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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mikhaleva E. A., Gorev M. V., Molokeev M. S., Kartashev A. V., Flerov I. N.
Заглавие : Anisotropy of piezocaloric effect at ferroelectric phase transitions in ammonium hydrogen sulphate
Место публикации : J. Alloys Compd. - 2020. - Vol. 839. - Ст.155085. - ISSN 09258388 (ISSN), DOI 10.1016/j.jallcom.2020.155085
Примечания : Cited References: 31. - The reported study was supported by the Russian Science Foundation (project no. 19-72-00023 ). X-ray and dilatometric data were obtained using the equipment of Krasnoyarsk Regional Center of Research Equipment of Federal Research Center "Krasnoyarsk Science Center SB RAS"
Аннотация: The role of anisotropy of the thermal expansion in formation of piezocaloric effect (PCE) near ferroelectric phase transitions in NH4HSO4 was studied. Strong difference in linear baric coefficients and as a result in intensive and extensive PCE associated with the different crystallographic axes was found. PCE giving the main contribution to the barocaloric effect were determined at both phase transitions. Rather strong effect of the lattice dilatation on the tuning of PCE was observed. Comparative analysis of PCE at the phase transitions in different materials showed that NH4HSO4 can be considered as a promising solid-state refrigerant. A hypothetical cooling cycle based on alternate using uniaxial pressure along two axes was considered.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Pugachev A. M., Zaytseva I. V., Surovtsev N. V., Krylov A. S.
Заглавие : Anharmonicity and local noncentrosymmetric regions in BaTiO3 pressed powder studied by the Raman line temperature dependence
Место публикации : Ceram. Int. - 2020. - Vol. 46, Is. 14. - P.22619-22623. - ISSN 02728842 (ISSN), DOI 10.1016/j.ceramint.2020.06.024
Примечания : Cited References: 26. - The reported study was funded by RFBR , according to the research project No. 18-02-00399 and 19-42-543-016 , Government of Novosibirsk region No. 19-42-543-016 and State assignment No AAAA-A17-117052410033-9. The experiments were performed in the multiple-access center “High-Resolution Spectroscopy of Gases and Condensed Matter” in IA&E SB RAS (Novosibirsk, Russia) and Center for Common Use of the Krasnoyarsk Scientific Center, SB RAS (Krasnoyarsk, Russia)
Аннотация: The temperature dependencies of position, width, and integral amplitude the E(TO) line near 307 cm−1 in Raman spectra in barium titanate powders with different non-hydrostatic pressure and temperature treatment were studied. It was found that parameters of the E(TO) line near 307 cm−1 are different in the crystal, the untreated powder, the powder treated by the non-hydrostatic pressure, and the powder annealed after the pressure treatment. The line width (FWHM) increase with temperature according to Klemens model. It indicates that the origin of the line broadening is the anharmonicity of the E(TO) phonons. The pressure treatment changes the anharmonicity of the phonon potential. It was found that the temperature dependence of the integral intensity of the E(TO) line is similar to that of the second optical harmonic signal and reflects the presence of the local polar regions. Thus, the E(TO) line in the Raman spectrum allows one to characterize the average polarity of local regions and their anharmonicity depending on non-hydrostatic pressures and thermal treatment.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Ma, Yalin, Molokeev M. S., Zhu, Chuanhui, Zhao, Shuang, Han, Yifeng, Wu, Meixia, Liu, Sizhan, Tyson, Trevor A., Croft, Mark, Li, Man-Rong
Заглавие : Magnetic transitions in exotic perovskites stabilized by chemical and physical pressure
Место публикации : J. Mater. Chem. C. - 2020. - Vol. 8, Is. 15. - P.5082-5091. - ISSN 2050-7526, DOI 10.1039/c9tc06976c. - ISSN 2050-7534(eISSN)
Примечания : Cited References: 79. - This work was financially supported by the National Science Foundation of China (NSFC-21801253, 11804404 and 21875287) and the National Science Foundation (NSF) Grant No. DMR-1809931. Structural analysis of exotic materials in this study was partly supported by the Research Grant No. 075-15-2019-1886 from the Government of the Russian Federation. The XANES work at the Brookhaven National Laboratory, NSLS-II, was supported by the DOEBES (DE-SC0012704). The NSLS-II work was performed on beamline 7-BM and the authors gratefully acknowledge the invaluable help of the beamline scientists Steven Ehrlich and Syed Khalid.
Предметные рубрики: COLOSSAL MAGNETORESISTANCE
CATION ORDER
RMN3O6 R
T-C
TEMPERATURE
Аннотация: Exotic perovskites significantly enrich materials for multiferroic and magnetoelectric applications. However, their design and synthesis is a challenge due to the mostly required recipe conditions at extremely high pressure. Herein, we presented the Ca2−xMnxMnTaO6 (0 ≤ x ≤ 1.0) solid solutions stabilized by chemical pressure assisted with intermediate physical pressure up to 7 GPa. The incorporation of Mn2+ into the A-site neither drives any cationic ordering nor modifies the orthorhombic Pbnm structure, namely written as (Ca1−x/2Mnx/2)(Mn1/2Ta1/2)O3 with disordered A and B site cationic arrangements. The increment of x is accompanied by a ferromagnetic to antiferromagnetic transition around x = 0.2, which is attributed to the double-exchange interactions between A-site Mn2+ and B-site Mn3+. Partial charge disproportionation of the B-site Mn3+ into Mn2+ and Mn4+ occurs for x above 0.8 samples as manifested by X-ray spectrum and magnetic behaviors. The coexistence of B-site Mn3+ (Jahn–Teller distortion ion) and B′-site Ta5+ (second-order Jahn–Teller distortion ion) could be energetically responsible for the absence of A-site columnar ordering as observed in other quadruple perovskites with half of the A-sites occupied by small transition-metal cations. These exceptional findings indicate that exotic perovskites can be successfully stabilized at chemical and intermediate physical pressure, and the presence of Jahn–Teller distortion cations at the same lattice should be avoided to enable cationic ordering.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Gorev M. V., Kartashev A. V., Bogdanov E. V., Flerov I. N., Laptash N. M.
Заглавие : Calorimetric, dilatometric and DTA under pressure studies of the phase transitions in elpasolite (NH4)2KZrF7
Место публикации : J. Fluor. Chem. - 2020. - Vol. 235. - Ст.109523. - ISSN 00221139 (ISSN), DOI 10.1016/j.jfluchem.2020.109523
Примечания : Cited References: 45. - The reported study was funded by RFBR according to the research project No. 18-02-00269 a. X-ray and dilatometric data were obtained using the equipment of Krasnoyarsk Regional Center of Research Equipment of Federal Research Center "Krasnoyarsk Science Center SB RAS"
Аннотация: Heat capacity, thermal expansion, and sensitivity to the hydrostatic pressure of (NH4)2KZrF7 elpasolite are studied in a wide temperature range. The changes in deformation and entropy during successive phase transitions are determined: Δ(ΔV/V) = 3·10−4; ΔS = 8 J/mol K The temperatures and entropies of phase transitions turned out to be slightly sensitive to pressure changes. An analysis of the entropy of phase transformations was performed in the framework of the model of the cubic phase structure Fm-3 m. In the low temperature phase, an anomalous behavior of thermodynamic properties, which is not characteristic of phase transitions, was observed, accompanied by a significant change in the crystal lattice entropy.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mikhaleva E. A., Flerov I. N., Bogdanov E. V., Bondarev V. S., Gorev M. V., Rysiakiewicz-Pasek E.
Заглавие : Size effect on sensitivity to external pressure and caloric effects in TGS: Ceramics and nanocomposites
Место публикации : Mater. Today Commun. - 2020. - Vol. 25. - Ст.101463. - ISSN 23524928 (ISSN), DOI 10.1016/j.mtcomm.2020.101463
Примечания : Cited References: 39
Аннотация: Experimental study of temperature-pressure phase diagrams revealed a slight difference in the sensitivity to hydrostatic pressure of triglycine sulfate (TGS) as a bulk (single crystal, ceramics), and nanoparticles embedded in porous glass (TGS + PG). An analysis of the pressure sensitivity, dT0/p and dT0/dσ, and entropies of the P21 ↔ P21/m phase transition showed the closeness of the barocaloric parameters in various materials under study. Due to the strong anisotropy of thermal expansion, the piezocaloric effect under pressure along the axis c exceeds the barocaloric effect in single-crystal TGS. The reasons for the strong reduction in the electrocaloric effect in the ferroelectric component of nanocomposites compared with a single-crystal are discussed.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Krylov A. S., Senkovska I., Ehrling S., Maliuta M., Krylova S. N., Slyusareva E., Vtyurin A. N., Kaskel S.
Заглавие : Single particle Raman spectroscopy analysis of the metal-organic framework DUT-8(Ni) switching transition under hydrostatic pressure
Место публикации : Chem. Commun. - 2020. - Vol. 56, Is. 59. - P.8269-8272. - ISSN 1364548X (ISSN), DOI 10.1039/d0cc02491k
Примечания : Cited References: 40. - This work is financially supported by the Russian Foundation for Basic Research No18-02-00754 and German research foundation (FOR 2433, MOF-switches). The authors would like to thank Dr. V. Bon for support and scientific discussions
Аннотация: Experimental in situ observations of phase coexistence in switchable metal-organic frameworks are reported to provide a fundamental understanding of dynamic adsorbents that can change their pore structure in response to external stimuli. A prototypical flexible pillared layer framework DUT-8(Ni) (DUT = Dresden University of Technology) was studied under hydrostatic pressure by in situ Raman spectroscopy on single crystals. The closing transition of the open pore phase (op) containing DMF in the pores in silicon oil as a pressure transmitting fluid, as well as the closed pore phase (cp) to op transition under pressure in methanol, were studied. Phase coexistences during both transitions were observed.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Bogdanov E. V., Pogoreltsev E. I., Kartashev A. V., Gorev M. V., Molokeev M. S., Mel'nikova S. V., Flerov I. N., Laptash N. M.
Заглавие : Thermodynamic properties of vanadium oxypentafluoride (IV) (NH4)3VOF5
Место публикации : Phys. Solid State. - 2020. - Vol. 62, Is. 7. - P.1271-1279. - ISSN 10637834 (ISSN), DOI 10.1134/S1063783420070057
Примечания : Cited References: 17. - This study was supported by the Russian Foundation for Basic Research, the Government of the Krasnoyarsk Territory, and the Krasnoyarsk Territorial Foundation for Support of Scientific and R&D Activity, project no. 18-42-243003 “Effect of Deuteration on Orientational Ordering and Phase Transitions in Ammonium Fluorine-Oxygen Vanadates”
Аннотация: The (NH4)3VOF5 crystals have been synthesized and their homogeneity and single-phase structure has been established by the X-ray diffraction, energy dispersive spectroscopy, and X-ray photoelectron spectroscopy studies. The investigations of the temperature dependences of specific heat, entropy, strain, and pressure susceptibility show the occurrence of three phase transitions caused by the structural transformations in the (NH4)3VOF5 crystals. The T–p phase diagram shows the temperature limits of stability of the crystalline phases implemented in (NH4)3VOF5. The optical and dielectric studies disclose the ferroelastic nature of the phase transitions. An analysis of the experimental data together with the data on the isostructural (NH4)3VO2F4 crystal makes it possible to distinguish the physical properties of oxyfluorides containing vanadium of different valences (IV and V).
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Ushakov A. V., Karpov I. V., Fedorov L. Y., Demin V. G., Goncharova E. A., Shaihadinov A. A., Zeer G. M., Zharkov S. M.
Заглавие : The effect of microstructural features on the ferromagnetism of nickel oxide nanoparticles synthesized in a low-pressure arc plasma
Место публикации : Physica E. - 2020. - Vol. 124. - Ст.114352. - ISSN 13869477 (ISSN), DOI 10.1016/j.physe.2020.114352
Примечания : Cited References: 31. - The work was performed with a support of the grant of the Russian Science Foundation (Project No. 16-19-10054 ). The electron microscopy investigations were conducted in the SFU Joint Scientific Center supported by the State assignment (#FSRZ-2020-0011) of the Ministry of Science and Higher Education of the Russian Federation
Аннотация: Nickel oxide nanoparticles were first synthesized by sputtering high-purity nickel in an oxygen plasma of a low-pressure arc discharge. The structure, morphology, and optical and magnetic properties of NiO nanoparticles were studied by XRD, TEM, FTIR, UV-VIS, and VSM. TEM images showed that the obtained NiO nanoparticles have a narrow particle size distribution and an average particle size of 12 nm. The XRD results and the processing of diffractograms by the Rietveld method showed that the obtained nanoparticles have a face-centered cubic lattice with an average particle size of 13 nm. With decreasing temperature, residual stresses increase and peaks corresponding to the superstructure appear. The band gap of NiO was determined from the optical absorption spectrum and amounted to 3.21 eV. Magnetic measurements showed that, at temperatures of 200 and 300 K, NiO nanoparticles, unlike bulk particles, exhibit ferromagnetic behavior, and at 5 K a magnetic hysteresis loop appears. Based on the studies, a dendritic model of the nanoparticle microstructure is proposed.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Kuz'min V. I., Orlov Yu. S., Zarubin A. E., Ovchinnikova T. M., Ovchinnikov S. G.
Заглавие : Magnetism in spin crossover systems: Short-range order and effects beyond the Heisenberg model
Коллективы : Russian Scientific FoundationRussian Science Foundation (RSF) [18-12-00022]
Место публикации : Phys. Rev. B. - 2019. - Vol. 100, Is. 14. - Ст.144429. - ISSN 2469-9950, DOI 10.1103/PhysRevB.100.144429. - ISSN 2469-9969(eISSN)
Примечания : Cited References: 72. - The authors thank the Russian Scientific Foundation for the financial support under Grant No. 18-12-00022.
Предметные рубрики: LOWER-MANTLE
STATE
TRANSITION
PRESSURE
IRON
SUSCEPTIBILITY
Аннотация: To study non-Heisenberg effects in the vicinity of spin crossover in strongly correlated electron systems we derive an effective low-energy Hamiltonian for the two-band Kanamori model. It contains a Heisenberg high-spin term proportional to exchange constant as well as a low-spin term proportional to spin gap parameter ɛs. Using cluster mean field theory we obtain several non-Heisenberg effects. Near the critical value of spin gap ɛcs there is a magnetic phase transition of first order. In the vicinity of ɛcs in the paramagnetic phase we observe nontrivial behavior of the Curie constant in the paramagnetic susceptibility in the wide range of temperature. Reentrant temperature behavior of nearest-neighbor spin-spin correlations is observed at ɛsɛcs. Finally, the pressure-temperature magnetic phase diagram for ferroperriclase is obtained using the effective Hamiltonian.
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Lyubutin I. S., Gavriliuk A. G., Andryushin N. D., Pavlovskiy M. S., Zinenko V. I., Lyubutina M. V., Troyan I. A., Smirnova E. S.
Заглавие : Pressure-Induced Structural Transition to the Polar Phase in GdFe3(BO3)4
Место публикации : Cryst. Growth Des. - 2019. - Vol. 19, Is. 12. - P.6935-6944. - ISSN 15287483 (ISSN), DOI 10.1021/acs.cgd.9b00609
Примечания : Cited References: 39. - The authors express their deep gratitude to Prof. S. G. Ovchinnikov for initiating this work and fruitful discussions. These studies were performed with the support of the Ministry of Science and Higher Education within the State assignment FSRC "Crystallography and Photonics" RAS in part for the synchrotron Mössbauer measurements. Support from RFBR Grant No. 17-02-00766 in part for the Raman spectroscopy measurements and from No. 18-02-00696 in part for the theoretical calculations is also acknowledged. For preparation and tests of high-pressure cells, (39) the facilities of Center for Collective Use “Accelerator Center for Neutron Research of the Structure of Substance and Nuclear Medicine” of the INR RAS were used.
Аннотация: The GdFe3(BO3)4 crystal has attracted great interest as a magnetic-field-induced multiferroic. In this paper, we show that the multiferroic properties in this crystal can be induced by high pressure. At high pressures up to 50 GPa, created in diamond anvil cells, the structural and vibrational (phonon) properties of the GdFe3(BO3)4 crystal were studied. The structural phase transition was detected at about 23–25 GPa by Raman and synchrotron Mössbauer (NFS) spectroscopy. First-principle calculations of the crystal lattice dynamics at pressures below and above the structural transition were carried out. It was established that at pressures above the structural transition, the space group R32 of GdFe3(BO3)4 is changed to the polar space group R3, and the crystal becomes a ferroelectric. At the R32 → R3 transition, the displacement of the boron ion B(2) and oxygen O results in the formation of boron–oxygen B(2)O4 tetrahedrons instead of the plane BO3 triangles. Meanwhile, the triangle oxygen environment of boron in the site B(1) remains unchanged. The nearest environment of the gadolinium ion also changes significantly. Instead of six oxygen ions in the R32 phase, the nearest surroundings of Gd in the R3 phase consist of nine oxygen ions forming a complex polyhedron. A large hysteresis of the transition indicates that this crystal remains a ferroelectric with a decrease in pressure to about ambient pressure.
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