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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Denisova L. T., Molokeev M. S., Galiakhmetova N. A., Denisov V. M., Vasil'ev G. V.
Заглавие : Synthesis, crystal structure, and thermal properties of substituted titanates Bi2Pr2Ti3O12 and Bi2Nd2Ti3O12
Коллективы : [FSRZ-2020-0013]
Место публикации : Phys. Solid State. - 2021. - Vol. 63. Is. 8. - P.1159-1164. - ISSN 1063-7834, DOI 10.1134/S1063783421080084. - ISSN 1090-6460(eISSN)
Примечания : Cited References: 39. - This study was carried out in part within the state assignment for the Siberian Federal University, project no. FSRZ-2020-0013
Предметные рубрики: BI4-XRXTI3O12 R-X
PHASE-EQUILIBRIA
HEAT-CAPACITY
ND
BI4TI3O12
PR
Аннотация: Titanates Bi2Pr2Ti3O12 and Bi2Nd2Ti3O12 have been obtained by the solid-phase synthesis using sequential annealing of the Bi2O3, Nd2O3, Pr6O11, and TiO2 stoichiometric mixtures in air at temperatures of 1003–1323 K. Their crystal structure has been established by X-ray diffractometry and the high-temperature heat capacity has been determined by differential scanning calorimetry. Based on the experimental Cp = f(T) data, the main thermodynamic functions have been calculated.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Denisova L. T., Molokeev M. S., Kargin, Yu F., Gerasimov V. P., Krylov A. S., Aleksandrovskii A. S., Chumilina L. G., Denisov V. M., Vasil'ev G. V.
Заглавие : Synthesis, crystal structure, and physicochemical properties of Bi4-xPrxTi3O12 (x=0.4, 0.8, 1.2, 1.6) solid solutions
Место публикации : Inorg. Mater. - 2021. - Vol. 57, Is. 9. - P.919-928. - ISSN 0020-1685, DOI 10.1134/S002016852109003X. - ISSN 1608-3172(eISSN)
Примечания : Cited References: 40
Предметные рубрики: BI4-XRXTI3O12 R-X
HEAT-CAPACITY
AURIVILLIUS PHASES
PR
ND
BI4TI3O12
Аннотация: Bi4–xPrxTi3O12 (x = 0.4, 0.8, 1.2, 1.6) solid solutions have been prepared by solid-state reactions, via multistep firing of stoichiometric mixtures of their constituent oxides in air at temperatures from 1003 to 1323 K. Their crystal structure has been determined using X-ray diffraction, and their luminescence spectra have been measured at room temperature. High-temperature heat capacity of polycrystalline substituted bismuth titanate samples has been determined by differential scanning calorimetry. The Cp(T) curves of the solid solutions with x = 0.4 and 0.8 have extrema related to phase transitions. Experimental data have been used to calculate the main thermodynamic functions of the solid solutions.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Fausti D., Nugroho A. A., van Loosdrecht PHM, Klimin S. A., Popova M. N., Bezmaternykh L. N.
Заглавие : Raman scattering from phonons and magnons in RFe3(BO3)(4)
Разночтения заглавия :авие SCOPUS: Raman scattering from phonons and magnons in RFe3 (BO3) 4
Место публикации : Phys. Rev. B: AMER PHYSICAL SOC, 2006. - Vol. 74, Is. 2. - Ст.24403. - ISSN 1098-0121, DOI 10.1103/PhysRevB.74.024403
Примечания : Cited References: 26
Предметные рубрики: IRON BORATE GDFE3(BO3)(4)
LIGHT-SCATTERING
CRYSTALS
ND
CRYSTALLIZATION
TRANSITIONS
GENERATION
LASER
Аннотация: Inelastic light scattering spectra of several members of the RFe3(BO3)(4) family reveal a cascade of phase transitions as a function of temperature, starting with a structural, weakly first-order, phase transition followed by two magnetic phase transitions. Those consist of the ordering of the Fe-spin sublattice, revealed by all the compounds, and a subsequent spin-reorientational transition for GdFe3(BO3)(4). The Raman data evidence a strong coupling between the lattice and magnetic degrees of freedom in these borates. The Fe-sublattice ordering leads to a strong suppression of the low-energy magnetic scattering, and a multiple peaked two-magnon scattering continuum is observed. Evidence for short-range correlations is found in the "paramagnetic" phase by the observation of a broad magnetic continuum in the Raman data, which persists up to surprisingly high temperatures.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Peschanskii A. V., Glamazda, A. Yu., Gudim I. A.
Заглавие : Spectroscopic study of the TbAl3(BO3)4 single crystal: Raman and luminescence spectroscopy
Место публикации : Физ. низких температур. - 2020. - Т. 46, Вып. 12. - С.1437-1445. - ISSN 0132-6414. - ISSN 1816-0328(eISSN)
Примечания : Cited References: 20
Предметные рубрики: SCATTERING
GENERATION
ND
Аннотация: The vibrational and luminescence properties of the TbAl3(BO3)4 single crystal were studied in the temperature range of 5–300 K. Raman spectra of the single crystal revealed 5 of 7 A1 and all E phonon modes predicted by the group-theory analysis. The splitting energy between the LO and TO components of polar E phonons is determined. A group of intense bands associated with the 5D4 → 7F0 electronic transition was observed in the energy range of 14520–14680 cm−1 of the luminescence spectra. The intensity of these bands decreases upon heating. At the same time, the bands which can be assigned with 5D4 → 7F6, 5D4 → 7F5, and 5D4 → 7F4 transitions were revealed in luminescence spectra at room temperature. The intensity of these bands is comparable to the intensity of the Raman spectrum of TbAl3(BO3)4. The observation of luminescence from the 5D4 multiplet (20600–20750 cm−1) upon excitation at λexc = 632.8 nm (15803 cm−1) and λexc = 532 nm (18797 cm−1) indicates strong nonlinear properties of the studied crystal. The structure of the main 7F6 multiplet of Tb+3 in the TbAl3(BO3)4 single crystal has been studied at 5 K by Raman spectroscopy. The energies of the electronic levels of 7F6 and 5D4 multiplets were determined from the luminescence spectra measured at 300 K.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Peschanskii A. V., Glamazda, A. Yu., Gudim I. A.
Заглавие : Spectroscopic study of the TbAl3(BO3)4 single crystal: Raman and luminescence spectroscopy
Место публикации : Low Temp. Phys. - 2020. - Vol. 46, Is. 12. - P.1223-1230. - ISSN 1063-777X, DOI 10.1063/10.0002478. - ISSN 1090-6517(eISSN)
Примечания : Cited References: 20
Предметные рубрики: SCATTERING
GENERATION
ND
Аннотация: The vibrational and luminescence properties of the TbAl3(BO3)4 single crystal were studied in the temperature range of 5–300 K. Raman spectra of the single crystal revealed 5 of 7 A1 and all E phonon modes predicted by the group-theory analysis. The splitting energy between the LO and TO components of polar E phonons is determined. A group of intense bands associated with the 5D4 → 7F0 electronic transition was observed in the energy range of 14520–14680 cm−1 of the luminescence spectra. The intensity of these bands decreases upon heating. At the same time, the bands which can be assigned with 5D4 → 7F6, 5D4 → 7F5, and 5D4 → 7F4 transitions were revealed in luminescence spectra at room temperature. The intensity of these bands is comparable to the intensity of the Raman spectrum of TbAl3(BO3)4. The observation of luminescence from the 5D4 multiplet (20600–20750 cm−1) upon excitation at λexc = 632.8 nm (15803 cm−1) and λexc = 532 nm (18797 cm−1) indicates strong nonlinear properties of the studied crystal. The structure of the main 7F6 multiplet of Tb+3 in the TbAl3(BO3)4 single crystal has been studied at 5 K by Raman spectroscopy. The energies of the electronic levels of 7F6 and 5D4 multiplets were determined from the luminescence spectra measured at 300 K.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Popova M. N., Stanislavchuk T. N., Malkin B. Z., Bezmaternykh L. N.
Заглавие : Optical spectroscopy of PrFe3(BO3)(4): Crystal-field and anisotropic Pr-Fe exchange interactions
Коллективы : Russian Foundation for Basic Research [07-02-01185, 09-02-00930]; Russian Academy of Sciences under the Programs for Basic Research
Разночтения заглавия :авие SCOPUS: Optical spectroscopy of PrFe3 (BO3) 4: Crystal-field and anisotropic Pr-Fe exchange interactions
Место публикации : Phys. Rev. B. - 2009. - Vol. 80, Is. 19. - Ст.195101. - ISSN 1098-0121, DOI 10.1103/PhysRevB.80.195101
Примечания : Cited References: 36. - We thank S. Klimin for useful information concerning the structure of PrFeINF3/INF(BOINF3/INF)INF4/INF and E. Chukalina for participating in some measurements. This work was supported in part by the Russian Foundation for Basic Research (Grants No. 07-02-01185 and No. 09-02-00930) and by the Russian Academy of Sciences under the Programs for Basic Research.
Предметные рубрики: TRIGONAL GDFE3(BO3)(4)
NDFE3(BO3)(4)
DYFE3(BO3)(4)
TRANSITIONS
BORATE
ION
ND
Ключевые слова (''Своб.индексиров.''): antiferromagnetic materials--crystal field interactions--exchange interactions (electron)--infrared spectra--iron compounds--magnetic susceptibility--magneto-optical effects--paramagnetic materials--praseodymium compounds--spin hamiltonians--visible spectra
Аннотация: High-resolution polarized optical absorption spectra of PrFe3(BO3)(4) in the paramagnetic and antiferromagnetic phases are reported. The measured energies of the crystal-field (CF) levels within the 4f(2) configuration of Pr3+ in the paramagnetic PrFe3(BO3)(4) are described by the CF model that involves the 4f(2)/4f5d and 4f(2)/4f6p configuration interactions. Ordering of Fe spins along the crystalline c axis below T-N=32 K is confirmed by the analysis of the spectra of Er3+ introduced as a probe into PrFe3(BO3)(4). To account for the observed changes in the optical spectra of Pr3+ at temperatures below T-N, in particular, for the shift of the CF levels, splitting of the CF doublets, and the appearance of forbidden lines, the Pr-Fe exchange Hamiltonian defined by seven parameters is considered. The theoretical approach has been tested by calculating the temperature dependence of the magnetic susceptibility. A good agreement between theory and optical and magnetic experimental data is found demonstrating the validity of the model used. The obtained results confirm that the model of the iron dimers inside the spiral chains of Fe3+(O2-)(6) octahedrons introduced by us earlier for NdFe3(BO3)(4) and modified in the present work may serve as a basis for analyzing the low-temperature properties of other rare-earth iron borates.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Zvyagina G. A., Zhekov K. R., Bezmaternykh L. N., Gudim I. A., Bilych I. V., Zvyagin A. A.
Заглавие : Magnetoelastic effects in terbium ferroborate
Место публикации : Low Temp. Phys. - 2008. - Vol. 34, Is. 11. - P.901-908. - ISSN 1063-777X, DOI 10.1063/1.3009584; \b Физика низких температур
Примечания : Cited References: 17
Предметные рубрики: CRYSTAL-STRUCTURE
ND
Ключевые слова (''Своб.индексиров.''): acoustic wave velocity--antiferromagnetic materials--elastic moduli--exchange interactions (electron)--iron compounds--magnetoelastic effects--solid-state phase transformations--terbium compounds
Аннотация: The behavior of the elastic moduli and sound absorption in a terbium orthoborate single crystal at low temperatures is studied. The components of the tensor of the elastic moduli of this system are determined. A structural phase transition and a transition of the magnetic subsystem into an antiferromagnetically ordered state appear in the temperature dependences of the sound velocities and absorption. The magnetic field dependences of the velocities of transverse sound exhibit singularities in the form of jumps at a magnetic field equal to the field of the spin-flop transition of the antiferromagnetic subsystem. Theoretical analysis shows that the observed behavior of the acoustic characteristics are associated not with the rare-earth subsystem of ferroborate but rather with the renormalization of the exchange interaction between iron ions as a result of the magnetoelastic coupling.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Kazak N. V., Ovchinnikov S. G., Balaev A. D., Ivanova N.B., Pashkevich, Yu. G., Michel C.R., Bondarenko G. V.
Заглавие : Magnetic and transport properties of Gd(0.9)A(0.1)CoO(3-delta) (A = Ba, Sr)
Место публикации : J. Magn. Magn. Mater. - 2009. - Vol. 321, Is. 9. - P.1266-1271. - ISSN 0304-8853, DOI 10.1016/j.jmmm.2008.11.087
Примечания : Cited Reference Count: 31. - Гранты: This study was supported by the Rosnauka (Project no. MK-4278.2008.2), Russian Foundation for Basic Research (Project no. 08-02-90708 mob_st) and "Strongly correlated electrons'' program of the Department of Physical Sciences of RAS.Финансирующая организация: Rosnauka [MK-4278.2008.2]; Russian Foundation for Basic Research [08-02-90708 mob_st]; "Strongly correlated electrons'' program of the Department of Physical Sciences of RAS
Предметные рубрики: PEROVSKITE
PR
LA
EU
ND
LN
TRANSITION
SPIN
GD
SM
Ключевые слова (''Своб.индексиров.''): perovskite structure--doped cobaltite--magnetic susceptibility--metal-insulator transition--doped cobaltite--magnetic susceptibility--metal-insulator transition--perovskite structure--antiferromagnetism--barium--cobalt compounds--electric conductivity--ferromagnetic materials--ferromagnetism--gadolinium--magnetic susceptibility--metal insulator boundaries--oxide minerals--paramagnetic materials--perovskite--phase separation--semiconductor insulator boundaries--transport properties--antiferromagnetic--doped cobaltite--doped samples--electrical conductivity measurements--ferromagnetic transitions--insulator-metal transitions--magnetic and transport properties--magnetic behaviors--perovskite structure--temperature ranges--transport datum--x- ray diffractions--metal insulator transition
Аннотация: The X-ray diffraction, magnetization and electrical conductivity measurements for Gd(0.9)A(0.1)CoO(3-delta) (A = Ba, Sr) have been made. The complicated magnetic behavior, including the paramagnetic-ferromagnetic-antiferromagnetic and paramagnetic-ferromagnetic transitions, was found for Ba- and Sr-doped samples. The gradual insulator-metal transitions were observed in a wide temperature range T = 600-800 K. The complex magnetic and transport data could be explained on the basis of the structural phase separation. (C) 2009 Elsevier B.V. All rights reserved.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Ivanova N. B., Kazak N. V., Michel C. R., Balaev A. D., Ovchinnikov S. G.
Заглавие : Low-temperature magnetic behavior of the rare-earth cobaltites GdCoO3 and SmCoO3
Разночтения заглавия :авие SCOPUS: Low-temperature magnetic behavior of the rare-earth cobaltites GdCoO 3 and SmCoO3
Место публикации : Phys. Solid State: MAIK NAUKA/INTERPERIODICA/SPRINGER, 2007. - Vol. 49, Is. 11. - P2126-2131. - ISSN 1063-7834, DOI 10.1134/S1063783407110182
Примечания : Cited References: 32. - This study was supported by the Branch of General Physics and Astronomy of the Russian Academy of Sciences within the framework of the program “Strong Electron Correlations” and the Russian Science Support Foundation
Предметные рубрики: METAL-INSULATOR-TRANSITION
RCOO3 R
SPIN-STATE
OXIDE
SM
ND
PEROVSKITE
GLASSES
PR
EU
Аннотация: The temperature and magnetic field dependences of the static magnetization of the polycrystalline rare-earth cobaltites GdCoO3 and SmCoO3 have been measured. It is shown that, below room temperature, the magnetization of both compounds derives primarily from the rare-earth ion paramagnetism. The GdCoO3 and SmCoO3 compounds have been found to differ substantially in magnetic behavior, which can be traced to differences in their electronic shell structures. The magnetic behavior of GdCoO3 is close to that of an array of free Gd3+ ions, whereas in SmCoO3 the deviation from the free-ion properties is very large because of the Sm3+ ground state being crystal-field split. Van Vleck magnetic susceptibility measurements of SmCoO3 suggest that the splitting is similar to 10 K.
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Zvyagina G. A., Zhekov K. R., Bilych I. V., Zvyagin A. A., Bezmaternykh L. N., Gudim I. A.
Заглавие : Low-temperature behavior of the magnetoelastic characteristics of praseodymium ferroborate
Место публикации : Low Temp. Phys. - 2010. - Vol. 36, Is. 4. - P.296-302. - ISSN 1063-777X, DOI 10.1063/1.3420962; \b Физика низких температур
Примечания : Cited References: 16
Предметные рубрики: CRYSTAL
STATE
ND
Аннотация: The behavior of the elastic moduli and sound absorption in a PrFe(3)(BO(3))(4) single crystal at low temperatures is studied. A transition of the magnetic subsystem into an antiferromagnetically ordered state is manifested in the temperature behavior of the sound velocities and absorption. The characteristic behavior of the elastic properties of PrFe(3)(BO(3))(4) in an external magnetic field is observed. A phenomenological theory that gives a qualitative description of the observed features is constructed. It is proposed that a weak magnetic moment exists in the crystal. (C) 2010 American Institute of Physics. [doi: 10.1063/1.3420962]
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