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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Kirillov V. L., Balaev D. A., Semenov S. V., Shaikhutdinov K. A., Martyanov O. N.
Заглавие : Size control in the formation of magnetite nanoparticles in the presence of citrate ions
Коллективы : Siberian Branch of the Russian Academy of Sciences
Место публикации : Mater. Chem. Phys.: Elsevier Science, 2014. - Vol. 145, Is. 1-2. - P.75-81. - ISSN 0254-0584, DOI 10.1016/j.matchemphys.2014.01.036. - ISSN 1879-3312
Примечания : Cited References: 46. - This work was supported by the Interdisciplinary Integration Project no. 45 of the Siberian Branch of the Russian Academy of Sciences for 2012-2014.
Предметные рубрики: OLEIC-ACID
CATALYST
HYPERTHERMIA
PARTICLES
OXIDATION
REMOVAL
CO
Ключевые слова (''Своб.индексиров.''): magnetic materials--magnetic properties--precipitation--electron paramagnetic resonance
Аннотация: A one-pot synthesis method for the controllable growth of magnetite nanoparticles directly during the process of co-precipitation using citrate ions was developed. The effects of the concentration of citrate ions and the solution pH on the characteristics of magnetite particles with sizes in the range of 4-10 nm synthesized by the method of co-precipitation were studied. The results showed that the specified concentration of citrate ions allowed the preparation of magnetite particles with a definite size that exhibited superparamagnetic behaviour in a particular temperature range. As the concentration ratio of citrate to iron ions was increased from 0 to 0.11, the average size of the prepared magnetite particles decreased from 10.5 to 4.4 nm. As a result, the superparamagnetic blocking temperature decreased from 300 to 20 K, the saturation magnetisation decreased from 50 to 20 emu g(-1), and the average magnetic moment decreased from 8000 mu(B) to 340 mu(B) (at T = 300 K). The obtained experimental data proved that the size effects of the magnetite nanoparticles can be attributed to the capping of the magnetite surface by adsorbed citrate ions. Thus, the suggested approach allows magnetite nanoparticles to be prepared with an optimum particle size around superparamagnetic threshold that prevents their irreversible agglomeration and simultaneously allows them to be removed from a solution at an acceptable rate. (C) 2014 Elsevier B.V. All rights reserved.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Smolyarova T. E., Lukyanenko A. V., Tarasov A. S., Sokolov A. Е.
Заглавие : Dip-Pen Nanolithography method for fabrication of biofunctionalized magnetic nanodiscs applied in medicine
Коллективы : International Symposium on Nanostructures - Physics and Technology , Russian Foundation for Basic Research, Government of Krasnoyarsk Territory, Krasnoyarsk Region Science and Technology Support Fund [17-42-240080, 16-42-243046, 16-42-242036]; Russian Federation [NSh-7559.2016.2]
Место публикации : Semiconductors. - 2018. - Vol. 52: 25th International Symposium on Nanostructures - Physics and Technology (Jun 26-30, 2017, Saint Petersburg, Russia), Is. 5. - P.675-677. - ISSN 1063-7826, DOI 10.1134/S1063782618050305. - ISSN 1090-6479(eISSN)
Примечания : Cited References:22. - The study was funded by Russian Foundation for Basic Research, Government of Krasnoyarsk Territory, Krasnoyarsk Region Science and Technology Support Fund to the research project nos. 17-42-240080, 16-42-243046, 16-42-242036 and the Grant of the President of the Russian Federation no. NSh-7559.2016.2.
Предметные рубрики: DRUG-DELIVERY
FORCE MICROSCOPY
NANOPARTICLES
HYPERTHERMIA
THERAPY
Аннотация: The magnetic properties of ferromagnetic nanodiscs coated with gold, manufactured using the Dip-Pen Nanolithography method, and were studied by atomic-force and magnetic force microscopy methods. The magnetic discs (dots) are represented as nanoagents (nanorobots) applied in medicine for the cancer cell destruction. The motivation of this work stem from the necessity of the understanding of the magnetization distribution in ferromagnetic discs that is crucial for their application in biomedicine. We have performed the theoretical calculations in order to compare the theoretical image contrast to experimental results. Herein, we report about the fabrication and analysis of biocompatible ferromagnetic nanodiscs with the homogenous magnetized state.
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