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    Kirik, S. D.
    Monitoring MCM-41 synthesis by X-ray mesostructure analysis / S. D. Kirik, V. A. Parfenov, S. M. Zharkov // Micropor. Mesopor. Mater. - 2014. - Vol. 195. - P. 21-30, DOI 10.1016/j.micromeso.2014.04.012. - Cited References: 70. - The investigation was made with financial support of the Program of Presidium RAS (Project 24.37), RF State contracts No 02.740.11.0629, RFBR Grants: 11-03-00610a and 11-03-12161-ofi, RSF 14-13-000025. . - ISSN 1387-1811. - ISSN 1873-3093
   Перевод заглавия: Контроль синтеза МСМ-41 с помощью рентгеновского мезоструктурного анализа

РУБ Chemistry, Applied + Chemistry, Physical + Nanoscience & Nanotechnology + Materials Science, Multidisciplinary
Рубрики:
ORDERED MESOPOROUS MATERIALS
   ORDERED MESOPOROUS MATERIALS
   IN-SITU
   POWDER DIFFRACTION
   SILICA/SURFACTANT COMPOSITES
   ELECTRON-MICROSCOPY
   MOLECULAR-SIEVES
   STABLE MCM-41
   SILICA
   ADSORPTION
Кл.слова (ненормированные):
Hydrothermal stability -- MCM-41 -- Mesostructure -- TEM -- X-ray diffraction
Аннотация: The electron density maps calculated from X-ray diffraction patterns of the mesoporous silica material MCM-41 present averaged mesostructure images which in contrast to transmission electron microscopy (TEM) images are exceptionally repeating and represent the whole sample. It was shown that the averaged mesostructure parameters such as a unit cell parameter, a pore diameter, a wall width, a pore shape estimated from the X-ray powder diffraction data in combination with the continuous electron density function approach allow monitoring continuous set of the silica framework states at different stages of the material synthesis. The mentioned technique supplemented by N 2-adsorption measurements and transmission electron microscopy was applied for consideration of the MCM-41 hydrothermal stability. Attention has been given to the variations of the synthesis conditions affecting the hydrothermal stability, in particular the maintaining the basicity of the synthesis solution as well the substitution of the synthesis solution with water or a salt solution at hydrothermal treatment. The averaged pore shape was observed to be changed from cylindrical to hexagonal-prismatic form. The observed wall thickness was in the range from 0.75 to 1.25 nm. The competition of silica polycondensation and surface hydrolysis was shown to be responsible for the variety of framework geometry and hydrothermal stability. It has been established that the pore diameter increases generally due to the osmotic pressure of water. If the pores acquire the average prismatic hexagonal shape, the sample has low hydrothermal stability. Under the conditions favorable for the polycondensation the pores have averaged cylindrical shape and material demonstrates higher hydrothermal stability. Cooperative mechanism of mesostructure destruction under hydrothermal conditions was observed using TEM data and was discussed in connection with irregular polycondensation. © 2014 Elsevier Inc. All rights reserved.

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Держатели документа:
Siberian Fed Univ, Krasnoyarsk 660041, Russia
Inst Chem & Chem Technol SB RAS, Krasnoyarsk 660036, Russia
Kirensky Inst Phys SB RAS, Krasnoyarsk 660036, Russia

Доп.точки доступа:
Parfenov, V. A.; Zharkov, S. M.; Жарков, Сергей Михайлович
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Polarizing properties of a stretched film of a polymer-dispersed liquid crystal with a surfactant dopant / M. H. Egamov [et al.] // J. Opt. Technol. - 2014. - Vol. 81, Is. 7. - P. 414-417, DOI 10.1364/JOT.81.000414. - Cited References: 17. - This work was carried out with the partial support of Grant 12-03-00816 of the Russian Foundation for Basic Research, Grants 24.32 and 24.29 of the Presidium of the Russian Academy of Sciences, and joint project 30 of the Siberian Section of the Russian Academy of Sciences (SO RAN), and a joint project of the SO RAN and the National Scientific Council of Taiwan. . - ISSN 1070-9762. - ISSN 1091-0786

РУБ Optics
Рубрики:
ANISOTROPY
Аннотация: The transmittance anisotropy of a composite polymer-liquid-crystal film has been studied as it varies with the degree to which it is elongated. The composite film includes polyvinyl alcohol, the nematic liquid crystal 4-n-pentyl-4'-cyanobiphenyl, and the surfeiting cetyltrimethylammonium bromide, which initiates homeotropic adhesion of the nematic to the surface of the polymer. It is shown that, when the film is uniaxially stretched, the transmittance of the orthogonally polarized component of directly transmitted radiation and accordingly the degree of polarization abruptly increase, reaching saturation when it is stretched to twice its length. Such variation of the film's macroscopic optical properties can be caused by an orientational-structural transition to a homogeneous configuration of the director in deformed droplets of the nematic and makes it possible to substantially improve the optical characteristics of light polarizers based on such composite media. (C) 2014 Optical Society of America.

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Публикация на русском языке Поляризующие свойства вытянутой пленки капсулированного полимером жидкого кристалла с примесью сурфактанта [Текст] / М. Х. Эгамов [и др.] // Оптич. журн. : Санкт-Петербургский НИУ ИТМО, 2014. - Т. 81 № 7. - С. 67-71

Доп.точки доступа:
Egamov, M. H.; Эгамов, Мухтор Хасанович; Gerasimov, V. P.; Герасимов, Виктор Петрович; Krakhalev, M. N.; Крахалев, Михаил Николаевич; Prishchepa, O. O.; Прищепа, Оксана Олеговна; Zyryanov, V. Ya.; Зырянов, Виктор Яковлевич; Loiko, V. A.; Russian Foundation for Basic Research [12-03-00816]; Presidium of the Russian Academy of Sciences [24.32, 24.29]; Siberian Section of the Russian Academy of Sciences (SO RAN); SO RAN; National Scientific Council of Taiwan
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Specific Features of Ionic-Surfactant Method to Control Liquid Crystals (ILCC 2014) / V. S. Sutormin [et al.] // Book of abstracts of 25th International Liquid Crystal Conference (ILCC 2014). - 2014

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Доп.точки доступа:
Sutormin, V. S.; Сутормин, Виталий Сергеевич; Krakhalev, M. N.; Крахалев, Михаил Николаевич; Prishchepa, O. O.; Прищепа, Оксана Олеговна; Zyryanov, V. Ya.; Зырянов, Виктор Яковлевич; International Liquid Crystal Conference (25 ; 2014 ; 29 June - 4 July 2014 ; Dublin, Ireland)
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Electrically-controlled anchoring transitions in nematics doped with ionic surfactant / V. Ya. Zyryanov [et al.] // 12th Eur. Conf. Liq. Cryst. (ECLC-2013). - 2013. - Ст. O.29

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Доп.точки доступа:
Zyryanov, V.Ya.; Зырянов, Виктор Яковлевич; Sutormin, V. S.; Сутормин, Виталий Сергеевич; Krakhalev, M. N.; Крахалев, Михаил Николаевич; Prishchepa, O. O.; Прищепа, Оксана Олеговна; European Conference on Liquid Crystals(12 ; 2013 ; Sept. ; 22-27)
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Polarizing properties of the elongated PDLC films doped by surfactant / O. O. Prishchepa [et al.] // Book of abstracts of 25th International Liquid Crystal Conference (ILCC 2014). - 2014. - Ст. P3.040

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Доп.точки доступа:
Prishchepa, V. S.; Прищепа, Оксана Олеговна; Krakhalev, M. N.; Крахалев, Михаил Николаевич; Egamov, M. H.; Эгамов, Мухтор Хасанович; Loiko, V. A.; Gerasimov, V. P.; Герасимов, Виктор Петрович; International Liquid Crystal Conference (25 ; 2014 ; 29 June - 4 July 2014 ; Dublin, Ireland)
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Light scattering in the stretched film of polymer dispersed liquid crystal doped with surfactant / V. A. Loiko [et al.] // 15th Electromag. and Light Scattering Conf. (ELS-XV) : book of abstr. - 2015. - P. 139

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Доп.точки доступа:
Loiko, V. A.; Лойко В. А.; Krakhalev, M. N.; Крахалев, Михаил Николаевич; Egamov, M. H.; Эгамов, Мухтор Хасанович; Gerasimov, V. P.; Герасимов, Виктор Петрович; Prishchepa, O. O.; Прищепа, Оксана Олеговна; Zyryanov, V. Ya.; Зырянов, Виктор Яковлевич; Electromagnetic and Light Scattering Conference(15 ; 2015 ; Jun. ; 21-26 ; Leipzig, Germany)
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Gardymova, A. P.
Multistability in polymer-dispersed cholesteric liquid crystal film doped with ionic surfactant / A. P. Gardymova, V. Y. Zyryanov, V. A. Loiko // Tech. Phys. Lett. - 2011. - Vol. 37, Is. 9. - P. 805-808, DOI 10.1134/S1063785011090094. - Cited References: 12. - This study was supported in part by the Federal Targeted Program "Scientific and Pedagogical Personnel for Innovative Russia" (project no. P901) and the Siberian Branch of the Russian Academy of Sciences (project nos. 110 and 144). . - ISSN 1063-7850

РУБ Physics, Applied
Рубрики:
REFLECTIVE DISPLAYS
Аннотация: A memory effect has been discovered in composite films based on a polymer containing dispersed cholesteric liquid crystal, which is related to the modification of the surface anchoring by an ionic surfactant under the action of an applied electric field. Parameters of electric signals are selected that ensure the switching of the composite film between some stable states with different levels of optical transmittance.

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Держатели документа:
[Gardymova, A. P.] Siberian Fed Univ, Inst Engn Phys & Radio Elect, Krasnoyarsk 660041, Russia
Russian Acad Sci, LV Kirensky Phys Inst, Krasnoyarsk Sci Ctr, Siberian Branch, Krasnoyarsk 660036, Russia
Reshetnev Siberian State Aerosp Univ, Krasnoyarsk 660014, Russia
Natl Acad Sci Belarus, BI Stepanov Phys Inst, Minsk 220072, Byelarus
ИФ СО РАН
Institute of Engineering Physics and Radio Electronics, Siberian Federal University, Krasnoyarsk 660041, Russian Federation
Kirensky Institute of Physics, Krasnoyarsk Scientific Center, Siberian Branch, Russian Academy of Sciences, Krasnoyarsk 660036, Russian Federation
Reshetnev Siberian State Aerospace University, Krasnoyarsk 660014, Russian Federation
Stepanov Institute of Physics, National Academy of Sciences of Belarus, Minsk 220072, Belarus

Доп.точки доступа:
Zyryanov, V. Y.; Зырянов, Виктор Яковлевич; Loiko, V. A.
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Krakhalev, M. N.
Electro-Optical Characteristics of Polymer-Dispersed Liquid Crystal Film Controlled by Ionic-Surfactant Method / M. N. Krakhalev, V. A. Loiko, V. Y. Zyryanov // Tech. Phys. Lett. - 2011. - Vol. 37, Is. 1. - P. 34-36, DOI 10.1134/S1063785011010056. - Cited References: 5. - This study was supported in part by Russian Federal Agencies (project nos. P901 and 02.740.11.0220), the Russian Foundation for Basic Research (project no. 08-03-01007), and the Siberian Branch of the Russian Academy of Sciences (project nos. 27.1, 110, and 144). . - ISSN 1063-7850

РУБ Physics, Applied

Аннотация: The electro-optical characteristics of a composite film based on a polymer containing dispersed nematic liquid crystal (NLC) doped with an ionic surfactant have been studied. The threshold character of the reorientation of NLC droplets as well as the dependence of the modulation amplitude of light transmission on the electric field strength has been revealed for the effect of ionic modification of surface anchoring. The dynamical parameters of the optical response have been determined.

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Держатели документа:
[Krakhalev, M. N.] Russian Acad Sci, Siberian Branch, Krasnoyarsk Sci Ctr, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
Reshetnev Siberian State Aerosp Univ, Krasnoyarsk 660014, Russia
Natl Acad Sci Belarus, BI Stepanov Phys Inst, Minsk 220072, Byelarus
ИФ СО РАН
Kirensky Institute of Physics, Krasnoyarsk Scientific Center, Siberian Branch, Russian Academy of Sciences, Krasnoyarsk, 660036, Russian Federation
Reshetnev Siberian State Aerospace University, Krasnoyarsk, 660014, Russian Federation
Stepanov Institute of Physics, National Academy of Sciences of Belarus, Minsk, 220072, Belarus

Доп.точки доступа:
Loiko, V. A.; Zyryanov, V. Y.; Зырянов, Виктор Яковлевич; Крахалев, Михаил Николаевич
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Orientational transition in the cholesteric layer induced by electrically controlled ionic modification of the surface anchoring / V. S. Sutormin [et al.] // Liq. Cryst. - 2017. - Vol. 44, Is. 3. - P. 484-489, DOI 10.1080/02678292.2016.1218557. - Cited References:38. - This work was supported by Russian Foundation for Basic Research (RFBR) [Grant Numbers 15-02-06924 and 16-53-00073] and by the Siberian Branch of the Russian Academy of Sciences under Complex Program [II.2P 0358-2015-0010]. V.S.S. acknowledges financial support from RFBR [Grant Numbers 16-32-60036 and 16-32-00164]. . - ISSN 0267-8292. - ISSN 1366-5855

РУБ Chemistry, Multidisciplinary + Crystallography + Materials Science,
Рубрики:
NEMATIC LIQUID-CRYSTALS
   FIELD
   DROPLETS
   CELL
   ALIGNMENT
   GRATINGS
Кл.слова (ненормированные):
Cholesteric -- ionic surfactant -- anchoring transition -- twisted hybrid -- structure -- electrooptics
Аннотация: A reorientation of cholesteric liquid crystal with a large helix pitch induced by the electrically controlled ionic modification of the surface anchoring has been studied. In initial state, the cholesteric helix is untwisted completely owing to the normal surface anchoring specified by the cations adsorbed at the substrates. As a result, the homeotropic director configuration is observed within the cell. Under the action of DC electric field, one of the substrates becomes free from the layer of surface active cations, therefore, setting the planar surface anchoring. The latter, in turn, leads to the formation of the hybrid chiral structure. The threshold value and dynamic parameters have been estimated for this process as well as the range of control voltages, which do not allow the electrohydrodynamic instabilities. The twisted hybrid director configuration observed in the experiment has been analysed by means of the simulation of polarisation change of light propagating through the cholesteric layer with asymmetric (planar and homeotropic) surface anchoring on the cell substrates.

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Держатели документа:
Russian Acad Sci, Kirensky Inst Phys, Siberian Branch, Krasnoyarsk Sci Ctr, Krasnoyarsk 660036, Russia.
Siberian Fed Univ, Inst Engn Phys & Radio Elect, Krasnoyarsk, Russia.

Доп.точки доступа:
Sutormin, V. S.; Сутормин, Виталий Сергеевич; Timofeev, I. V.; Тимофеев, Иван Владимирович; Krakhalev, M. N.; Крахалев, Михаил Николаевич; Prishchepa, O. O.; Прищепа, Оксана Олеговна; Zyryanov, V. Ya.; Зырянов, Виктор Яковлевич; Russian Foundation for Basic Research (RFBR) [15-02-06924, 16-53-00073]; Siberian Branch of the Russian Academy of Sciences [II.2P 0358-2015-0010]; RFBR [16-32-60036, 16-32-00164]
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10.

Electrically induced anchoring transition in nematics with small or zero dielectric anisotropy / V. S. Sutormin [et al.] // Liq. Cryst. - 2017. - Vol. 44, Is. 3. - P. 577-581, DOI 10.1080/02678292.2016.1225840. - Cited References:23. - This work was supported by Russian Foundation for Basic Research under Grants [15-02-06924 and 16-53-00073] and by the Siberian Branch of Russian Academy of Sciences under Complex Program [II.2P 0358-2015-0010]. V.S.S. acknowledges financial support from Russian Foundation for Basic Research under Grants [16-32-60036 and 16-32-00164]. . - ISSN 0267-8292. - ISSN 1366-5855

РУБ Chemistry, Multidisciplinary + Crystallography + Materials Science,
Рубрики:
LIQUID-CRYSTAL
   IONIC MODIFICATION
   ORIENTATION
   ALIGNMENT
   DROPLETS
Кл.слова (ненормированные):
Nematic -- ionic surfactant -- anchoring transition -- hybrid homeoplanar -- structure -- dielectric anisotropy -- electrooptics
Аннотация: The orientational transitions induced by electrically controlled ionic modification of surface anchoring in liquid crystal cells based on the nematics with small or zero dielectric anisotropy Δε are considered. The type of director reorientation is shown to be independent of the sign of dielectric anisotropy and can be the same for the nematics with both negative and positive Δε. Besides, the orientational transition and corresponding switchable optical states do not depend on the Δε value and can be effectively realised even for the nematics with zero dielectric anisotropy.

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Держатели документа:
Russian Acad Sci, Kirensky Inst Phys, Siberian Branch, Krasnoyarsk Sci Ctr, Krasnoyarsk 660036, Russia.
Siberian Fed Univ, Inst Engn Phys & Radio Elect, Krasnoyarsk, Russia.

Доп.точки доступа:
Sutormin, V. S.; Сутормин, Виталий Сергеевич; Krakhalev, M. N.; Крахалев, Михаил Николаевич; Prishchepa, O. O.; Прищепа, Оксана Олеговна; Zyryanov, V. Ya.; Зырянов, Виктор Яковлевич; Russian Foundation for Basic Research [15-02-06924, 16-53-00073, 16-32-60036, 16-32-00164]; Siberian Branch of Russian Academy of Sciences [II.2P 0358-2015-0010]
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