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    Oxidation of Ag nanoparticles in aqueous media: Effect of particle size and capping / Y. L. Mikhlin [et al.] // Appl. Surf. Sci. - 2014. - Vol. 297. - P. 75-83, DOI 10.1016/j.apsusc.2014.01.081. - Cited References: 58. - This work was partially financially supported by the Ministry of Education and Science of RF (Grant 8580) and RFBR (12-03-31178). . - ISSN 0169-4332. - ISSN 1873-5584
   Перевод заглавия: Окисление наночастиц Ag в водной среде: Влияние размера частиц и оболочки.

РУБ Chemistry, Physical + Materials Science, Coatings & Films + Physics, Applied + Physics, Condensed Matter
Рубрики:
EX-SITU XPS
   POLYCRYSTALLINE SILVER ELECTRODES
   RAY PHOTOELECTRON-SPECTROSCOPY
   METAL NANOPARTICLES
   ELECTROCHEMICAL OXIDATION
   ABSORPTION SPECTROSCOPY
   PYROLYTIC-GRAPHITE
   OXYGEN-ADSORPTION
   TRANSFORMATIONS
   DISSOLUTION
Кл.слова (ненормированные):
Silver nanoparticles -- Oxidation -- Resistive switching effect -- X-ray photoelectron spectroscopy
Аннотация: Many applications and environmental impact of silver-bearing nanomaterials critically depend upon their specific reactivity, which is still poorly understood. Here, silver nanoparticles (Ag NPs) of about 3-5 nm and 10-12 nm in diameter, uncapped and capped with l-glucose or citrate, were prepared, characterized using UV-vis absorption spectroscopy, SAXS, TEM, and their (electro) chemical oxidation was examined in comparison with each other and bulk metal applying scanning tunneling microscopy and spectroscopy, cyclic voltammetry, and XPS. A resistive switching effect was found in the tunneling spectra measured in air at the smaller uncapped Ag NPs deposited on HOPG and was interpreted in terms of Ag transfer between the particle and the probe. The anodic oxidation of these Ag NPs in 1 M NaOH yielded 3D Ag2O, while only a layer of "primary"Ag(I) oxide emerged on larger uncapped nanoparticles during the potential sweep. The formation of AgO at higher potentials proceeded readily at the "primary"oxide but was retarded at the smaller NPs. The citrate- and glucose-capping substantially impeded the formation both of Ag2O and AgO. The findings highlighted, particularly, a non-trivial effect of particle size and transient mobilization of Ag species on the reactions of silver nanoparticles. (c) 2014 Elsevier B.V. All rights reserved.

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Держатели документа:
Russian Acad Sci, Siberian Branch, Inst Chem & Chem Technol, Krasnoyarsk 660036, Russia
Siberian Fed Univ, Krasnoyarsk 660041, Russia
Russian Acad Sci, Siberian Branch, Boreskov Inst Catalysis, Novosibirsk 630090, Russia
Russian Acad Sci, Siberian Branch, Kirensky Inst Phys, Krasnoyarsk 660036, Russia

Доп.точки доступа:
Mikhlin, Y. L.; Vishnyakova, E. A.; Romanchenko, A. S.; Saikova, S. V.; Сайкова, С. В.; Likhatski, M. N.; Larichev, Y. V.; Tuzikov, F. V.; Zaikovskii, V. I.; Zharkov, S. M.; Жарков, Сергей Михайлович
}
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High performance hybrid rGO/ Ag quasi-periodic mesh transparent electrodes for flexible electrochromic devices / A. S. Voronin [et al.] // Appl. Surf. Sci. - 2016. - Vol. 364. - P. 931–937, DOI 10.1016/j.apsusc.2015.12.182. - Cited References: 31 . - ISSN 0169-4332. - ISSN 1873-5584

РУБ Chemistry, Physical + Materials Science, Coatings & Films + Physics, Applied + Physics, Condensed Matter
Рубрики:
NANOWIRE NETWORKS
   GRAPHENE FILMS
   OXIDE
   OXIDATION
   HEATERS
Кл.слова (ненормированные):
Quasi-periodic mesh transparent electrode self-organized template -- Reduced graphene oxide (rGO) -- Flexible electrochromic device
Аннотация: A possibility of creating a stable hybrid coating based on the hybrid of a reduced graphene oxide (rGO)/ Ag quasi-periodic mesh (q-mesh) coating has been demonstrated. The main advantages of the suggested method are the low cost of the processes and the technology scalability. The Ag q-mesh coating is formed by means of the magnetron sputtering of silver on the original template obtained as a result of quasi-periodic cracking of a silica film. The protective rGO film is formed by low temperature reduction of a graphene oxide (GO) film, applied by the spray-deposition in the solution of NaBH4. The coatings have low sheet resistance (12.3 Ω/sq) and high optical transparency (82.2%). The hybrid coating are characterized by high chemical stability, as well as they show high stability to deformation impacts. High performance of the hybrid coatings as electrodes in the sandwich-system «electrode – electrochromic composition – electrode» has been demonstrated. The hybrid electrodes allow the electrochromic sandwich to function without any visible degradation for a long time, while an unprotected mesh electrode does not allow performing even a single switching cycle.

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Доп.точки доступа:
Voronin, A. S.; Ivanchenko, F. S.; Simunin, M. M.; Shiverskiy, A. V.; Aleksandrovsky, A. S.; Александровский, Александр Сергеевич; Nemtsev, I. V.; Fadeev, Y. V.; Karpova, D. V.; Khartov, S. V.
}
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Vasil'ev, E. N.
Numerical simulation of the spatial structure of a moving arc discharge / E. N. Vasil'ev, D. A. Nesterov // High Temp. - 2008. - Vol. 46, Is. 6. - P. 746-751, DOI 10.1134/S0018151X08060023. - Cited References: 9 . - ISSN 0018-151X

РУБ Physics, Applied

Кл.слова (ненормированные):
52 -- 80 -- Mg -- Cavity resonators -- Computer simulation -- Discharge (fluid mechanics) -- Magnetic fields -- Three dimensional -- Arc discharges -- Current strengths -- Experimental datums -- Gas flows -- Magnetogasdynamics -- Numerical simulations -- Parallel electrodes -- Physical parameters -- Spatial shapes -- Spatial structures -- State processes -- Transverse magnetic fields -- Electric discharges
Аннотация: Results are given of the calculation of the structure of an arc discharge moving on parallel electrodes in air under the effect of a transverse magnetic field (0.086 T) at a current strength of 320 A. The numerical simulation is performed within an unsteady-state three-dimensional mathematical model of radiation magnetogasdynamics. The calculations reveal that fluctuations of values of physical parameters and of spatial shape of arc arise in the arc, which are caused by the gas flow past the discharge column and by unsteady-state processes in the electrode regions. Comparison is made with the available experimental data.

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Держатели документа:
[Vasil'ev, E. N.
Nesterov, D. A.] Russian Acad Sci, Inst Computat Modeling, Siberian Div, Krasnoyarsk 660036, Russia
ИВМ СО РАН
Institute of Computational Modeling, Siberian Division, Russian Academy of Sciences, Krasnoyarsk 60036, Russian Federation

Доп.точки доступа:
Nesterov, D. A.; Васильев, Евгений Николаевич
}
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Preparation and investigation of composite transparent electrodes of poly(3, 4-ethylenedioxythiophene) polystyrene sulfonate/single-wall carbon nanotubes / A. S. Voronin [et al.] // Tech. Phys. Lett. - 2017. - Vol. 43, Is. 9. - P. 783-786, DOI 10.1134/S1063785017090127. - Cited References:7. - This study was supported by the Russian Foundation for Basic Research (RFBR project no. 16-32-00302 mol_a) and jointly by the RFBR, Government of Krasnoyarsk Krai, and the Krasnoyarsk Krai Foundation for the Support of Scientific and Technological Work within scientific projects nos. 16-42-243059 r_mol_a, 16-42-243006 r_mol_a, and 16-48-242092 r_ofi_m. . - ISSN 1063-7850. - ISSN 1090-6533

РУБ Physics, Applied
Рубрики:
SOLAR-CELLS
Аннотация: The preparation of composite transparent electrodes of poly(3, 4-ethylenedioxythiophene) polystyrene sulfonate/single-wall carbon nanotubes by the spray method is described. The influence of the successive treatment of each functional layer in acid media with different activities on the optical and electric film characteristics is considered. The composite with the surface resistance of 89 Ω/sq at the transparency of 85.3% (550 nm) on a polymer substrate is obtained.

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Публикация на русском языке Формирование и исследование композитных прозрачных электродов поли(3, 4-этилендиокситиофен) полистиролсульфонат/одностенные углеродные нанотрубки [Текст] / А. С. Воронин [и др.] // Журн. техн. физ. : Наука, 2017. - Т. 43 Вып. 17. - С. 12-19

Держатели документа:
Russian Acad Sci, Siberian Branch, Fed Res Ctr, Krasnoyarsk Sci Ctr, Krasnoyarsk 660036, Russia.
Natl Res Univ Elect Technol MIET, Moscow 124498, Russia.
Siberian Fed Univ, Krasnoyarsk 660041, Russia.
Russian Acad Sci, Kirensky Inst Phys, Siberian Branch, Krasnoyarsk 660036, Russia.

Доп.точки доступа:
Voronin, A. S.; Simunin, M. M.; Ivanchenko, F. S.; Shiverskii, A. V.; Fadeev, Yu. V.; Tambasov, I. A.; Тамбасов, Игорь Анатольевич; Nemtsev, I. V.; Matsynin, A. A.; Мацынин, Алексей Александрович; Khartov, S. V.; Russian Foundation for Basic Research [16-32-00302 mol_a]; RFBR; Government of Krasnoyarsk Krai; Krasnoyarsk Krai Foundation [16-42-243059 r_mol_a, 16-42-243006 r_mol_a, 16-48-242092 r_ofi_m]
}
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    The influence of magnetic field on the rate of cathode erosion at vacuum arc spraying / I. V. Karpov [et al.] // IOP Conf. Ser.: Mater. Sci. Eng. - 2017. - Vol. 255, Is. 1. - Ст. 012007, DOI 10.1088/1757-899X/255/1/012007. - Cited References: 27
   Перевод заглавия: Влияние магнитного поля на скорость эрозии катода при дуговом распылении в вакууме
Кл.слова (ненормированные):
Cathodes -- Copper compounds -- Electrodes -- Magnetic fields -- Magnetism -- Metals -- Vacuum applications -- Vacuum technology -- Cathode erosion -- Influence of magnetic field -- Metal oxides -- Nano powders -- Particular condition -- Vacuum arcs -- Magnetoplasma
Аннотация: The influence of the magnetic field in the cathode space on the synthesis of metal oxide nanopowders by vacuum-arc spraying was studied. It was found that, depending on the geometry of the magnetic field and the pressure of gaseous medium in plasma-chemical reactor, particular conditions which enhance the efficiency of CuO synthesis, appear.

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Доп.точки доступа:
Karpov, I. V.; Ushakov, A. V.; Lepeshev, A. A.; Лепешев, Анатолий Александрович; Fedorov, L. Y.; Dorozhkina, E. A.; Karpova, O. N.; Shaikhadinov, A. A.; Demin, V. G.; Bachurina, E. P.; Lichargin, D. V.; Abkaryan, A. K.; Zeer, G. M.; Зеер Г.М.; Zharkov, S. M.; Жарков, Сергей Михайлович; International Scientific Conference Reshetnev Readings(20 ; 2016 ; Nov. 9-12 ; Krasnoyarsk)
}
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    The investigation of the influence of oxygen concentration in the gas mixture on nanodispersed oxides synthesis / I. V. Karpov [et al.] // IOP Conf. Ser.: Mater. Sci. Eng. - 2017. - Vol. 255, Is. 1. - Ст. 012008, DOI 10.1088/1757-899X/255/1/012008. - Cited References: 25
   Перевод заглавия: Исследование влияния концентрации кислорода в газовой смеси на синтез нанодисперсных оксидов
Кл.слова (ненормированные):
Cathodes -- Electrodes -- Particle size -- Vacuum applications -- Average particle size -- Cathode process -- Discharge gaps -- Energy of ions -- Influence of oxygen -- Low pressure arc -- Oxides synthesis -- Superheated gas -- Gases
Аннотация: Thermal effects in cathode space of low-pressure arc discharge, which contribute to the synthesis of nanopowders with an average particle size of less than 10 nm, are considered. One of the most important parameters, characterizing the cathode processes of vacuum arc, is a voltage drop across the discharge gap. All the gases demonstrate a decrease of a voltage drop across the discharge gap under the condition ofincreasing the gas pressure in the range of p = 10-3 - 1 Pa. Dissipation of energy of ions and electrons on gas molecules causes abrupt heating of the gas. Heat, coming from gas plasma, has a significant impact on evaporating material of a cathode. It can be assumed that a microdrop fraction, formed as a result of a cathode spraying in a liquid phase, will further evaporate in a superheated gas.

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Доп.точки доступа:
Karpov, I. V.; Ushakov, A. V.; Lepeshev, A. A.; Лепешев, Анатолий Александрович; Fedorov, L. Y.; Dorozhkina, E. A.; Karpova, O. N.; Shaikhadinov, A. A.; Demin, V. G.; Bachurina, E. P.; Lichargin, D. V.; Abkaryan, A. K.; Zeer, G. M.; Зеер Г.М.; Zharkov, S. M.; Жарков, Сергей Михайлович; International Scientific Conference Reshetnev Readings(20 ; 2016 ; Nov. 9-12 ; Krasnoyarsk)
}
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Localization and transfer of charge carriers in CuO nanopowder by impedance spectroscopy / A. A. Lepeshev [et al.] // J. Mater. Sci.: Mater. Electron. - 2018. - Vol. 29, Is. 14. - P. 12118–12125, DOI 10.1007/s10854-018-9319-2. - Cited References: 26. - The work was performed with a support of the Grant of the Russian Science Foundation (Project No. 16-19-10054). . - ISSN 0957-4522
Кл.слова (ненормированные):
Copper oxides -- Electric charge -- Electric fields -- Electrodes -- Metal nanoparticles -- Permittivity -- Spectroscopy
Аннотация: Particular electro-physical characteristics of CuO nanopowder were investigated by impedance spectroscopy using a sensor based on interdigitated structure in the frequency range from 1 Hz to 100 MHz. The results of investigation were considered. Simulation of impedance spectra by equivalent electric circuits was carried out for numerical approximations of the frequency dependences of the dielectrical permittivity and conductivity. Electric charge accumulation of on the boundaries of nanoparticles and near the metal electrodes of the sensor was revealed. It was shown that a double electric layer is formed near the electrodes, which leads to the appearance of anomalously large values of dielectrical permittivity and an increase in the conductivity in the low-frequency region. The obtained results can be explained by proton conductivity in the nanopowder caused by moisture which is adsorbed on the surface of the nanoparticles. It was shown that after high-temperature annealing of CuO nanopowders, accumulation of electric charges was not observed. It was established that hopping or polaron conductivity occurs in the annealed CuO samples, which increases with increasing electric field frequency according to the power law with a fractional exponent.

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Держатели документа:
Krasnoyarsk Scientific Center of the Siberian Branch of the Russian Academy of Science, Krasnoyarsk, Russian Federation
Siberian Federal University, Krasnoyarsk, Russian Federation
Siberian Branch, Kirensky Institute of Physics, Russian Academy of Sciences, Krasnoyarsk, Russian Federation

Доп.точки доступа:
Lepeshev, A. A.; Drokin, N. A.; Дрокин, Николай Александрович; Ushakov, A. V.; Karpov, I. V.; Fedorov, L. Y.; Bachurina, E. P.
}
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Technological Basis of the Formation of Micromesh Transparent Electrodes by Means of a Self-Organized Template and the Study of Their Properties / A. S. Voronin [et al.] // Tech. Phys. Lett. - 2019. - Vol. 45, Is. 4. - P. 366-369, DOI 10.1134/S1063785019040187. - Cited References: 15. - This work was supported by the Russian Foundation for Basic Research, project no. 18-38-00852_mol-a. . - ISSN 1063-7850. - ISSN 1090-6533

РУБ Physics, Applied
Рубрики:
UNIFORM
Аннотация: This Letter presents the results of a study of the physical properties of micromesh transparent electrodes on a flexible substrate, obtained using a template in the form of silica layers subjected to controlled cracking. For the first time, a combined approach to the control of parameters of a micromesh structure (crack width and cell size) by varying the pH and the thickness of the sol layer is proposed. Using this approach, transparent electrodes with a surface resistance of 4.1 Ω/sq with a transparency of 85.7% were obtained. Micromesh electrodes are characterized by linear optical transmission in the visible and IR ranges, which opens up prospects for their use in optoelectronics.

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Публикация на русском языке Технологические основы формирования микросетчатых прозрачных электродов при помощи самоорганизованного шаблона и исследование их свойств [Текст] / А. С. Воронин [и др.] // Письма в ЖТФ. - 2019. - Т. 45 Вып. 7. - С. 59-62

Держатели документа:
Russian Acad Sci, Siberian Branch, Krasnoyarsk Sci Ctr, Krasnoyarsk 660036, Russia.
Siberian Fed Univ, Krasnoyarsk 660041, Russia.
Russian Acad Sci, Kirensky Inst Phys, Siberian Branch, Krasnoyarsk 660036, Russia.

Доп.точки доступа:
Voronin, A. S.; Simunin, M. M.; Fadeev, Yu. V.; Ivanchenko, F. S.; Karpova, D. V.; Tambasov, I. A.; Тамбасов, Игорь Анатольевич; Khartov, S. V.; Russian Foundation for Basic Research [18-38-00852_mol-a]
}
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Cu-Ag and Ni-Ag meshes based on cracked template as efficient transparent electromagnetic shielding coating with excellent mechanical performance / A. S. Voronin, Y. V. Fadeev, I. V. Govorun [et al.] // J. Mater. Sci. - 2021. - Vol. 56. Is. 26. - P. 14741-14762, DOI 10.1007/s10853-021-06206-4. - Cited References: 79. - This work was supported by Russian Foundation for Basic Research project «mol_a» № 18-38-00852 and a scholarship from the President of the Russian Federation SP-2235.2019.1. The sputtering Ag seed mesh and physicochemical analysis of materials was carried out on the equipment of Krasnoyarsk Regional Center of Research Equipment of Federal Research Center «Krasnoyarsk Science Center SB RAS» . - ISSN 0022-2461. - ISSN 1573-4803

РУБ Materials Science, Multidisciplinary
Рубрики:
COPPER NANOWIRES
   METALLIC MESH
   PLASTIC SUBSTRATE
   ELECTRODES
   FILMS
Аннотация: Nowadays, the technical advances call for efficient electromagnetic interference (EMI) shielding of transparent devices which may be subject to data theft. We developed Cu–Ag and Ni–Ag meshes on flexible PET substrate for highly efficiency transparent EMI shielding coating. Cu–Ag and Ni–Ag meshes obtained with galvanic deposition of copper and nickel on thin Ag seed mesh which was made by cracked template method. Coefficients S11, S21 and shielding efficiency (SE) were measured for Cu–Ag and Ni–Ag meshes in X-band (8–12 GHz) and K-band (18–26.5 GHz). 90 s copper deposition increase SE from 23.2 to 43.7 dB at 8 GHz with a transparency of 82.2% and a sheet resistance of 0.25 Ω/sq. The achieved maximum SE was 47.6 dB for Cu–Ag mesh with 67.8% transparency and 41.1 dB for Ni–Ag mesh with 77.8% transparency. Cu–Ag and Ni–Ag meshes have high bending and long-term stability. Minimum bend radius is lower than 100 µm. This effect allows to produce different forms of transparent shielding objects, for example, origami method. Our coatings are the leading among all literary solutions in three-dimensional coordinates: of sheet resistance–optical transmittance–cost of produced.

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Держатели документа:
Russian Acad Sci, Siberian Branch, Krasnoyarsk Sci Ctr, Fed Res Ctr,FRC KSC SB RAS, Krasnoyarsk 660036, Russia.
Siberian Fed Univ, Krasnoyarsk 660041, Russia.
Russian Acad Sci, Siberian Branch, Kirensky Inst Phys, Krasnoyarsk 660036, Russia.
Reshetnev Univ, Reshetnev Siberian State Univ Sci & Technol, Krasnoyarsk 660037, Russia.
Russian Acad Sci, Siberian Branch, Inst Chem & Chem Technol, Krasnoyarsk 660036, Russia.

Доп.точки доступа:
Voronin, A. S.; Fadeev, Y. V.; Govorun, I. V.; Говорун, Илья Валерьевич; Podshivalov, I. V.; Подшивалов, Иван Валерьевич; Simunin, M. M.; Tambasov, I. A.; Тамбасов, Игорь Анатольевич; Karpova, D. V.; Smolyarova, T. E.; Смолярова, Татьяна Евгеньевна; Lukyanenko, A. V.; Лукьяненко, Анна Витальевна; Karacharov, A. A.; Nemtsev, I. V.; Немцев, Иван Васильевич; Khartov, S. V.; Russian Foundation for Basic Research projectRussian Foundation for Basic Research (RFBR) [18-38-00852]; Russian FederationRussian Federation [SP-2235.2019.1]
}
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10.

Synthesizing zinc sulfide films on the gold surface as the sensor for electrochemical quartz crystal microbalance / D. O. Krinitsyn, A. S. Romanchenko, S. A. Vorob'ev [et al.] // Russ. J. Electrochem. - 2021. - Vol. 57, Is. 12. - P. 1157-1163, DOI 10.1134/S1023193521120041. - Cited References: 23. - The study was supported by the Russian Scientific Foundation (grant no. 18-17-00135) . - ISSN 1023-1935. - ISSN 1608-3342

РУБ Electrochemistry
Рубрики:
CHEMICAL BATH DEPOSITION
   ZNS
   SPHALERITE
   ELECTRODES
   ACTIVATION
Кл.слова (ненормированные):
sphalerite -- thin films -- hydrochemical deposition -- electrochemistry -- quartz crystal microbalance -- dynamic light scattering -- gold -- spectroscopy
Аннотация: A zinc sulfate film is deposited from aqueous solutions of zinc sulfate onto the gold surface with the aim of preparation of a sensor for electrochemical quartz crystal microbalance (EQCM). The kinetics of this process, the particles formed in solution, and the film itself are studied by the methods of electrochemical quartz crystal microbalance, X-ray photoelectron spectroscopy, transmission electron microscopy, atomic force microscopy, optical and Raman spectroscopies, and dynamic light scattering. The effect of the procedure of gold surface preparation, the reagent concentration, and the temperature on the film adhesion, the length of induction period, the kinetics of film growth, and its structure and thickness are studied. It is shown that the film formation proceeds as a result of deposition of sufficiently coarse 200-700 nm colloid particles of sphalerite. It is demonstrated that this sensor can be used in studying the electrochemical reactions of ZnS and the interface phenomena by the methods of EQCM and cyclic voltammetry.

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Публикация на русском языке Получение пленок сульфида цинка на поверхности золота как сенсора электрохимического кварцевого микробаланса / Д. О. Криницын, А. С. Романченко, С. А. Воробьев [и др.] // Электрохим. - 2021. - Т. 57 № 12. - С. 762-768

Держатели документа:
Russian Acad Sci, Inst Chem & Chem Technol, Siberian Branch, Krasnoyarsk, Russia.
Siberian Fed Univ, Krasnoyarsk, Russia.
Russian Acad Sci, Kirenskii Inst Phys, Siberian Branch, Krasnoyarsk, Russia.

Доп.точки доступа:
Krinitsyn, D. O.; Romanchenko, A. S.; Vorob'ev, S. A.; Likhatskii, M. N.; Karacharov, A. A.; Krylov, A. S.; Крылов, Александр Сергеевич; Volochaev, M. N.; Волочаев, Михаил Николаевич; Mikhlin, Yu L.; Russian Scientific FoundationRussian Science Foundation (RSF) [18-17-00135]
}
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