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Труды сотрудников ИФ СО РАН

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    Raman spectra and structural phase transition in Pr3Sb5O12 crystal / A. Hojiboev [et al.] // Ferroelectrics. - 2015. - Vol. 486, Is. 1. - P. 86-90, DOI 10.1080/00150193.2015.1100043. - Cited References: 11. - A.S.O. and A.N.V. are partially supported by the Ministry of Education and Science of the Russian Federation . - ISSN 0015-0193
   Перевод заглавия: Спектры комбинационного рассеяния и структурный фазовый переход в кристалле Pr3Sb5O12

РУБ Materials Science, Multidisciplinary + Physics, Condensed Matter

Кл.слова (ненормированные):
Antimonite -- praseodymium -- soft mode -- Raman spectroscopy
Аннотация: Raman spectroscopy investigation of phase transition in Pr3Sb5O12 crystal is reported. Spectra were obtained in temperature range from 300 to 800 K. Soft mode restoration has been found below 735 K, that allows to attribute structural phase transition as displacive.

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Держатели документа:
Department of Theoretical Physics, Khujand State University, Khujand, Tajikistan
Laboratory of Molecular Spectroscopy, Kirensky Institute of Physics, SB RAS, Krasnoyarsk, Russian Federation
Department of Photonics and Laser Technology, Siberian Federal University, Krasnoyarsk, Russian Federation
Department of Biomedical Engineering, Vologda State University, Vologda, Russian Federation

Доп.точки доступа:
Hojiboev, A.; Oreshonkov, A. S.; Орешонков, Александр Сергеевич; Umarov, M.; Vtyurin, A. N.; Втюрин, Александр Николаевич
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Low-temperature behavior of the magnetoelastic characteristics of praseodymium ferroborate / G. A. Zvyagina [et al.] // Low Temp. Phys. - 2010. - Vol. 36, Is. 4. - P. 296-302 ; Физика низких температур, DOI 10.1063/1.3420962. - Cited References: 16 . - ISSN 1063-777X

РУБ Physics, Applied
Рубрики:
CRYSTAL
STATE
ND
Аннотация: The behavior of the elastic moduli and sound absorption in a PrFe(3)(BO(3))(4) single crystal at low temperatures is studied. A transition of the magnetic subsystem into an antiferromagnetically ordered state is manifested in the temperature behavior of the sound velocities and absorption. The characteristic behavior of the elastic properties of PrFe(3)(BO(3))(4) in an external magnetic field is observed. A phenomenological theory that gives a qualitative description of the observed features is constructed. It is proposed that a weak magnetic moment exists in the crystal. (C) 2010 American Institute of Physics. [doi: 10.1063/1.3420962]

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Держатели документа:
[Zvyagina, G. A.
Zhekov, K. R.
Bilych, I. V.
Zvyagin, A. A.] Natl Acad Sci Ukraine, BI Verkin Inst Low Temp Phys & Engn, UA-61103 Kharkov, Ukraine
[Zvyagin, A. A.] Tech Univ Dresden, Inst Solid State Phys, D-01069 Dresden, Germany
[Bezmaternykh, L. N.
Gudim, I. A.] Russian Acad Sci, Siberian Branch, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
ИФ СО РАН
B. I. Verkin Inst. for Low-Temperature Physics, Engineering, National Academy of Sciences of Ukraine, pr. Lenina 47, Kharkov 61103, Ukraine
B. I. Verkin Inst. for Low-Temperature Physics, Engineering, National Academy of Sciences of Ukraine, pr. Lenina 47, Kharkov 61103, Ukraine
Institute for Solid State Physics, Technical University Dresden, Dresden D-01069, Germany
L. V. Kirenskii Inst. of Physics of the Siberian Branch, The Russian Academy of Sciences, Krasnoyarsk 660036, Russian Federation

Доп.точки доступа:
Zvyagina, G. A.; Zhekov, K. R.; Bilych, I. V.; Zvyagin, A. A.; Bezmaternykh, L. N.; Безматерных, Леонард Николаевич; Gudim, I. A.; Гудим, Ирина Анатольевна

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Magnetooptic activity of f-d and f-f electron transitions in Pr3+ in the glass matrix LiB3O5 / A. M. Potseluyko [et al.] // Physica B. - 2000. - Vol. 291, Is. 1-2. - P. 89-96, DOI 10.1016/S0921-4526(99)01869-4. - Cited References: 17 . - ISSN 0921-4526

РУБ Physics, Condensed Matter
Рубрики:
FARADAY-ROTATION
OXIDE GLASSES
Кл.слова (ненормированные):
Faraday rotation -- magnetooptic activity -- praseodymium -- Electron transitions -- Faraday effect -- Light absorption -- Lithium compounds -- Praseodymium compounds -- Faraday rotation -- Transition wavelength -- Optical glass
Аннотация: The results of absorption, Faraday rotation and magnetic circular dichroism measurements for glasses with the composition of LiB3O5 + Pr2O3 are presented. The effective wavelength of the transition giving the main contribution to Faraday rotation in these glasses is determined. The contributions of several f-f transitions to Faraday rotation are separated and their magnetooptical activities are evaluated in comparison with the activity of the f-d transition. (C) 2000 Elsevier Science B.V. All rights reserved.

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Держатели документа:
SB RAS, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
ИФ СО РАН
L.V. Kirensky Institute of Physics, SB RAS, 660036, Krasnoyarsk, Russian Federation

Доп.точки доступа:
Potseluyko, A. M.; Edelman, I. S.; Эдельман, Ирина Самсоновна; Zabluda, V. N.; Заблуда, Владимир Николаевич; Bolsunovskaya, O. A.; Zamkov, A. V.; Замков, Анатолий Васильевич; Parshikov, S. A.; Zaytsev, A. I.
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Optical spectroscopy of PrFe3(BO3)(4): Crystal-field and anisotropic Pr-Fe exchange interactions / M. N. Popova [et al.] // Phys. Rev. B. - 2009. - Vol. 80, Is. 19. - Ст. 195101, DOI 10.1103/PhysRevB.80.195101. - Cited References: 36. - We thank S. Klimin for useful information concerning the structure of PrFeINF3/INF(BOINF3/INF)INF4/INF and E. Chukalina for participating in some measurements. This work was supported in part by the Russian Foundation for Basic Research (Grants No. 07-02-01185 and No. 09-02-00930) and by the Russian Academy of Sciences under the Programs for Basic Research. . - ISSN 1098-0121

РУБ Physics, Condensed Matter
Рубрики:
TRIGONAL GDFE3(BO3)(4)
   NDFE3(BO3)(4)
   DYFE3(BO3)(4)
   TRANSITIONS
   BORATE
   ION
   ND
Кл.слова (ненормированные):
antiferromagnetic materials -- crystal field interactions -- exchange interactions (electron) -- infrared spectra -- iron compounds -- magnetic susceptibility -- magneto-optical effects -- paramagnetic materials -- praseodymium compounds -- spin Hamiltonians -- visible spectra
Аннотация: High-resolution polarized optical absorption spectra of PrFe3(BO3)(4) in the paramagnetic and antiferromagnetic phases are reported. The measured energies of the crystal-field (CF) levels within the 4f(2) configuration of Pr3+ in the paramagnetic PrFe3(BO3)(4) are described by the CF model that involves the 4f(2)/4f5d and 4f(2)/4f6p configuration interactions. Ordering of Fe spins along the crystalline c axis below T-N=32 K is confirmed by the analysis of the spectra of Er3+ introduced as a probe into PrFe3(BO3)(4). To account for the observed changes in the optical spectra of Pr3+ at temperatures below T-N, in particular, for the shift of the CF levels, splitting of the CF doublets, and the appearance of forbidden lines, the Pr-Fe exchange Hamiltonian defined by seven parameters is considered. The theoretical approach has been tested by calculating the temperature dependence of the magnetic susceptibility. A good agreement between theory and optical and magnetic experimental data is found demonstrating the validity of the model used. The obtained results confirm that the model of the iron dimers inside the spiral chains of Fe3+(O2-)(6) octahedrons introduced by us earlier for NdFe3(BO3)(4) and modified in the present work may serve as a basis for analyzing the low-temperature properties of other rare-earth iron borates.

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Держатели документа:
[Popova, M. N.
Stanislavchuk, T. N.] Russian Acad Sci, Inst Spect, Troitsk 142190, Moscow Region, Russia
[Malkin, B. Z.] Kazan VI Lenin State Univ, Kazan 420008, Russia
[Bezmaternykh, L. N.] RAS, Siberian Branch, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
ИФ СО РАН
Institute of Spectroscopy, Russian Academy of Sciences, Troitsk, 142190 Moscow Region, Russian Federation
Kazan State University, 420008 Kazan, Russian Federation
L.V. Kirensky Institute of Physics, Siberian Branch, RAS, 660036 Krasnoyarsk, Russian Federation

Доп.точки доступа:
Popova, M. N.; Stanislavchuk, T. N.; Malkin, B. Z.; Bezmaternykh, L. N.; Безматерных, Леонард Николаевич; Russian Foundation for Basic Research [07-02-01185, 09-02-00930]; Russian Academy of Sciences under the Programs for Basic Research
}
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Breaking of the Selection Rules for Optical Transitions in the Dielectric PrFe3(BO3)(4) Crystal by a Praseodymium-Iron Exchange Interaction / M. N. Popova [et al.] // Phys. Rev. Lett. - 2009. - Vol. 102, Is. 18. - Ст. 187403, DOI 10.1103/PhysRevLett.102.187403. - Cited References: 26. - This work was supported in part by the RFBR under Grants No. 07-02-01185 and No. 07-02-00704 and by the Russian Academy of Sciences under the Programs for Basic Research. . - ISSN 0031-9007

РУБ Physics, Multidisciplinary
Рубрики:
SINGLE-CRYSTAL
   GDFE3(BO3)(4)
   PHASE
   DYFE3(BO3)(4)
   SPECTRUM
   LINES
Кл.слова (ненормированные):
Magnetic ordering temperatures -- Optical spectrum -- Order parameters -- Point symmetries -- Selection rules -- Exchange interactions -- Neon -- Praseodymium -- Single crystals -- Crystal symmetry
Аннотация: We report on the emergence of new lines in the optical spectrum of the PrFe3(BO3)(4) single crystal at the magnetic ordering temperature. The transitions between singlet crystal-field sublevels of Pr3+ ion with the same transformational properties, strictly forbidden for the trigonal D-3 point symmetry of this ion in PrFe3(BO3)(4), appear below the Neel temperature and grow in intensity as a square of the order parameter. We show that the phenomenon originates from the mixing of wave functions of different Pr3+ sublevels by the Pr-Fe exchange interaction.

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Держатели документа:
[Popova, M. N.
Stanislavchuk, T. N.] Russian Acad Sci, Inst Spect, Troitsk 142190, Moscow Region, Russia
[Malkin, B. Z.] Kazan VI Lenin State Univ, Kazan 420008, Russia
[Bezmaternykh, L. N.] Russian Acad Sci, LV Kirensky Phys Inst, Siberian Branch, Krasnoyarsk 660036, Russia
ИФ СО РАН
Institute of Spectroscopy, Russian Academy of Sciences, 142190 Troitsk, Moscow region, Russian Federation
Kazan State University, 420008 Kazan, Russian Federation
L.V. Kirensky Institute of Physics, Siberian Branch, RAS, 660036 Krasnoyarsk, Russian Federation

Доп.точки доступа:
Popova, M. N.; Stanislavchuk, T. N.; Malkin, B. Z.; Bezmaternykh, L. N.; Безматерных, Леонард Николаевич; RFBR [07-02-01185, 07-02-00704]; Russian Academy of Sciences
}
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Samoshkina, Yu. E.
Electronic and magnetic states of Pr and Mn in the Pr1–xSrxMnO3 films studied by XANES and XMCD spectroscopy / Y. E. Samoshkina, A. Rogalev // J. Exp. Theor. Phys. - 2018. - Vol. 126, Is. 5. - P. 660-665, DOI 10.1134/S1063776118040131. - Cited References: 35. - We thank V.I. Chichkov and N.V. Andreev (National University of Science and Technology MISiS) for the preparation of the manganite films. - This work was supported by the Russian Foundation for Basic Research (project no. 16-32-00209 mol_a) and a grant of the President of the Russian Federation (NSh-7559.2016.2). . - ISSN 1063-7761
Кл.слова (ненормированные):
Circular dichroism spectroscopy -- Dichroism -- Film growth -- Magnetic moments -- Manganese -- Praseodymium -- Strontium compounds -- X ray absorption
Аннотация: The spectral dependences of X-ray absorption near-edge spectroscopy (XANES) and X-ray magnetic circular dichroism (XMCD) and the field dependences of XMCD near the K edge of Mn and the L2,3 edges of Pr in the Pr0.8Sr0.2MnO3 and Pr0.6Sr0.4MnO3 films at T = 90 K are studied. The spectral dependences point to a mixed valence state of Mn and Pr in the films. It is found that, as compared to XANES, XMCD is more sensitive to the valence state of Pr4+. The field dependences of XMCD point to ferromagnetic behavior of Mn ions and the Van Vleck paramagnetism of Pr ions, which makes a significant contribution to the total magnetization of the films. It is shown that as the Sr concentration increases, the XMCD intensity at the K edge of Mn increases, which indicates a growth of the total magnetic moment of the film due to an increase in the 4p–3d hybridization.

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Публикация на русском языке Самошкина, Юлия Эрнестовна. Электронные и магнитные состояния Pr и Mn в пленках Pr1-xSrxMnO3 по данным спектроскопии XANES и XMCD [Текст] / Ю. Э. Самошкина, А. Л. Рогалев // Журн. эксперим. и теор. физ. - 2018. - Т. 153 Вып. 5. - С. 794-799

Держатели документа:
Kirensky Institute of Physics, Federal Research Center “Krasnoyarsk Scientific Center,” Siberian Branch, Russian Academy of Sciences, Krasnoyarsk, Russian Federation
European Synchrotron Radiation Facility, Grenoble, CS, France

Доп.точки доступа:
Rogalev, A.; Самошкина, Юлия Эрнестовна
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Heat capacity and thermodynamic properties of germanates CaR2Ge3O10 (R = Pr, Nd) in the region of 320–1000 K / L. T. Denisova, M. S. Molokeev, N. A. Galiakhmetova [et al.] // Russ. J. Phys. Chem. A. - 2022. - Vol. 96, Is. 5. - P. 913-917, DOI 10.1134/S0036024422050077. - Cited References: 30. - The authors are grateful to the Krasnoyarsk Regional Shared Resource Center of the Krasnoyarsk Science Center. This work was performed as part of a State Task for Siberian Federal University, project no. FSRZ-2020-0013 . - ISSN 0036-0244
Кл.слова (ненормированные):
neodymium and praseodymium calcium germanates -- differential scanning calorimetry -- high-temperature heat capacity
Аннотация: Sequential annealing of stoichiometric mixtures of CaCO3, Pr6O11(Nd2O3), and GeO2 in air at 1423–1473 K yields germanates CaPr2Ge3O10 and CaNd2Ge3O10. Their crystal structure is refined via X-ray diffraction. The high-temperature heat capacity (320–1000 K) is measured by means of differential scanning calorimetry. The thermodynamic properties of germanates are calculated using experimental dependences Cp = f(T).

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Публикация на русском языке Теплоемкость и термодинамические свойства германатов CaR2Ge3O10 (R = Pr, Nd) в области 320–1000 K [Текст] / Л. Т. Денисова, М. С. Молокеев, Н. А. Галиахметова [и др.] // Журн. физ. химии. - 2022. - Т. 96 № 5. - С. 615-620

Держатели документа:
Siberian Federal University, Krasnoyarsk, 660041, Russian Federation
Krasnoyarsk Science Center, Siberian Branch, Russian Academy of Sciences, Krasnoyarsk, 660036, Russian Federation

Доп.точки доступа:
Denisova, L. T.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Galiakhmetova, N. A.; Denisov, V. M.; Belousova, N. V.
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    Exploration of the crystal structure and thermal and spectroscopic properties of monoclinic praseodymium sulfate Pr2(SO4)3 / Y. G. Denisenko, V. V. Atuchin, M. S. Molokeev [et al.] // Molecules. - 2022. - Vol. 27, Is. 13. - Ст. 3966, DOI 10.3390/molecules27133966. - Cited References: 95. - This research was funded by the Russian Science Foundation (project 21-19-00046, in part of conceptualization). Some parts of the experiments were performed in the Krasnoyarsk Regional Center of Research Equipment of Federal Research Center “Krasnoyarsk Science Center SB RAS” . - ISSN 1420-3049
   Перевод заглавия: Исследование кристаллической структуры, термических и спектроскопических свойств моноклинного сульфата празеодима Pr2(SO4)3
Кл.слова (ненормированные):
praseodymium sulfate -- crystal structure -- thermal analysis -- thermal expansion anisotropy -- photoluminescence -- band structure -- vibrational properties
Аннотация: Praseodymium sulfate was obtained by the precipitation method and the crystal structure was determined by Rietveld analysis. Pr2(SO4)3 is crystallized in the monoclinic structure, space group C2/c, with cell parameters a = 21.6052 (4), b = 6.7237 (1) and c = 6.9777 (1) Å, β = 107.9148 (7)°, Z = 4, V = 964.48 (3) Å3 (T = 150 °C). The thermal expansion of Pr2(SO4)3 is strongly anisotropic. As was obtained by XRD measurements, all cell parameters are increased on heating. However, due to a strong increase of the monoclinic angle β, there is a direction of negative thermal expansion. In the argon atmosphere, Pr2(SO4)3 is stable in the temperature range of T = 30–870 °C. The kinetics of the thermal decomposition process of praseodymium sulfate octahydrate Pr2(SO4)3·8H2O was studied as well. The vibrational properties of Pr2(SO4)3 were examined by Raman and Fourier-transform infrared absorption spectroscopy methods. The band gap structure of Pr2(SO4)3 was evaluated by ab initio calculations, and it was found that the valence band top is dominated by the p electrons of oxygen ions, while the conduction band bottom is formed by the d electrons of Pr3+ ions. The exact position of ZPL is determined via PL and PLE spectra at 77 K to be at 481 nm, and that enabled a correct assignment of luminescent bands. The maximum luminescent band in Pr2(SO4)3 belongs to the 3P0 → 3F2 transition at 640 nm.

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Держатели документа:
Department of Inorganic and Physical Chemistry, Tyumen State University, Tyumen, 625003, Russian Federation
Department of General and Special Chemistry, Industrial University of Tyumen, Tyumen, 625000, Russian Federation
Institute of Inorganic and Analytical Chemistry, Justus-Liebig-University Giessen, Giessen, 35392, Germany
Laboratory of Optical Materials and Structures, Institute of Semiconductor Physics, SB RAS, Novosibirsk, 630090, Russian Federation
Research and Development Department, Kemerovo State University, Kemerovo, 650000, Russian Federation
Department of Applied Physics, Novosibirsk State University, Novosibirsk, 630090, Russian Federation
Department of Industrial Machinery Design, Novosibirsk State Technical University, Novosibirsk, 630073, Russian Federation
R&D Center “Advanced Electronic Technologies”, Tomsk State University, Tomsk, 634034, Russian Federation
Laboratory of Crystal Physics, Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
School of Engineering Physics and Radio Electronics, Siberian Federal University, Krasnoyarsk, 660041, Russian Federation
Department of Physics, Far Eastern State Transport University, Khabarovsk, 680021, Russian Federation
Laboratory of Coherent Optics, Kirensky Institute of Physics Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
Institute of Nanotechnology, Spectroscopy and Quantum Chemistry, Siberian Federal University, Krasnoyarsk, 660041, Russian Federation
Laboratory of Molecular Spectroscopy, Kirensky Institute of Physics Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
School of Engineering and Construction, Siberian Federal University, Krasnoyarsk, 660041, Russian Federation
Institute of Automation and Electrometry, Russian Academy of Sciences, Novosibirsk, 630090, Russian Federation
Research Department, Northern Trans-Ural Agricultural University, Tyumen, 625003, Russian Federation
Center for Materials Research (LaMa), Justus-Liebig-University Giessen, Giessen, 35392, Germany

Доп.точки доступа:
Denisenko, Y. G.; Atuchin, V. V.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Sedykh, A. E.; Khritokhin, N. A.; Aleksandrovsky, A. S.; Александровский, Александр Сергеевич; Oreshonkov, A. S.; Орешонков, Александр Сергеевич; Shestakov, N. P.; Шестаков, Николай Петрович; Adichtchev, S. V.; Pugachev, A. M.; Sal’nikova, E. I.; Andreev, O. V.; Razumkova, I. A.; Muller-Buschbaum, K.
}
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