Библиотека института физики им. Л.В. Киренского СО РАН

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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Kirik S. D., Parfenov V. A., Zharkov S. M.
Заглавие : Monitoring MCM-41 synthesis by X-ray mesostructure analysis
Место публикации : Micropor. Mesopor. Mater.: Elsevier Science, 2014. - Vol. 195. - P.21-30. - ISSN 1387-1811, DOI 10.1016/j.micromeso.2014.04.012. - ISSN 1873-3093
Примечания : Cited References: 70. - The investigation was made with financial support of the Program of Presidium RAS (Project 24.37), RF State contracts No 02.740.11.0629, RFBR Grants: 11-03-00610a and 11-03-12161-ofi, RSF 14-13-000025.
Предметные рубрики: ORDERED MESOPOROUS MATERIALS
ORDERED MESOPOROUS MATERIALS
IN-SITU
POWDER DIFFRACTION
SILICA/SURFACTANT COMPOSITES
ELECTRON-MICROSCOPY
MOLECULAR-SIEVES
STABLE MCM-41
SILICA
ADSORPTION
Ключевые слова (''Своб.индексиров.''): hydrothermal stability--mcm-41--mesostructure--tem--x-ray diffraction
Аннотация: The electron density maps calculated from X-ray diffraction patterns of the mesoporous silica material MCM-41 present averaged mesostructure images which in contrast to transmission electron microscopy (TEM) images are exceptionally repeating and represent the whole sample. It was shown that the averaged mesostructure parameters such as a unit cell parameter, a pore diameter, a wall width, a pore shape estimated from the X-ray powder diffraction data in combination with the continuous electron density function approach allow monitoring continuous set of the silica framework states at different stages of the material synthesis. The mentioned technique supplemented by N 2-adsorption measurements and transmission electron microscopy was applied for consideration of the MCM-41 hydrothermal stability. Attention has been given to the variations of the synthesis conditions affecting the hydrothermal stability, in particular the maintaining the basicity of the synthesis solution as well the substitution of the synthesis solution with water or a salt solution at hydrothermal treatment. The averaged pore shape was observed to be changed from cylindrical to hexagonal-prismatic form. The observed wall thickness was in the range from 0.75 to 1.25 nm. The competition of silica polycondensation and surface hydrolysis was shown to be responsible for the variety of framework geometry and hydrothermal stability. It has been established that the pore diameter increases generally due to the osmotic pressure of water. If the pores acquire the average prismatic hexagonal shape, the sample has low hydrothermal stability. Under the conditions favorable for the polycondensation the pores have averaged cylindrical shape and material demonstrates higher hydrothermal stability. Cooperative mechanism of mesostructure destruction under hydrothermal conditions was observed using TEM data and was discussed in connection with irregular polycondensation. © 2014 Elsevier Inc. All rights reserved.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Frolov G. I., Zhigalov V. S., Bayukov O. A.
Заглавие : Phase composition of nanocrystalline iron films deposited in a nitrogen atmosphere
Место публикации : Phys. Solid State: MAIK NAUKA/INTERPERIODICA/SPRINGER, 1999. - Vol. 41, Is. 10. - P1669-1671. - ISSN 1063-7834, DOI 10.1134/1.1131050
Примечания : Cited References: 14
Предметные рубрики: ELECTRON-MICROSCOPY
MOSSBAUER
Аннотация: The phase composition of iron films prepared by pulsed-plasma deposition in a controlled nitrogen atmosphere is investigated by Mossbauer spectroscopy. The observed changes in the phase composition are dictated by the nanocrystalline structure of the samples and the dynamics of the substrate temperature during film deposition. (C) 1999 American Institute of Physics. [S1063-7834(99)02110-3].
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Feggeler, Thomas, Meckenstock, Ralf, Spoddig, Detlef, Zingsem, Benjamin W., Ohldag, Hendrik, Wende, Heiko, Farle M., Winklhofer, Michael, Ollefs, Katharina J.
Заглавие : Spatially resolved GHz magnetization dynamics of a magnetite nano-particle chain inside a magnetotactic bacterium
Коллективы : Deutsche Forschungsgemeinschaft (DFG, German Research Foundation)German Research Foundation (DFG) [405553726 TRR 270, OL513/1-1, 321560838]; government of the Russian Federation [075-15-2019-1886]; US Department of Energy, Office of Science, Office of Basic Energy SciencesUnited States Department of Energy (DOE) [DE-AC02-76SF00515]
Место публикации : Phys. Rev. Research. - 2021. - Vol. 3, Is. 3. - Ст.033036. - ISSN 2643-1564(eISSN), DOI 10.1103/PhysRevResearch.3.033036
Примечания : Cited References: 40. - This work is funded by the Deutsche Forschungsgemeinschaft (DFG, German Research Foundation) -Project No. OL513/1-1, 321560838, and in part by the Deutsche Forschungsgemeinschaft (DFG, German Research Foundation) -Project-ID 405553726 TRR 270. M.F. acknowledges support by the government of the Russian Federation (agreement No. 075-15-2019-1886). We gratefully acknowledge A. Ney for fruitful discussions. The use of the Stanford Synchrotron Radiation Lightsource, SLAC National Accelerator Laboratory, is supported by the US Department of Energy, Office of Science, Office of Basic Energy Sciences under Contract No. DE-AC02-76SF00515
Предметные рубрики: AQUASPIRILLUM-MAGNETOTACTICUM
ELECTRON-MICROSCOPY
SP-NOV
Аннотация: Understanding magnonic properties of nonperiodic magnetic nanostructures requires real-space imaging of ferromagnetic resonance modes with spatial resolution well below the optical diffraction limit and sampling rates in the 5-100 GHz range. Here, we demonstrate element-specific scanning transmission x-ray microscopydetected ferromagnetic resonance (STXM-FMR) applied to a chain of dipolarly coupled Fe3O4 nano-particles (40-50 nm particle size) inside a single cell of a magnetotactic bacterium Magnetospirillum magnetotacticum. The ferromagnetic resonance mode of the nano-particle chain driven at 6.748 GHz and probed with 50 nm x-ray focus size was found to have a uniform phase response but non-uniform amplitude response along the chain segments due to the superposition of dipolar coupled modes of chain segments and individual particles, in agreement with micromagnetic simulations.
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