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Features of the Preparation and Study of Electrophysical Characteristics (BeO+TiO2)-Ceramics by Impedance Spectroscopy / A. A. Lepeshev [et al.] // Refract. Ind. Ceram. - 2019. - Vol. 60, Is. 3. - P. 309-317, DOI 10.1007/s11148-019-00359-1. - Cited References: 26 . - ISSN 1083-4877. - ISSN 1573-9139
Кл.слова (ненормированные):
(BeO + TiO2)-ceramic -- electrophysical properties -- impedance -- frequency dependence -- dielectric permittivity -- dielectric loss tangent
Аннотация: An electrically conducting two-component BeO-ceramic with the addition of micro- and nano-crystalline TiO2 powder is prepared that can be used as a material for scattered microwave radiation absorption in high-power electronic devices. The nature of the occurrence of electrical conductivity and absorption of the microwave field in (BeO + TiO2)-ceramics is not completely established. Impedance spectroscopy is used for the first time to investigate the electrical and dielectric characteristics of this ceramic in the frequency range from 100 Hz to 100 MHz in relation to presence of micro- and nano-sized TiO2 phase within the BeO ceramic composition. It is established that the static resistance of ceramics with addition of a TiO2 nanopowder is significantly reduced compared with the resistance of original ceramic with TiO2 micropowder. It is shown that real and imaginary components of the dielectric constant of the ceramic studied increase to abnormally large values with a reduction in frequency of the effective electric field, and in the high frequency range f ≥ 108 Hz the process of dielectric relaxation commences leading to an increase in dielectric loss angle. Dielectric properties of ceramic samples are determined under blocking conditions for through conduction. The effect of TiO2 micropowder additions on dielectric polarization processes with frequency increasing up to 12 × 109 Hz is considered.

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Публикация на русском языке Особенности получения и исследование электрофизических характеристик (ВеО + TiO2)-керамики методом импедансной спектроскопии [Текст] / А. А. Лепешев [и др.] // Новые огнеупоры. - 2019. - № 6. - С. 55-63

Держатели документа:
FGBOU VO Siberian Federal University, Krasnoyarsk, Russia
FGBUN Federal Research Center, Krasnoyarsk Scientific Center, Siberian Section of the Russian Academy of Sciences, Krasnoyarsk, Russia
FGBOU VO Academician M. F. Reshetnev Siberian Aerospace University, Krasnoyarsk, Russia
FGAOU VO Ural Federal University, Ekaterinburg, Russia

Доп.точки доступа:
Lepeshev, A. A.; Pavlov, A. V.; Drokin, N. A.; Дрокин, Николай Александрович; Malkin, A. I.; Kiiko, V. S.; Knyazev, N. S.
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BT-30 Ceramic Electrophysical Properties / N. A. Drokin, V. S. Kiiko, A. V. Pavlov, A. I. Malkin // Refract. Ind. Ceram. - 2020. - Vol. 61, Is. 3. - P. 341-348, DOI 10.1007/s11148-020-00484-2. - Cited References: 12 . - ISSN 1083-4877. - ISSN 1573-9139
Кл.слова (ненормированные):
(BeO + TiO2)-ceramic -- electrophysical properties -- electrical resistance activation energy
Аннотация: A total complex resistance (impedance) method is used to study the electrophysical characteristics of (BeO + TiO2)-ceramics modified with TiO2 micro- and nanoparticles in an amount of 30 wt.% (BT-30). Dispersion of the actual ε′ and imaginary ε′′ components of the dielectric permittivity component and specific conductivity in the frequency range from 100 Hz to 100 MHz from room temperature to the boiling point of liquid nitrogen are determined. High values of ε′ and ε′′ in the low-frequency range are typical for structurally inhomogeneous materials due to the accumulation of electric charges at the surface and within microcrystals. Two dielectric relaxation processes associated with electrical conductivity within the body and at the surface of ceramics are detected for the first time. An increase in conductivity with an increase in the microwave field frequency above 1 MHz is explained by the appearance of a current relaxation component. The activation energy of the static resistance of ceramic specimens is determined as a function of the reciprocal temperature that depends little on the weight content of TiO2 nanoparticles and varies in the range of 0.024 – 0.10 eV This also confirms the existence of two independent conduction processes, weakly dependent on the nanoparticle content in the ceramic composition. With placement of ceramic in a high-frequency electric field, spatial charges are formed, the field of which contributes to creation of additional polarization and dielectric losses.

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Держатели документа:
FGBOU VO Academician M. F. Reshetnev Siberian Aerospace University, Krasnoyarsk, Russia.
FGBUN Federal Research Center, Krasnoyarsk Scientific Center of the Siberian Section, Russian Academy of Sciences, Krasnoyarsk, Russia.
FGAOU VO Ural Federal University, Ekaterinburg, Russia.
FGAOU VO Siberian Federal University, Krasnoyarsk, Russia.

Доп.точки доступа:
Drokin, N. A.; Дрокин, Николай Александрович; Kiiko, V. S.; Pavlov, A. V.; Malkin, A. I.
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