa, T = 900–1600°C, and t = 18–20 h. The study aimed to characterize the conditions of iron carbide stability in a reduced lithospheric mantle and to reveal the possibility of the formation of elemental carbon by the interaction of iron carbide and sulfur. It was found that the reaction at T 1200°C proceeds with the formation of a pyrrhotite–graphite assemblage by the following scheme: 2Fe3C + 3S2 → 6FeS + 2C0. The crystallization of graphite at T 1200°C is accompanied by the generation of sulfide and metal–sulfide melts and via 2Fe3C + 3S2 → 6[Fe–S(melt) + Fe–S–C(melt)] + 2C(graphite)0 reaction. Resulting from the carbon-generating reactions, not only graphite crystallized in sulfide or metal–sulfide melts, but the growth of diamond also takes place. The obtained data allow one to consider cohenite as a potential source of carbon in the processes of diamond and graphite crystallization under the conditions of a reduced lithospheric mantle. The interaction of iron carbide and sulfur under which carbon extraction proceeds may be one of possible processes of the global carbon cycle. © 2015, Pleiades Publishing, Ltd
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Karavayskiy A. Yu., Lukin Y. I.
Заглавие : Influence of dielectric relaxations of soil water on the temperature dependence of soil permittivity
Колич.характеристики :10 с
Место публикации : Opt. Spectrosc. - 2023. - Vol. 131, Is. 12. - P.1190-1199. - ISSN 0030400X (ISSN), DOI 10.1134/S0030400X24700206. - ISSN 15626911 (eISSN)
Примечания : Cited References: 23. - This work was supported by the Russian Science Foundation and the Krasnoyarsk Regional Fund of Science and Technology Support within the framework of scientific project no. 22-27-20112
Аннотация: Using a generalized refractive mixture dielectric model, the influence of the relative permittivity spectra of bound and unbound water in mineral soil on the nature of the temperature dependence of the relative permittivity of natural mineral soil, with a clay fraction content of 41.3%, was studied in the electromagnetic field frequency range from 50 MHz to 15 GHz. The causes of the emergence of intersections in the relative permittivity spectra of mineral soil, obtained at different temperatures but for a sample of the same moisture content, have been studied. It has been proved that the emergence of such an intersection point in the frequency range up to 1.5 GHz is due to the Maxwell–Wagner effect in bound water. The dependences of the frequency of the intersection point of the relative permittivity spectra of mineral soil on the temperature and volumetric content of bound and unbound water have been studied.
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