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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Goryainov, Sergey, V, Krylova S. N., Borodina, Ulyana O., Krylov A. S.
Заглавие : Dynamical immiscibility of aqueous carbonate fluid in the shortite-water system at high-pressure-temperature conditions
Коллективы : RFBRRussian Foundation for Basic Research (RFBR); DFGGerman Research Foundation (DFG)European Commission [21-52-12018]; Ministry of Science and Higher EducationMinistry of Science and Higher Education, PolandEuropean Commission
Место публикации : J. Phys. Chem. C. - 2021. - Vol. 125, Is. 33. - P.18501-18509. - ISSN 1932-7447, DOI 10.1021/acs.jpcc.1c05077. - ISSN 1932-7455(eISSN)
Примечания : Cited References: 47. - The reported study was funded by the RFBR and DFG, project number 21-52-12018. Work is done on the state assignment of the Sobolev Institute of Geology and Mineralogy, Kirensky Institute of Physics SB RAS, Equipment of Federal Research Center of Krasnoyarsk Science Center SB RAS, and supported by the Ministry of Science and Higher Education. Authors thank A.N. Vtyurin, A.G. Sokol, A.Yu. Likhacheva, and A.F. Shatskiy for fruitful discussion
Предметные рубрики: SIMULTANEOUSLY HIGH-PRESSURE
SODIUM FORMATE
RAMAN-SPECTRA
Аннотация: Anhydrous carbonate shortite, Na2Ca2(CO3)3, compressed in water at high pressure–temperature (up to 5 GPa, 350 °C) was studied by Raman spectroscopy. At 3.2 GPa and 250 °C, shortite begins to dissolve, followed by crystallization of aragonite and aragonite’. The unusual behavior of aqueous carbonate fluid was observed at 4.8 GPa and 300–350 °C. This process is characterized by the active formation of microbubbles within 2–60 s that are inserted one into another. Microbubbles are considered to be a result of the two immiscible fluid stratification. This dynamical immiscibility of the fluid accompanies the appearance of several crystalline carbonates and organic molecular crystals. Na-formate and some polymorphs of Ca-formate were observed.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Krylov A. S., Pavlovskiy M. S., Kitaev Y., Gudim I. A., Andryshin N. D., Vtyurin A. N., Jiang, Qinghui, Krylova S. N.
Заглавие : Phase transitions and p–T phase diagram of the multiferroic TbFe3(BO3)4 crystal
Коллективы : Russian Foundation for Basic ResearchRussian Foundation for Basic Research (RFBR); RFBR, Krasnoyarsk Territory and Krasnoyarsk Regional Fund of Science [20-42-240009]; Russian Foundation for Basic Research and DFG (Deutsche Forschungsgemeinschaft)German Research Foundation (DFG) [448809307, 21-52-12018]
Место публикации : J. Raman Spectrosc. - 2022. - Vol. 53, Is. 6. - P.1179-1187. - ISSN 0377-0486, DOI 10.1002/jrs.6341. - ISSN 1097-4555(eISSN)
Примечания : Cited References: 48. - Russian Foundation for Basic Research; RFBR, Krasnoyarsk Territory and Krasnoyarsk Regional Fund of Science, Grant/Award Number: 20-42-240009; Russian Foundation for Basic Research and DFG (Deutsche Forschungsgemeinschaft), Grant/Award Numbers: 448809307, 21-52-12018
Предметные рубрики: BILBAO CRYSTALLOGRAPHIC SERVER
RAMAN-SPECTRA
HIGH-TEMPERATURE
Аннотация: The structural phase transitions in multiferroic TbFe3(BO3)4 with change hydrostatic pressures and temperatures have been studied by Raman spectroscopy and calculation within density functional theory. Lattice dynamics calculations in the TbFe3(BO3)4 crystal in the ��32 phase under various values of applied hydrostatic pressure (from 0 up to 5 GPa with 1 GPa step) were performed. The calculation performed in this work in a TbFe3(BO3)4 crystal showed that the applied pressure can increase the phase transition temperature. Raman spectra of the TbFe3(BO3)4 crystal have been investigated at simultaneously high temperature and high pressure (up to 5.14 GPa and 465 K). The appearance of a soft mode was observed with decreasing temperature at normal pressure. The manifestations of the interaction of the structural and magnetic order parameters in the range from 13 to 50 K were observed at normal pressure. With increasing pressure and a fixed temperature, recovery of the soft modes is also observed. The experimental p–T phase diagram of TbFe3(BO3)4 was established. An increase in pressure leads to an increase in the temperature of transition.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Mishra S., Yogi P., Chaudhary A., Pathak D. K., Saxena S. K., Krylov A. S., Sagdeo P. R., Kumar R.
Заглавие : Understanding perceived color through gradual spectroscopic variations in electrochromism
Коллективы : Department of Science and Technology (DST), Govt. of India; MHRD; CSIR (Govt. of India); DST under FIST scheme [SR/FST/PSI-225/2016]
Место публикации : Indian J. Phys. - 2019. - Vol. 93, Is. 7. - P.927-933. - ISSN 0973-1458, DOI 10.1007/s12648-018-1353-7. - ISSN 0974-9845(eISSN)
Примечания : Cited References: 34. - Authors acknowledge financial support from the Department of Science and Technology (DST), Govt. of India. Authors are thankful to Dr. K. V. Adarsh (IISER Bhopal) for Raman measurements. Authors thank Prof. V.D. Vankar (IIT Delhi) for useful discussions. Authors (AC and DKP) are thankful to MHRD and CSIR (Govt. of India), respectively, for providing fellowships. Support received from DST under FIST scheme (grant number: SR/FST/PSI-225/2016) is also acknowledged.
Предметные рубрики: 3 REDOX FORMS
TUNGSTEN-OXIDE
RAMAN-SPECTRA
VIOLOGEN
SALTS
Аннотация: A bias-dependent in situ Raman scattering and UV–Vis absorption spectroscopic change has been correlated with the corresponding color change of an electrochromic device in an attempt to explain how to understand the relationship between actual perceived color and its absorption/transmittance spectra. For this, the bias across an electrochromic device was increased gradually, rather than abruptly turning ON and OFF, to see subtle variations in Raman and absorption spectra due to bias. Raman scattering establishes that viologen changes its oxidation state reversibly between two redox species (EV2+ to EV+•) as a result of bias-induced dynamic redox process. A gradual variation in Raman and absorption spectra, which shows maximum absorption corresponding to the yellow light, accompanies similar variation in color change of the device as visible by naked eye. These spectroscopic results are correlated with the perceived blue color, in the reflected light, by the eye to understand the actual reason behind this. Maximum absorption of yellow light by the device resulting in blue appearance has been explained using the concept of additive and subtractive primary colors.
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