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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Denisova E. A., Komogortsev S. V., Li O. A., Chekanova L. A., Patrusheva T. N., Eremin E. V.
Заглавие : Magnetic particles in mesoporous silica MCM-41
Коллективы : Euro-Asian Symposium "Trends in MAGnetism": Nanomagnetism
Место публикации : V Euro-Asian simposium "Trend in MAGnetism": Nanomagnetism: abstracts. - Vladivostok: FEFU, 2013. - С. 176. - ISBN 978-5-7444-3124-2
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Морозов, Евгений Владимирович, Шабанова О. В., Фалалеев, Олег Владимирович
Заглавие : Применение ЯМР томографии для исследования межфазных границ в системах коллоидного кремнезема
Место публикации : Конденсир. среды и межфаз. границы. - Воронеж: Воронеж. гос. ун-т, 2012. - Т.14. № 1. - С. 60-69. - ISSN 1606-867X
Аннотация: В работе представлены результаты ЯМР томографических исследований золей коллоидного кремнезема, полученных из силикатов щелочных металлов кислотным выщелачиванием. Исследована динамика времен ядерной спин-решеточной и спин-спиновой релаксации в процессе гелеобразования, а также визуализировано пространственное распределение протекающих процессов. Рассмотрена методологическая сторона проблемы обеспечения контраста на ЯМР томограммах модельных коллоидных систем при золь-гель переходе. Экспериментально продемонстрирована актуальность разработки методологии исследования межфазных границ с помощью нового для данного направления метода.The NMR Imaging investigation results of colloid silica obtained from alkali metals silicates by acidic leaching are presented. The dynamic of nuclear spin-lattice and spin-spin relaxation times was studied during the sol-gel transfer processes and the spatial distribution of occurred processes was visualized. The methodological direction of problem associated with contrast supply on the NMR Images was examined using model colloids samples during sol-gel transfer. It was demonstrated experimentally that the development of interfaces investigation methodology seems to be very important for advance of NMR Imaging to this field of research.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Kirik S. D., Parfenov V. A., Zharkov S. M.
Заглавие : Monitoring MCM-41 synthesis by X-ray mesostructure analysis
Место публикации : Micropor. Mesopor. Mater.: Elsevier Science, 2014. - Vol. 195. - P.21-30. - ISSN 1387-1811, DOI 10.1016/j.micromeso.2014.04.012. - ISSN 1873-3093
Примечания : Cited References: 70. - The investigation was made with financial support of the Program of Presidium RAS (Project 24.37), RF State contracts No 02.740.11.0629, RFBR Grants: 11-03-00610a and 11-03-12161-ofi, RSF 14-13-000025.
Предметные рубрики: ORDERED MESOPOROUS MATERIALS
ORDERED MESOPOROUS MATERIALS
IN-SITU
POWDER DIFFRACTION
SILICA/SURFACTANT COMPOSITES
ELECTRON-MICROSCOPY
MOLECULAR-SIEVES
STABLE MCM-41
SILICA
ADSORPTION
Ключевые слова (''Своб.индексиров.''): hydrothermal stability--mcm-41--mesostructure--tem--x-ray diffraction
Аннотация: The electron density maps calculated from X-ray diffraction patterns of the mesoporous silica material MCM-41 present averaged mesostructure images which in contrast to transmission electron microscopy (TEM) images are exceptionally repeating and represent the whole sample. It was shown that the averaged mesostructure parameters such as a unit cell parameter, a pore diameter, a wall width, a pore shape estimated from the X-ray powder diffraction data in combination with the continuous electron density function approach allow monitoring continuous set of the silica framework states at different stages of the material synthesis. The mentioned technique supplemented by N 2-adsorption measurements and transmission electron microscopy was applied for consideration of the MCM-41 hydrothermal stability. Attention has been given to the variations of the synthesis conditions affecting the hydrothermal stability, in particular the maintaining the basicity of the synthesis solution as well the substitution of the synthesis solution with water or a salt solution at hydrothermal treatment. The averaged pore shape was observed to be changed from cylindrical to hexagonal-prismatic form. The observed wall thickness was in the range from 0.75 to 1.25 nm. The competition of silica polycondensation and surface hydrolysis was shown to be responsible for the variety of framework geometry and hydrothermal stability. It has been established that the pore diameter increases generally due to the osmotic pressure of water. If the pores acquire the average prismatic hexagonal shape, the sample has low hydrothermal stability. Under the conditions favorable for the polycondensation the pores have averaged cylindrical shape and material demonstrates higher hydrothermal stability. Cooperative mechanism of mesostructure destruction under hydrothermal conditions was observed using TEM data and was discussed in connection with irregular polycondensation. © 2014 Elsevier Inc. All rights reserved.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Yakushkin S. S., Dubrovskiy A. A., Balaev A. D., Shaykhutdinov K. A., Bukhtiyarova G. A., Martyanov O. N.
Заглавие : Magnetic properties of few nanometers ɛ-Fe2O3 nanoparticles supported on the silica
Место публикации : J. Appl. Phys.: American Institute of Physics, 2012. - Vol. 111, Is. 4. - Ст.44312. - ISSN 0021-8979, DOI 10.1063/1.3686647
Примечания : Cited References: 27. - authors thank A. D. Balaev and N. V. Volkov for fruitful discussions and comments. This work was supported by Program of RAS No. 27.46.
Предметные рубрики: HIGH-TEMPERATURE
IRON
STABILIZATION
OXIDE
GEL
Аннотация: Magnetic properties of ɛ-Fe2O3nanoparticles supported on silica with the average size of few nanometers, narrow size distribution and no admixture of any other iron oxide polymorphs are investigated. The investigation of the temperature behavior of magnetization within the temperature range from 4.2 to 1000 K revealed the presence of several magnetic subsystems in the species under study. The temperatures’ behavior of the magnetic moment value indicates ferrimagnetic ordering in the ɛ-Fe2O3nanoparticles with a Curie temperature of about 800 K and points to the existence of a significant paramagnetic contribution becoming apparent at low temperatures. According to the electron spin resonance data, the particles possess superparamagnetic behavior at temperature higher ∼120 K. The model of the magnetic structure of monophase system of few nanometers ɛ-Fe2O3nanoparticles supported on silica is proposed.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Dubrovskii A. A., Balaev D. A., Shaikhutdinov K. A., Yakushkin S. S., Bukhtiyarova G. A., Martyanov O. N.
Заглавие : The effect of the particle size on the magnetic properties of nanosized ε-Fe2O3 particles on a silica support
Коллективы : Moscow International Symposium on Magnetism, Московский государственный университет им. М.В. Ломоносова
Место публикации : Moscow Int. Symp. on Magnet. (MISM-2014): Book of abstracts. - 2014. - Ст.2OR-H-7. - P.655. - ISBN 978-5-91978-025-0
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Balaev D. A., Yakushkin S. S., Dubrovskii A. A., Bukhtiyarova G. A., Shaikhutdinov K. A., Martyanov O. N.
Заглавие : Study of the high-coercivity material based on ε-Fe2O3 nanoparticles in the silica gel matrix
Место публикации : Tech. Phys. Lett.: MAIK Nauka-Interperiodica / Springer, 2016. - Vol. 42, Is. 4. - P.347-350. - ISSN 10637850 (ISSN), DOI 10.1134/S1063785016040039
Примечания : Cited References: 17. - This study was supported by the Federal Agency for Scientific Organizations of Russia (base budget financing no. V.44.1.15), the Scientific and Educational Center of Energy-Efficient Catalysis at the Novosibirsk State University, and the Russian Foundation for Basic Research (project no. 15-32-50919).
Предметные рубрики: Phase
Field
State
Oxide
Iron
Аннотация: We report the results of investigations of ε-Fe2O3 magnetic nanoparticles obtained by incipient wetness impregnation of silica gel. It was established that the obtained samples with an iron content of 12‒16% mass % containing ε-Fe2O3 nanoparticles with an average size of 10 nm on the silica gel surface exhibit a room-temperature coercivity of about 10 kOe. Along with fabrication simplicity, this fact makes the prepared samples promising for application as a magnetically hard material. © 2016, Pleiades Publishing, Ltd
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Belyaev B. A., Drokin N. A., Kumakhov M. A., Shabanov V. F.
Заглавие : Dielectric properties of liquid crystals in polycapillary matrices
Коллективы :
Место публикации : Phys. Solid State: MAIK NAUKA/INTERPERIODICA/SPRINGER, 2010. - Vol. 52, Is. 6. - P1315-1322. - ISSN 1063-7834, DOI 10.1134/S1063783410060314
Примечания : Cited References: 24. - This study was supported by the Council on Grants from the President of the Russian Federation (grant no. 3818.2008.3) and the Siberian Branch of the Russian Academy of Sciences (Integration Project no. 5) and performed within the framework of the State Contract (no. 02.740.11.0220).
Предметные рубрики: MOLECULAR-SIEVES
SILICA AEROGEL
POROUS-GLASS
MEMBRANES
NMR
8CB
Аннотация: This paper reports on the results of investigations into the dielectric properties of liquid crystals embedded in polycapillary matrices and describes a technique for their measurement. It has been revealed that the chemical structure of the rigid core and the length of mobile alkyl groups of liquid-crystal molecules of the alkylcyanobiphenyl group substantially affect the equilibrium configuration of the liquid-crystal director in capillaries. The reorientation of liquid-crystal molecules embedded in capillaries in the nematic phase under the influence of an external magnetic field has been investigated.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Bukhtiyarova G. A., Mart'yanov O. N., Yakushkin S. S., Shuvaeva M. A., Bayukov O. A.
Заглавие : State of iron in nanoparticles prepared by impregnation of silica gel and aluminum oxide with FeSO4 solutions
Коллективы :
Место публикации : Phys. Solid State: MAIK NAUKA/INTERPERIODICA/SPRINGER, 2010. - Vol. 52, Is. 4. - P826-837. - ISSN 1063-7834, DOI 10.1134/S1063783410040268
Примечания : Cited References: 27. - This study was supported by the Presidium of the Russian Academy of Sciences within the framework of the Program no. 27 "Principles of Basic Research of Nanotechnologies and Nanomaterials," Project no. 46 "Magnetically Ordered Nanoparticles in Catalytic Systems: Synthesis, Evolution, and Physicochemical Properties."
Предметные рубрики: THERMAL-DECOMPOSITION
BETA-FEOOH
MOSSBAUER
FERRIHYDRITE
EPSILON-FE2O3
FE-2(SO4)(3)
SULFATE
FE-57
Аннотация: The state of iron in nanoparticles prepared by impregnating silica gel and aluminum oxide with iron(II) sulfate solutions has been investigated using Mossbauer spectroscopy. It has been revealed that the state of iron depends on the nature of the support. Iron(III) hydroxysulfate and iron(III) oxysulfate nanoparticles are formed on the surface of silica gel, and iron oxide nanoparticles are formed on the surface of aluminum oxide. An increase in the concentration of iron ions or in the size of iron-containing particles leads to hydration of the nanoparticle surface. The calcination of the samples results in the formation of E -Fe2O3 oxide in a strongly disordered or amorphous state in iron-containing particles on the surface of silica gel.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Deich L. I.
Заглавие : Low-frequency raman-scattering in glasses
Разночтения заглавия :авие SCOPUS: Low-frequency Raman scattering in glasses
Место публикации : Phys. Rev. B. - 1995. - Vol. 51, Is. 13. - P.8131-8139. - ISSN 0163-1829, DOI 10.1103/PhysRevB.51.8131
Примечания : Cited References: 32
Предметные рубрики: AMORPHOUS SOLIDS
VITREOUS SILICA
THERMAL-CONDUCTIVITY
LIGHT-SCATTERING
TEMPERATURE
STATES
MODES
HEAT
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Deich L. I.
Заглавие : Far-infrared attenuation in glasses
Разночтения заглавия :авие SCOPUS: Far-infrared attenuation in glasses
Место публикации : Phys. Rev. B. - 1994. - Vol. 49, Is. 1. - P.109-113. - ISSN 0163-1829, DOI 10.1103/PhysRevB.49.109
Примечания : Cited References: 29
Предметные рубрики: VITREOUS SILICA
TEMPERATURE
MODEL
LOCALIZATION
ABSORPTION
SOLIDS
STATES
Аннотация: The influence of quasilocal vibrations on the far-infrared spectra of glasses is investigated under the supposition that the quasilocal vibrations are directly inactive in the attenuation. It is shown that taking into account phonon-quasilocal-vibration coupling and both medium- and short-range structure of the inhomogeneities of a photon-phonon coupling parameter can give rise to an attenuation curve similar to one observed for a-SiO2 and related materials.
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