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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Petrov M. I., Balaev D. A., Gokhfel'd Yu. S., Dubrovskii A. A., Shaikhutdinov K. A.
Заглавие : Effect of heterovalent substitution of rare-earth elements on the magnetic and transport properties of YBa2Cu3O7
Место публикации : Phys. Solid State: MAIK NAUKA/INTERPERIODICA/SPRINGER, 2007. - Vol. 49, Is. 11. - P2047-2051. - ISSN 1063-7834, DOI 10.1134/S1063783407110054
Примечания : Cited References: 18
Предметные рубрики: PR
SUPERCONDUCTIVITY
CE
ND
TRANSITION
SYSTEM
LA
Аннотация: The Y(1-x) Ce (x) Ba2Cu3O7 system with low cerium concentrations has been synthesized. The cerium solubility limit measured using x-ray powder diffraction analysis is about 2.4 at. %. The temperature dependences of the magnetization M(T) are measured for samples cooled in a magnetic field (FC) and in a zero field (ZFC). The difference between the magnetizations M-ZFC-M-FC at 77.4 K, which is proportional to the pinning potential, passes through a maximum at x = 0.0156. This concentration corresponds to the average distance (equal to eight lattice constants) between the impurity ions in the plane of the rare-earth elements, which is comparable to the diameter of Abrikosov vortices in YBa2Cu3O7.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Shtarev D. S., Shtareva, A., V, Kevorkyants R., Rudakova, A., V, Molokeev M. S., Bakiev, T., V, Bulanin K. M., Ryabchuk V. K., Serpone N.
Заглавие : Materials synthesis, characterization and DFT calculations of the visible-light-active perovskite-like barium bismuthate Ba1.264(4)Bi1.971(4)O4 photocatalyst
Коллективы : Russian Science FoundationRussian Science Foundation (RSF) [19-73-10013]; Saint-Petersburg State University [39054581]; Russian Foundation for Basic ResearchRussian Foundation for Basic Research (RFBR) [18-03-00855]
Место публикации : J. Mater. Chem. C. - 2020. - Vol. 8, Is. 10. - P.3509-3519. - ISSN 2050-7526, DOI 10.1039/c9tc06457e. - ISSN 2050-7534(eISSN)
Примечания : Cited References: 42. - The current research was kindly funded by a grant from the Russian Science Foundation (project No. 19-73-10013). R. K., A. V. R., V. K. R. and T. V. B. acknowledge financial support from Saint-Petersburg State University (Pure ID 39054581). A. V. R. thanks the Russian Foundation for Basic Research for a Grant No. 18-03-00855 that supported studies into the photoinduced hydrophilicity of the bismuthate. The authors are further grateful to the staff of the Khabarovsk Innovation and Analytical Center of the Yu. A. Kosygin Institute of Tectonics and Geophysics of the Far Eastern Branch of the Russian Academy of Sciences, and the Resource Centers of the Research Park at the Saint-Petersburg State University: (i) the Center for Diagnostics of Functional Materials for Medicine, Pharmacology and Nanoelectronics, (ii) the Center for Physical Methods of Surface Investigation, (iii) the Center for Optical and Laser Materials Research, and the laboratories of (iv) Nanotechnology and (v) Nanophotonics for their valuable assistance in carrying out the research and in providing the needed equipment. One of us (N.S.) is grateful to Prof. Angelo Albini and the staff of the PhotoGreen Laboratory at the University of Pavia, Italy, for their continued hospitality.
Предметные рубрики: OXIDE
NIO/SRBI2O4
SPECTRA
DRIVEN
CO2
LA
Аннотация: A perovskite-like barium bismuthate of the BaBi2O4 class, Ba1.264(4)Bi1.971(4)O4, has been prepared by solid-state synthesis and subsequently characterized by a number of experimental techniques (XPS, DRS, SEM, EDX and Raman spectroscopy), as well as by a DFT computational approach using the GGA Perdew–Burke–Ernzerhof (PBE) density functional to determine the energy band structure. XRD peaks were indexed to a rhombohedral cell (R[3 with combining macron]m) with parameters close to Ba0.156Bi0.844O1.422 (i.e., to Ba0.439Bi2.374O4), which upon Rietveld refinement gave Ba1.264(4)Bi1.971(4)O4. The Bi–O bond lengths determined from this refinement (1.86 and 2.31 Å) accorded with the bond lengths estimated from Raman spectra (1.97 and 2.26 Å). DFT calculations revealed the bismuthate to display two bandgaps that correspond to lower-energy indirect (2.28 eV) and to higher-energy direct (2.36 eV) electronic transitions in good agreement with the experimental bandgaps of 2.26 eV and 2.43 eV, respectively, from Tauc plots of DRS spectra. Relative to the indirect bandgap energy of 2.26 eV, the energies of the valence band and of the conduction band were, respectively, +1.14 eV and −1.12 eV. The photoactivity of Ba1.264(4)Bi1.971(4)O4 was examined toward the photoreduction of the greenhouse gas CO2 in aqueous media photoelectrochemically yielding alcohols and alkanes, while in the gas phase in an infrared cell reactor the products were carbon monoxide and alkanes.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Denisenko, Yu. G., Sal'nikova E. I., Basova S. A., Molokeev M. S., Krylov A. S., Aleksandrovsky A. S., Oreshonkov A. S., Atuchin V. V., Volkova S. S., Khritokhin N. A., Andreev O. V.
Заглавие : Synthesis of samarium oxysulfate Sm2O2SO4 in the high-temperature oxidation reaction and its structural, thermal and luminescent properties
Коллективы : Russian Foundation for Basic ResearchRussian Foundation for Basic Research (RFBR) [18-02-00754, 18-32-20011]; Russian Science FoundationRussian Science Foundation (RSF) [19-42-02003]
Место публикации : Molecules. - 2020. - Vol. 25, Is. 6. - Ст.1330. - ISSN 1420-3049(eISSN), DOI 10.3390/molecules25061330
Примечания : Cited References: 56. - This research was funded by the Russian Foundation for Basic Research (Grants 18-02-00754, 18-32-20011) and Russian Science Foundation (project 19-42-02003).
Предметные рубрики: RARE-EARTH SULFATES
SPECTROSCOPIC PROPERTIES
OXYGEN-STORAGE
LN
LA
Аннотация: The oxidation process of samariumoxysulfide was studied in the temperature range of 500–1000 °C. Our DTA investigation allowed for establishing the main thermodynamic (∆Hºexp = −654.6 kJ/mol) and kinetic characteristics of the process (Ea = 244 kJ/mol, A = 2 × 1010). The enthalpy value of samarium oxysulfate (ΔHºf (Sm2O2SO4(monocl)) = −2294.0 kJ/mol) formation was calculated. The calculated process enthalpy value coincides with the value determined in the experiment. It was established that samarium oxysulfate crystallizes in the monoclinic symmetry class and its crystal structure belongs to space group C2/c with unit cell parameters a = 13.7442 (2), b = 4.20178 (4) and c = 8.16711 (8)Å, β = 107.224 (1)°, V = 450.498 (9)Å3, Z = 4. The main elements of the crystalline structure are obtained and the cation coordination environment is analyzed in detail. Vibrational spectroscopy methods confirmed the structural model adequacy. The Sm2O2SO4 luminescence spectra exhibit three main bands easily assignable to the transitions from 4G5/2 state to 6H5/2, 6H7/2, and 6H9/2 multiplets.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Orlov Yu. S., Vereshchagin S. N., Novikov, S., V, Burkov A. T., Borus A. A., Sitnikov, M., V, Solovyov L. A., Volochaev M. N., Dudnikov V. A.
Заглавие : Effect of mechanical activation on the thermoelectric properties of Sr1-xSmxTiO3 ceramics
Коллективы : Russian Science FoundationRussian Science Foundation (RSF) [19-72-00097]
Место публикации : Ceram. Int. - 2021. - Vol. 47, Is. 20. - P.28992-28999. - ISSN 0272-8842, DOI 10.1016/j.ceramint.2021.07.060. - ISSN 1873-3956(eISSN)
Примечания : Cited References: 31. - This study was supported by the Russian Science Foundation, project no. 19-72-00097
Предметные рубрики: SRTIO3
LA
MICROSTRUCTURE
CONDUCTIVITY
PERFORMANCE
FIGURE
MERIT
Аннотация: The Sr1-xSmxTiO3 (х = 0.025, 0.05, 0.075, 0.1, 0.2) strontium titanate solid solutions were prepared from oxides and carbonates using a conventional ceramic technology based on the mechanochemical activation. The electrical conductivity and Seebeck coefficient of the synthesized compounds were measured in the temperature range from 300 to 800 K. We found that the properties of the samples significantly depend on the preliminary mechanochemical activation. The thermoelectric power factor attains maximum value in the hydrogen reduced samples with concentration of х = 0.05 and 0.075 obtained from nanoparticles: 5.5 μW/(cm · K2) for Sr0.95Sm0.05TiO3 (580 K) and 4.10 μW/(cm · K2) for Sr0.925Sm0.075TiO3 (650 K). An increase in the annealing temperature of mechanically activated samples leads to an even greater increase in electrical conductivity and power factor: 9.2 μW/(cm · K2) for Sr0.925Sm0.075TiO3 (650 K).
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Kazak N. V., Ovchinnikov S. G., Balaev A. D., Ivanova N.B., Pashkevich, Yu. G., Michel C.R., Bondarenko G. V.
Заглавие : Magnetic and transport properties of Gd(0.9)A(0.1)CoO(3-delta) (A = Ba, Sr)
Место публикации : J. Magn. Magn. Mater. - 2009. - Vol. 321, Is. 9. - P.1266-1271. - ISSN 0304-8853, DOI 10.1016/j.jmmm.2008.11.087
Примечания : Cited Reference Count: 31. - Гранты: This study was supported by the Rosnauka (Project no. MK-4278.2008.2), Russian Foundation for Basic Research (Project no. 08-02-90708 mob_st) and "Strongly correlated electrons'' program of the Department of Physical Sciences of RAS.Финансирующая организация: Rosnauka [MK-4278.2008.2]; Russian Foundation for Basic Research [08-02-90708 mob_st]; "Strongly correlated electrons'' program of the Department of Physical Sciences of RAS
Предметные рубрики: PEROVSKITE
PR
LA
EU
ND
LN
TRANSITION
SPIN
GD
SM
Ключевые слова (''Своб.индексиров.''): perovskite structure--doped cobaltite--magnetic susceptibility--metal-insulator transition--doped cobaltite--magnetic susceptibility--metal-insulator transition--perovskite structure--antiferromagnetism--barium--cobalt compounds--electric conductivity--ferromagnetic materials--ferromagnetism--gadolinium--magnetic susceptibility--metal insulator boundaries--oxide minerals--paramagnetic materials--perovskite--phase separation--semiconductor insulator boundaries--transport properties--antiferromagnetic--doped cobaltite--doped samples--electrical conductivity measurements--ferromagnetic transitions--insulator-metal transitions--magnetic and transport properties--magnetic behaviors--perovskite structure--temperature ranges--transport datum--x- ray diffractions--metal insulator transition
Аннотация: The X-ray diffraction, magnetization and electrical conductivity measurements for Gd(0.9)A(0.1)CoO(3-delta) (A = Ba, Sr) have been made. The complicated magnetic behavior, including the paramagnetic-ferromagnetic-antiferromagnetic and paramagnetic-ferromagnetic transitions, was found for Ba- and Sr-doped samples. The gradual insulator-metal transitions were observed in a wide temperature range T = 600-800 K. The complex magnetic and transport data could be explained on the basis of the structural phase separation. (C) 2009 Elsevier B.V. All rights reserved.
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