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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Atuchin V. V., Bazarov B. G., Gavrilova T. A., Grossman V. G., Molokeev M. S., Bazarova Zh. G.
Заглавие : Preparation and structural properties of nonlinear optical borates K 2(1-x)Rb 2xAl 2B 2O 7, 0 ˂ x ˂ 0.75
Место публикации : J. Alloys Compd.: Elsevier, 2012. - Vol. 515. - P.119-122. - ISSN 0925-8388, DOI 10.1016/j.jallcom.2011.11.115
Примечания : Cited References: 30. - This study was supported by SB RAS (Grant 34) and RFBR Grants 11-02-90706-mob_st and 11-03-00867a.
Предметные рубрики: UV-light generation
Frequence-conversion
K2Al2B2O7 crystal
Composition ratio
Mixed-crystals
Growth
KRbAl2B2O7
NLO properties
Non-linear optical
Non-linear optical properties
Rietveld analysis of X-ray powder diffraction data
Solubility limits
Space Groups
Structural parameter
Ключевые слова (''Своб.индексиров.''): krbal2b2o7--solid solution--crystal structure--nlo properties
Аннотация: The structures of K 2(1-x)Rb 2xAl 2B 2O 7, x = 0.25, 0.5, 0.75, have been determined in space group P321 through Rietveld analysis of X-ray powder diffraction data. The solubility limit in K 2(1-x)Rb 2xAl 2B 2O 7 crystals has been estimated as x similar to 0.83-0.9. Nonlinear optical properties of KRbAl 2B 2O 7 have been verified by powder Kurtz-Perry method. Mechanisms of structural parameter variation in K 2Al 2B 2O 7 crystal family have been discussed.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Atuchin V. V., Chimitova O. D., Gavrilova T. A., Molokeev M. S., Kim S. J., Surovtsev N. V., Bazarov B. G., Bazarova Zh.G.
Заглавие : Synthesis, structural and vibrational properties of microcrystalline RbNd(MoO4)(2)
Коллективы : International Conference on Crystal Growth, International Conference on Vapor Growth and Epitaxy
Место публикации : J. Cryst. Growth: Elsevier Science BV, 2011. - Vol. 318, Is. 1. - P.683-686. - ISSN 0022-0248, DOI 10.1016/j.jcrysgro.2010.09.076
Примечания : Cited References: 26
Предметные рубрики: MOLYBDENUM TRIOXIDE
DOUBLE MOLYBDATES
CRYSTAL-STRUCTURE
GROWTH
LASER
MOO3
Ключевые слова (''Своб.индексиров.''): crystal structure--solid state synthesis--molybdate
Аннотация: Rubidium neodymium dimolybdate, RbNd(MoO4)(2), microcrystals have been fabricated by solid state synthesis at T=550-600 degrees C by t=324 ks. Crystal structure of RbNd(MoO4)(2) has been refined by Rietveld method in space group Pbcn with cell parameters a = 5.1772(1) angstrom, b = 18.7293(4) angstrom, and c = 8.2774(1) angstrom (R-B=5.05%). The crystal structure of RbNd(MoO4)(2) consists of layers of MoO4 tetrahedrons cornersharing with NdO8 square antiprisms. These layers are perpendicular to b-axis of the unit cell. About 20 narrow Raman lines have been observed in Raman spectrum recorded for RbNd(MoO4)(2) powder sample. (C) 2010 Elsevier B.V. All rights reserved.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Boldyrev K. N., Popova M. N., Bettinelli M., Temerov V. L., Gudim, Irina A., Bezmaternykh L. N., Loiseau P., Aka G., Leonyuk N. I.
Заглавие : Quality of the rare earth aluminum borate crystals for laser applications, probed by high-resolution spectroscopy of the Yb3+ ion
Место публикации : Opt. Mater.: Elsevier Science BV, 2012. - Vol. 34, Is. 11. - P.1885-1889. - ISSN 0925-3467, DOI 10.1016/j.optmat.2012.05.021
Примечания : Cited References: 20. - This work was supported by the Russian Academy of Sciences under the Programs for Basic Research, the Russian Foundation for Basic research under Grants No 10-02-01071-a and No 09-02-00171-a, and by the Ministry of Education and Science under Grant HIII-4828.2012.2.
Предметные рубрики: GROWTH
Y1-XYBXAL3(BO3)4
LUMINESCENCE
FREQUENCY
CENTERS
Ключевые слова (''Своб.индексиров.''): ytterbium--aluminum borates--impurities--high-resolution spectroscopy--uv edge
Аннотация: A comparative study was performed of the low-temperature high-resolution absorption spectra of the Yb3+ probe in R1−xYbxAl3(BO3)4 (R = Y, Tm, Lu) crystals grown by flux technique independently in four different laboratories using different solvents. We show that the incorporation of solvent components into the crystal in the course of crystallization gives rise to spectral satellites of the Yb3+ 0(2F7/2) → 0′(2F5/2) absorption lines and assign particular satellites to the Yb3+ centers near the bismuth and molybdenum impurities (which decrease the transparency of YAB in the UV spectral range). We suggest this spectroscopic method for a rapid analysis of the quality of UV laser crystals and for improvement of growth technologies.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Cherepakhin A. V., Zaitsev A. I., Aleksandrovsky A. S., Zamkov A. V.
Заглавие : Optical and nonlinear optical properties of orthorhombic BiB3O6
Место публикации : Opt. Mater.: Elsevier Science BV, 2012. - Vol. 34, Is. 5. - P.790-792. - ISSN 0925-3467, DOI 10.1016/j.optmat.2011.11.004
Примечания : Cited References: 13. - The work was supported by Ministry of Education and Science of Russian Federation (Contract 16.740.11.0150), Grant of President of Russian Federation for support of leading scientific schools No. SS-4645.2010.2, Grant No. RNP.2.1.1.3455, Project 3.9.1 of PSB RAS, and Projects No. 27.1 and No. 5 of SB RAS.
Предметные рубрики: BISMUTH BORATE BIB3O6
CRYSTAL
LASER
GENERATION
GROWTH
BIBO
Ключевые слова (''Своб.индексиров.''): orthorhombic bismuth triborate delta-bibo--refractive indices--nonlinear optical coefficients--nonlinear optical materials--phase matching
Аннотация: Dispersion of refraction coefficients of orthorhombic BiB3O6 in the wavelength range between 435.8 and 1060 nm is studied, nonlinear optical coefficients are determined, and phase matching angles, angular and spectral bandwidths for second harmonic generation processes are calculated. delta-BiBO may be suitable for doubling of lasers with a wavelength in the 1.3 mu m region as well as the matrix for self-doubling lasing media. (C) 2011 Elsevier B.V. All rights reserved.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Malakhovskii A. V., Kutsak T. V., Sukhachev A. L., Aleksandrovsky A. S., Krylov A. S., Gudim, Irina A., Molokeev M. S.
Заглавие : Spectroscopic properties of ErAl3(BO3)4 single crystal
Место публикации : Chem. Phys.: Elsevier Science, 2014. - Vol. 428. - P.137–143. - ISSN 0301-0104, DOI 10.1016/j.chemphys.2013.11.008. - ISSN 1873-4421
Примечания : Cited References: 43. - The work was supported by the Russian Foundation for Basic Researches grant 12-02-00026, by the Russian President Grants SS-1044.2012.2 and 4828.2012.2, by project No 3.9.5 PSB RAS, and by the Ministry of Education and Science of Russian Federation grant 8365
Предметные рубрики: RARE-EARTH IONS
GREEN UP-CONVERSION
ER3+ IONS
MICROCHIP LASER
ABSORPTION INTENSITIES
YAL3(BO3)4 CRYSTAL
OPTICAL-ABSORPTION
FIELD ANALYSIS
GROWTH
LUMINESCENCE
Ключевые слова (''Своб.индексиров.''): rare earth compounds--er3+--spectroscopic properties--judd-ofelt analysis--luminescence
Аннотация: Single crystal of ErAl3(BO3)4 was grown and its structure was studied. Polarized absorption spectra of ErAl3(BO3)4 single crystal were measured in the spectral range 1670–330 nm (6000–30000 cm−1). The Judd–Ofelt spectroscopic parameters have been determined: Ω2 = 4.87 × 10−20 cm2, Ω4 = 2.49 × 10−20 cm2, Ω6 = 2.72 × 10−20 cm2. These parameters have been used to calculate the radiative transition probabilities, the multiplet luminescence branching ratios and the fluorescence life times of the manifolds. The luminescence spectra due to transitions 2H11/2 → 4I15/2 (526 nm), 4S3/2 → 4I15/2 (548 nm), 4F9/2 → 4I15/2 (662 nm), 2H11/2 → 4I13/2 + 4I9/2 → 4I15/2 (800 nm) and 4S3/2 → 4I13/2 (855 nm) were recorded in α, σ and π polarizations. The most intensive luminescence belonged to 4S3/2 → 4I15/2 transition (548 nm).Поляризованные спектры поглощения ErAl3 (BO3) 4 монокристалла были измерены в спектральном диапазоне 1670-330 нм (6000-30000 см-1). Спектроскопические параметры Джадда-Офельта были определены как: Ω2 = 4,87 • 10-20 см2, Ω4 = 2.49 • 10-20 см2, Ω6 = 2,72 • 10-20 см2. Параметры были использованы для расчета вероятностей излучающих переходов, мультиплетные отношения люминесценции раскола и времена жизни мультиплетов. Спектры люминесценции за счет переходов 2П11 / 2 → 4I15 / 2 (526 нм), 4S3 / 2 → 4I15 / 2 (548 нм), 4F9 / 2 → 4I15 / 2 (662 нм), 2П11 / 2 → 4I13 / 2 + 4I9 / 2 → 4I15 / 2 (800 нм) и 4S3 / 2 → 4I13 / 2 (855 нм) были записаны в α, σ и π поляризации. Наиболее интенсивное свечение принадлежало переходу 4S3 / 2 → 4I15 / 2 (548 нм).
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Ikonnikov D. A., Malakhovskii A. V., Sukhachev A. L., Zaitsev A. I., Aleksandrovsky A. S., Jubera V.
Заглавие : Spectroscopic properties of Nd3+ in orthorhombic δ-BiB3O6 crystal
Место публикации : Opt. Mater.: ELSEVIER SCIENCE BV, 2012. - Vol. 34, Is. 11. - P.1839-1842. - ISSN 0925-3467, DOI 10.1016/j.optmat.2012.05.016
Примечания : Cited References: 23. - The work was supported by Ministry of Education and Science of Russian Federation (Contract 16.740.11.0150), by Russian Foundation for Basic Researches Grant 12-02-00026, Grant of President of Russian Federation for support of leading scientific schools No. SS-4828.2012.2, Grant No. SFU.F12, and Projects No. 28, 43 and No. 101 of SB RAS.
Предметные рубрики: SPECTRAL-LINE INTENSITIES
RARE-EARTH IONS
LASER CRYSTAL
NdAl3(BO3)(4) NAB
OPTICAL-SPECTRA
BiB3O6
SYSTEMS
GROWTH
Er3+
Tm3+
Ключевые слова (''Своб.индексиров.''): neodymium--orthorhombic bismuth triborate--absorption--judd-ofelt analysis
Аннотация: Absorption spectra of the Nd3+ ions in an orthorhombic δ-BiB3O6 single crystal were measured in the spectral range 11,000-20,500 cm-1. The f-f transition intensities were analyzed in terms of the Judd-Ofelt theory, and the following parameters of the theory were obtained: Ω2 = 6.35 × 10-20 cm2, Ω4 = 4.86 × 10-20 cm 2, and Ω6 = 11.233 × 10-20 cm 2. The strengths, spontaneous emission probabilities, branching ratios, spectroscopic quality factor and excited state radiative lifetime were calculated for laser transitions from the 4F3/2 state to 4IJ manifold. Spectroscopic properties of Nd 3+:δ-BiB3O6 crystal favor lasing at 1.3 μm, where this crystal possesses near non-critical phase matching for second harmonic generation. © 2012 Elsevier B.V. All rights reserved.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Melnikova S. V., Isaenko L. I.
Заглавие : Linear optical properties of γ-modification of bismuth borate BiB3O6
Место публикации : Phys. Solid State: MAIK Nauka-Interperiodica / Springer, 2012. - Vol. 54, Is. 10. - P.1966-1969. - ISSN 1063-7834, DOI 10.1134/S1063783412100228
Примечания : Cited References: 9. - This study was supported by the Council on Grants from the President of the Russian Federation for Support of Leading Scientific Schools of the Russian Federation (grant no. NSh-4828.2012.2) and the Siberian Branch of the Russian Academy of Science (integration project no. 28).
Предметные рубрики: GROWTH
Аннотация: The refractive index dispersion of the γ-BiB3O6 crystal in the wavelength range 0.43–0.81 μm has been measured. It has been shown that the principal refractive indices n 1, n 2, and n 3 are on average higher than those of α-BiB3O6, but are slightly lower than those of δ-BiB3O6. The temperature dependences of the rotation angle φ(T) of the optical indicatrix and birefringence Δn 2(T) = (n 1 − n 3)(T) have been studied in the temperature range 100–963 K. It has been shown that the γ-BiB3O6 crystal is stable in this temperature region.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Varnakov S. N., Gomoyunova M. V., Grebenyuk G.S ., Zabluda V. N., Ovchinnikov S. G., Pronin I. I.
Заглавие : Solid-phase synthesis of manganese silicides on the Si(100)2 x 1 surface
Коллективы : Russian-German Laboratory at HZB BESSY; Russian Foundation for Basic Research [13-02-00398, 13-02-01265]; Council on Grants from the President of the Russian Federation for Support of the Leading Scientific Schools [NSh-1044.2012.2]; Siberian Branch of the Russian Academy of Sciences [85]; Ural Branch of the Russian Academy of Sciences [85]
Место публикации : Phys. Solid State: MAIK Nauka-Interperiodica / Springer, 2014. - Vol. 56, Is. 4. - P.812-815. - ISSN 1063-7834, DOI 10.1134/S1063783414040337. - ISSN 1090-6460
Примечания : Cited References: 20. - This study was supported by the Russian-German Laboratory at HZB BESSY, the Russian Foundation for Basic Research (project nos. 13-02-00398 and 13-02-01265), the Council on Grants from the President of the Russian Federation for Support of the Leading Scientific Schools (grant no. NSh-1044.2012.2), and the Integration Project No. 85 of the Siberian and Ural Branches of the Russian Academy of Sciences.
Предметные рубрики: PHOTOELECTRON-SPECTROSCOPY
GROWTH
FILMS
Аннотация: The solid-phase synthesis of manganese silicides on the Si(100)2 × 1 surface coated at room temperature by a 2-nm-thick manganese film has been investigated using high-energy-resolution photoelectron spectroscopy with synchrotron radiation. The dynamics of variation of the phase composition and electronic structure of the near-surface region with increasing sample annealing temperature to 600°C, has been revealed. It has been shown that, under these conditions, a solid solution of silicon in manganese, metallic manganese monosilicide MnSi, and semiconductor silicide MnSi1.7 are successively formed on the silicon surface. The films of both silicides are not continuous, with the fraction of the substrate surface occupied by them decreasing with increasing annealing temperature. The binding energies of the Si 2p and Mn 3p electrons in the compounds synthesized have been determined.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Shi P. L., Xia, Zhiguo, Molokeev M. S., Atuchin V. V.
Заглавие : Crystal chemistry and luminescence properties of red-emitting CsGd1−xEux(MoO4)2 solid-solution phosphors
Место публикации : Dalton Trans.: Royal Society of Chemistry, 2014. - Vol. 43, Is. 25. - P.9669-9676. - ISSN 1477-9226, DOI 10.1039/C4DT00339J. - ISSN 1477-9234
Примечания : Cited References: 46. - The present work was supported by the National Natural Science Foundations of China (grant no. 51002146, 51272242), Natural Science Foundations of Beijing (2132050), the Program for New Century Excellent Talents in University of Ministry of Education of China (NCET-12-0950), Beijing Nova Program (Z131103000413047), Beijing Youth Excellent Talent Program (YETP0635), the Fundamental Research Funds for the Central Universities (2-9-2014-044), and the Funds of the State Key Laboratory of New Ceramics and Fine Processing, Tsinghua University (KF201306). V. V. A. gratefully acknowledges the Ministry of Education and Science of the Russian Federation for the financial support.
Предметные рубрики: WHITE-LIGHT
VIBRATIONAL PROPERTIES
HYDROTHERMAL SYNTHESIS
SINGLE-CRYSTALS
DIODES
EFFICIENCY
PHOTOLUMINESCENCE
CSGD(MOO4)2
MORPHOLOGY
GROWTH
Аннотация: Scheelite related alkali-metal rare-earth double molybdate compounds with a general formula of ALn(MoO4)2 can find wide application as red phosphors. The crystal chemistry and luminescence properties of red-emitting CsGd1−xEux(MoO4)2 solid-solution phosphors have been evaluated in the present paper. A detailed analysis of the structural properties indicates the formation of isostructural scheelite-type CsGd1−xEux(MoO4)2 solid-solutions over the composition range of 0 ≤ x ≤ 1. The photoluminescence emission (PL) and excitation (PLE) spectra, and the decay curves were measured for this series of compounds. The critical doping concentration of Eu3+ is determined to be x = 0.6 in order to realize the maximum emission intensity. The emission spectra of the as-obtained CsGd(1−x)Eux(MoO4)2 phosphors show narrow high intensity red lines at 592 and 615 nm upon excitation at 394 or 465 nm, revealing great potential for applications in white light-emitting diode devices.
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Tarasov I. A., Popov Z. I., Varnakov S. N., Molokeev M. S., Fedorov A. S., Yakovlev I. A., Fedorov D. A., Ovchinnikov S. G.
Заглавие : Optical characteristics of an epitaxial Fe3Si/Si(111) iron silicide film
Коллективы : Russian Foundation for Basic Research [13-02-01265, 14-02-31309]; Council of the President of the Russian Federation for Support of Young Scientists and Leading Scientific Schools [NSh-2886.2014.2]; Russian Ministry of Education and Science [02.G25.31.0043]; Presidium of the Russian Academy of Sciences [24.34]
Место публикации : JETP Letters. - 2014. - Vol. 99, Is. 10. - P.565-569. - ISSN 0021-3640, DOI 10.1134/S0021364014100105. - ISSN 1090-6487
Примечания : Cited References: 24. - This work was supported by the Russian Foundation for Basic Research (project nos. 13-02-01265 and 14-02-31309), by the Council of the President of the Russian Federation for Support of Young Scientists and Leading Scientific Schools (project no. NSh-2886.2014.2), by the Russian Ministry of Education and Science (state contract no. 02.G25.31.0043), and by the Presidium of the Russian Academy of Sciences (program no. 24.34).
Предметные рубрики: INITIO MOLECULAR-DYNAMICS
AUGMENTED-WAVE METHOD
N-K PLANE
GROWTH
FE3-XMNXSI
Аннотация: The dispersion of the relative permittivity E of a 27-nm-thick epitaxial Fe3Si iron silicide film has been measured within the E = 1.16-4.96 eV energy range using the spectroscopic ellipsometry technique. The experimental data are compared to the relative permittivity calculated in the framework of the density functional theory using the GGA-PBE approximation. For Fe3Si, the electronic structure and the electronic density of states (DOS) are calculated. The analysis of the frequencies corresponding to the transitions between the DOS peaks demonstrates qualitative agreement with the measured absorption peaks. The analysis of the single wavelength laser ellipsometry data obtained in the course of the film growth demonstrates that a continuous layer of Fe3Si iron silicide film is formed if the film thickness achieves 5 nm.
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11.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Denisov V. M., Denisova L. T., Gudim, I. A., Temerov V. L., Patrin G. S., Volkov N. V., Chumilina L. G.
Заглавие : High-temperature heat capacity of YbAl3(BO3)4
Место публикации : Russ. J. Phys. Chem. A: MAIK Nauka-Interperiodica / Springer, 2014. - Vol. 88, Is. 8. - P.1436-1437. - ISSN 0036-0244, DOI 10.1134/S0036024414080093. - ISSN 1531-863X
Примечания : Cited References: 14
Предметные рубрики: SINGLE-CRYSTALS
OPTICAL-PROPERTIES
LASER CRYSTAL
YAl3(BO3)4
GROWTH
Ключевые слова (''Своб.индексиров.''): ytterbium aluminum borate--high-temperature heat capacity--thermodynamic properties
Аннотация: The isobaric heat capacity Cp(T) of YbAl3(BO3)4 grown by spontaneous crystallization from solution (100 − n) wt % (Bi2Mo3O12 + 2.5% B2O3 + 0.75% Li2MoO4) + n wt % YbAl3(BO3)4 is studied experimentally in the region of 344–1016 K. It is established that there are no extrema on the Cp(T) dependence, and the obtained data can be described using the Berman-Brown polynomial. The temperature variations of enthalpy and entropy are calculated from the Cp(T) dependence.
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12.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Malakhovskii A. V., Sukhachev A. L., Sokolov V. V., Kutsak T. V., Bondarev V. S., Gudim, I. A.
Заглавие : Magneto-optical activity of f–f transitions in ErFe3(BO3)4 and ErAl3(BO3)4 single crystals
Коллективы : Russian Foundation for Basic Researches [12-02-00026], President of Russia Grant [Nsh-2886.2014.2]
Место публикации : J. Magn. Magn. Mater.: Elsevier, 2015. - Vol. 384. - P.255-265. - ISSN 0304-8853, DOI 10.1016/j.jmmm.2015.02.051. - ISSN 1873-4766
Примечания : Cited References: 44. - The work was supported by the Russian Foundation for Basic Researches Grant 12-02-00026 and by the President of Russia Grant no. Nsh-2886.2014.2.
Предметные рубрики: CIRCULAR-DICHROISM SPECTRA
GREEN UP-CONVERSION
SPECTROSCOPIC PROPERTIES
OPTICAL-PROPERTIES
LASER
Er3+
ABSORPTION
GROWTH
IONS
GdFe3(BO3)4
Ключевые слова (''Своб.индексиров.''): magnetic circular dichroism--natural circular dichroism--rare earth ferroborates--rare earth alumoborates--electronic structure
Аннотация: Absorption, magnetic circular dichroism and natural circular dichroism spectra of ErFe3(BO3)4 and ErAl3(BO3)4 single crystals were measured as a function of temperature in the range of 90–293 K. It was found out that magneto-optical activity of the same f–f transitions in the studied crystals substantially differed and their temperature dependences did not follow the Curie–Weiss law in contrast to the properties of allowed transitions. The observed phenomena were accounted for by the nature of f–f transitions allowance. Properties of the transition 4I15/2→4S3/2 were studied in detail. In particular, the Zeeman splitting and the natural optical activity of the absorption lines composed of the transition were determined. The vibronic line with the very large natural optical activity was revealed and identified. Two nonequivalent Er3+ ion positions with the opposite chirality were found out in one of the excited states. Polarization properties of the 4I15/2→4S3/2 transition in the ErFe3(BO3)4 crystal have shown that the local symmetry of Er3+ ion in this crystal in the range of 90–293 K is lower than the D3 one. From the heat capacity measurements it was revealed, that the first order structural phase transition to lower symmetry occurred in ErFe3(BO3)4 at 433–439 K.Поглощение, магнитный циркулярный дихроизм и спектры природного кругового дихроизма монокристаллов ErFe3(BO3)4 и ErAl3(BO3)4 были измерены в зависимости от температуры в диапазоне 90-293 К. Было обнаружено, что по магнитооптической активности одни и те жеF-F переходы в исследованных кристаллах существенно отличаются и их температурные зависимости не следовать закону Кюри-Вейсса в отличие от свойств разрешенных переходов. Наблюдаемые явления были учтены по характеру F-Fпереходов. Свойства перехода 4I15 / 2 → 4S3 / 2 были детально изучены. В частности, расщепление Зеемана и явление естественной оптической активности линий поглощения, состоящих в переходе были полны решимости. Вибронная линия очень большой естественной оптической активности выявлена и идентифицирована. Две неэквивалентных позиций ионовEr3 + с противоположной хиральности были найдены в одном из возбужденных состояний. Поляризационные свойства 4I15 / 2 → 4S3 / 2 перехода в ErFe3(BO3)4 кристалла показали, что локальная симметрия ионов Er3 + в этом кристалле в диапазоне 90-293 К ниже, чем D3. Из измерений теплоемкости Было обнаружено, что структурный фазовый переход первого типа к более низкой симметрии произошел в ErFe3(BO3) 4 при 433-439 К. Ключевые слова: Магнитный круговой дихроизм; Природные круговой дихроизм; Редкоземельные ферроборатов; Редкоземельныеalumoborates; Электронная структура; 44 источника.
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13.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Glushchenko G. A., Leonova T. A., Kolonenko A. L., Dudnik A. I., Osipova I. V., Vnukova N. G., Nemtsev I. V., Zharkov S. M., Churilov G. N.
Заглавие : Synthesis of 6H-SiC single-crystal nanowires in a flow of carbon-silicon high-frequency arc plasma
Место публикации : Phys. Solid State: Pleiades Publishing, 2014. - Vol. 56, Is. 10. - P.2107-2111. - ISSN 1063-7834, DOI 10.1134/S106378341410014X. - ISSN 1090-6460
Примечания : Cited References: 34. - This study was supported by the National Academy of Sciences of Belarus and the Siberian Branch of the Russian Academy of Sciences within the framework of the Interdisciplinary Integration project no. 24.
Предметные рубрики: LARGE-SCALE SYNTHESIS
BETA-SIC NANOWIRES
FIELD-EMISSION PROPERTIES
CARBIDE NANOWIRES
NANORODS
GROWTH
NANOSTRUCTURES
FULLERENES
DISCHARGE
Аннотация: Silicon carbide 6H-SiC nanoparticles and nanowires were obtained in carbon-silicon high-frequency arc plasma plasma in a helium atmosphere at a pressure of 0.1-0.6 MPa. It was shown that 6H-SiC nanowires grow from the arc plasma, as well as from the vapor, according to the known mechanism of vapor-solid condensation on a cold surface covered with single-crystal silicon carbide nuclei. The content of silicon carbide nanowires in the condensate reached 60 wt %. The obtained single-crystal silicon 6H-SiC nanowires had the diameter of 15-18 nm and length of 200-600 nm.
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14.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Isaenko L. I., Yelisseyev A. P., Lobanov S. I., Krinitsin P. G., Molokeev M. S.
Заглавие : Structure and optical properties of Li2Ga2GeS6 nonlinear crystal
Коллективы : Russian Foundation of Basic Research [15-02-03408a]
Место публикации : Opt. Mater.: Elsevier Science, 2015. - Vol. 47. - P.413-419. - ISSN 0925-3467, DOI 10.1016/j.optmat.2015.06.014
Примечания : Cited References:23. - This work was supported by the Russian Foundation of Basic Research (Grant No. 15-02-03408a)
Предметные рубрики: PHASE-MATCHING PROPERTIES
MID-IR
PARAMETRIC AMPLIFICATION
GENERATION
LiGaS2
GROWTH
DAMAGE
Ga
Te
Se
Ключевые слова (''Своб.индексиров.''): li2ga2ges6--structure--absorption--raman--luminescence--excitons
Аннотация: Structure and optical properties of new nonlinear crystal - Li2Ga2GeS6 single crystal of optical quality, grown by the Bridgman technique were studied. The data on transmission, Raman scattering, luminescence emission, excitation and thermal quenching as well as thermostimulated luminescence are presented. Fundamental absorption edge is determined by the direct allowed electronic transitions: The values of optical band gap are estimated. Absorption band at 8.0 mu m is due to S-S vibrations. Features in photoluminescence spectra are associated with excitons: both free (narrow line at 371 nm) and self-trapped ones (broad bands at 596, 730 and 906 nm). Spontaneous emission in the 80-170 K range, both at crystal heating and cooling, is typical of pyroelectrics: This confirms the absence of symmetry center in Li2Ga2GeS6 and an opportunity of laser frequency nonlinear conversion. (C) 2015 Elsevier B.V. All rights reserved.
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15.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Atuchin V. V., Beisel N. F., Galashov E. N., Mandrik E. M., Molokeev M. S., Yelisseyev A. P., Yusuf A. A., Xia Z.
Заглавие : Pressure-stimulated synthesis and luminescence properties of microcrystalline (Lu,Y)3Al5O12:Ce3+ garnet phosphors
Место публикации : ACS Appl. Mater. Interfaces: American Chemical Society, 2015. - Vol. 7, Is. 47. - P.26235-26243. - ISSN 19448244 (ISSN), DOI 10.1021/acsami.5b08411
Примечания : Cited References: 75. - This work was partly supported by the National Natural Science Foundations of China (Grant Nos. 51272242 and 51511130035) and the Russian Foundation for Basic Research (Grant No. 15-52-53080 GFEN_a). V.V.A. was partly supported by the Ministry of Education and Science of the Russian Federation
Предметные рубрики: LASER MASS-SPECTROMETRY
LIGHT-EMITTING-DIODES
WHITE-LIGHT
SINGLE-CRYSTALS
OPTICAL-PROPERTIES
ELECTRONIC-STRUCTURE
VIBRATIONAL PROPERTIES
PHASE-TRANSITIONS
PARTICLE-SIZE
GROWTH
Ключевые слова (''Своб.индексиров.''): synthesis--pressure--garnet--structure--luminescence--phosphor
Аннотация: The Lu2.98Ce0.01Y0.01Al5O12 and Y2.99Ce0.01Al5O12 phosphors were synthesized by solid state reaction at temperature 1623 K and pressure 1.5 × 107 Pa in (95% N2 + 5% H2) atmosphere. Under the conditions, the compounds crystallize in the form of isolated euhedral partly faceted microcrystals ∼19 μm in size. The crystal structures of the Lu2.98Ce0.01Y0.01Al5O12 and Y2.99Ce0.01Al5O12 garnets have been obtained by Rietveld analysis. The photoluminescence (PL) and X-ray excited luminescence (XL) spectra obtained at room temperature indicate broad asymmetric bands with maxima near 519 and 540 nm for Y2.99Ce0.01Al5O12 and Lu2.98Ce0.01Y0.01Al5O12, respectively. The light source was fabricated using the powder Lu2.98Ce0.01Y0.01Al5O12 phosphor and commercial blue-emitting n-UV LED chips (λex = 450 nm). It is found that the CIE chromaticity coordinates are (x = 0.388, y = 0.563) with the warm white light emission correlated color temperature (CCT) of 6400 K and good luminous efficiency of 110 lm/W. © 2015 American Chemical Society.
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16.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Frolov K. V., Lyubutin I. S., Smirnova E. S., Alekseeva O. A., Verin I. A., Artemov V. V., Kharlamova S. A., Bezmaternykh L. N., Gudim, I. A.
Заглавие : Low-temperature structural and magnetic phase transitions in multiferroic GdFe3(BO3)4
Коллективы : Russian Foundation for Basic Research [14-02-00483a, 13-02-12442]; Council on Grants from the President of the Russian Federation for Support of Leading Scientific Schools [NSh-1130.2014.5, NSh-924.2014.2]; Russian Ministry of Education and Science [RFMEFI62114X0005]
Место публикации : J. Alloys Compd.: Elsevier Science, 2016. - Vol. 671. - P.545-551. - ISSN 0925-8388, DOI 10.1016/j.jallcom.2016.02.083. - ISSN 1873-4669(eISSN)
Примечания : Cited References:36. - We thank Dr. A.P. Dudka for help in the low temperature XRD measurements. This study was supported in part by the Russian Foundation for Basic Research (projects # 14-02-00483a and 13-02-12442), and the Council on Grants from the President of the Russian Federation for Support of Leading Scientific Schools (grant # NSh-1130.2014.5 and # NSh-924.2014.2). This work was performed using the equipment of the Shared Research Center IC RAS and was supported by the Russian Ministry of Education and Science (project RFMEFI62114X0005).
Предметные рубрики: IRON BORATE GDFE3(BO3)4
BIFEO3 THIN-FILMS
MAGNETOELASTIC PROPERTIES
RM3(BO3)4 CRYSTALS
TRIGONAL GDFE3(BO3)4
ENHANCED POLARIZATION
HIGH-PRESSURES
CRYSTALLIZATION
BEHAVIOR
GROWTH
Ключевые слова (''Своб.индексиров.''): multiferroics--rare earth compounds--x-ray diffraction--mossbauer--spectroscopy--crystal structure--spin dynamics
Аннотация: X-ray analysis revealed that at temperature decreasing from room temperature to Tstr = 155 K the crystal unit cell GdFe3(BO3)4 is reduced only along the c axis (at 0.01 Å), while the a and b axes are unchanged within the error limits. The volume of the crystal decreases uniformly in the direction of all three axes at 155–80 K. At 80–30 K the crystal volume is decreased only by reduction of the parameters a and b, while the parameter c increases conversely. In the paramagnetic region Mössbauer spectra do not distinguish between the two structural positions of iron ions Fe1 and Fe2, appearing at T < Tstr. Below the temperature of the magnetic phase transition at TN = 38.0(1) K the Mössbauer data indicate quasi-one-dimensional magnetic ordering of iron moments in the sublattice Fe2 and a two-dimensional one in the iron sublattice Fe1. The dynamics of spin reorientation in sublattices Fe1 and Fe2 is studied in detail.Рентгеновский анализ показал, что при уменьшении температуры от комнатной до Tstr = 155 K изменение параметра элементарной ячейки кристалла GdFe3(BO3)4 происходит лишь вдоль оси с (при 0,01 Å), в то время как а и b оси остаются неизменными в пределах погрешности измерений. Объем кристалла уменьшается равномерно в направлении всех трех осей при 155-80 K. При 80-30 K объем кристалла уменьшается только уменьшением параметров a и b, в то время как параметр с наоборот увеличивается. В парамагнитной области Мессбауэровские спектры не различают двух структурных позиций ионов железа Fe1 и Fe2, появляющиеся при Т˂Tstr. Ниже температуры магнитного фазового перехода при TN = 38,0(1) К Мёссбауэрские данные указывают на квази-одномерный магнитное упорядочение моментов железа в подрешетке Fe2 и двумерное в железной подрешетке Fe1. Динамика спиновой переориентации в подрешетках Fe1 и Fe2 подробно изучается.
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17.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Altin S., Gokhfeld D. M.
Заглавие : Magnetization loops and pinning force of Bi-2212 single-crystal whiskers
Место публикации : Physica C. - 2011. - Vol. 471, Is. 7-8. - P.217-221. - ISSN 0921-4534, DOI 10.1016/j.physc.2011.01.006
Примечания : Cited References: 40. - The work is supported by Project No. 7 of RAS Program "Quantum physics of condensed matter", Grant No. 13 of Lavrentyev competition of young researchers of SB RAS and Scientific and Technical Research Council of Turkey (TUBITAK) under Contract No. TUBITAK-109T747.
Предметные рубрики: T-C SUPERCONDUCTORS
HIGH-TEMPERATURE SUPERCONDUCTORS
JOSEPHSON VORTICES
GROWTH
BI2SR2CACU2O8+DELTA
DENSITY
STATE
FIELD
MELT
Ключевые слова (''Своб.индексиров.''): bi-2212--whisker--magnetization loop--pinning force--extended critical state model--bi-2212--extended critical state model--magnetization loop--pinning force--whisker--bi-2212--extended critical state model--magnetization loop--pinning force--whisker--flux pinning--magnetic fields--magnetization--critical current density (superconductivity)
Аннотация: Dependence of magnetization on applied magnetic field for single-crystal Bi-2212 whiskers was measured at different temperatures. Symmetric and asymmetric magnetization loops were successfully described by the extended critical state model (the extended Valkov-Khrustalev model). Pinning force of whiskers was investigated. (C) 2011 Elsevier B.V. All rights reserved.
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18.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mel'nikova S. V., Isaenko L. I., Gorev M. V., Vasil'ev A. D., Lobanov S. I.
Заглавие : Investigation of the structure, physical properties, and phase transition in SrAlF5
Коллективы :
Место публикации : Phys. Solid State: MAIK NAUKA/INTERPERIODICA/SPRINGER, 2010. - Vol. 52, Is. 3. - P509-514. - ISSN 1063-7834, DOI 10.1134/S1063783410030108
Примечания : Cited References: 16. - This study was supported by the Russian Foundation for Basic Research (project no. 07-02-00442) and the Siberian Branch of the Russian Academy of Sciences within the framework of the Interdisciplinary Integration Project No. 34.
Предметные рубрики: CRYSTAL-STRUCTURE
BEHAVIOR
GROWTH
SRAIF5
Аннотация: Crystals of SrAlF5 have been grown by the Bridgman method from the melt and by sintering of the components. Optical polarization studies and measurements of the thermal expansion and birefringence coefficients have been carried out over a wide temperature range. The electromechanical coefficient d (33) has been measured, and the optical second harmonic, dielectric hysteresis loop, and optical quality of the crystal have been assessed. X-ray diffraction investigations have been performed to identify the revealed compounds. It has been demonstrated that the SrAlF5 crystals obtained under the growth conditions chosen have I4(1)/a symmetry and do not undergo structural phase transitions in the temperature range 100-800 K. Crystalline inclusions of the AlOF oxyfluoride have been revealed in crystals grown with an AlF3 excess. The birefringence of the AlOF crystal is an order of magnitude higher than that of SrAlF5, does not depend on temperature, and has no anomalies up to 800 K.
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19.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Myagkov V. G., Bykova L. E., Bondarenko G., Zhigalov V. S.
Заглавие : Solid-phase synthesis of solid solutions in Cu/Ni(001) epitaxial nanofilms
Коллективы :
Место публикации : JETP Letters. - 2008. - Vol. 88, Is. 8. - P.515-519. - ISSN 0021-3640, DOI 10.1134/S0021364008200101
Примечания : Cited References: 30. - This work was supported by Russian Foundation for Basic Research (project no. 07-03-00190).
Предметные рубрики: HIGH-TEMPERATURE SYNTHESIS
CU-NI SYSTEM
THIN-FILMS
MARTENSITIC TRANSFORMATIONS
MAGNETIC-PROPERTIES
MULTILAYERED FILMS
ATOM-PROBE
STABILITY
GROWTH
INTERDIFFUSION
Аннотация: Solid-phase synthesis of solid solutions in the epitaxial Cu/Ni(001) bilayer film systems of compositions 3Cu: 1Ni, 1Cu: 1Ni, and 1Cu: 3Ni has been studied using the X-ray diffraction methods. The saturation magnetization and the magnetic crystallographic anisotropy constant on nickel vary in accordance with the solid solution formation. The initiation temperature of the solid solutions is about 350 A degrees C and is independent of the Ni: Cu layer thickness ratio. The solid-phase synthesis of the solid solutions is presumably attributed to the transport of the Cu atoms to the epitaxial Ni(001) layer. It is found that the solid-phase synthesis in the Cu/Ni bilayer nanofilms and multilayers is determined by the spinodal decomposition in the Cu-Ni system.
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20.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Popova M. N., Boldyrev K. N., Petit P. O., Viana B., Bezmaternykh L. N.
Заглавие : High-resolution spectroscopy of YbAl(3)(BO(3))(4) stoichiometric nonlinear laser crystals
Коллективы :
Разночтения заглавия :авие SCOPUS: High-resolution spectroscopy of YbAl3(BO3) 4 stoichiometric nonlinear laser crystals
Место публикации : J. Phys.: Condens. Matter: IOP PUBLISHING LTD, 2008. - Vol. 20, Is. 45. - Ст.455210. - ISSN 0953-8984, DOI 10.1088/0953-8984/20/45/455210
Примечания : Cited References: 20. - The authors thank E Antic-Fidancev for helpful discussions on the 'barycenter curves', P Aschehoug for technical assistance, and B Mavrin for assistance in Raman spectra measurements. This work was supported by the CNRS-RAS exchange program (project No. 21241), by the Russian Foundation for Basic Research (Grants Nos 07-02-01185 and 06-02-16088), and by the Russian Academy of Sciences under the Programs for Basic Research.
Предметные рубрики: YB-YAB LASER
GROWTH
FREQUENCY
BORATE
Ключевые слова (''Своб.индексиров.''): crystal symmetry--crystals--light emission--light sources--luminescence--spectroscopic analysis--ytterbium--electronic levels--high resolutions--luminescence spectroscopies--main lines--nonlinear laser crystals--raman spectrums--vibronic structures--weak lines--single crystals
Аннотация: We present temperature-dependent high-resolution polarized transmittance spectroscopy as well as luminescence spectroscopy of YbAl(3)(BO(3))(4) single crystals. Positions and symmetries of all the Yb(3+) crystal-field electronic levels have been found from the analysis of the spectra. Near the main line of the optical transition (2)F(7/2)(0) - (2)F(5/2)(0) we observe a lot of narrow weak lines. These lines point to the presence of several different distorted sites of Yb(3+). We analyze the possible origin of the distorted sites. Vibronic structure in transmittance and luminescence spectra was observed and compared with room-temperature Raman spectra.
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