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    Kirik, S. D.
    Monitoring MCM-41 synthesis by X-ray mesostructure analysis / S. D. Kirik, V. A. Parfenov, S. M. Zharkov // Micropor. Mesopor. Mater. - 2014. - Vol. 195. - P. 21-30, DOI 10.1016/j.micromeso.2014.04.012. - Cited References: 70. - The investigation was made with financial support of the Program of Presidium RAS (Project 24.37), RF State contracts No 02.740.11.0629, RFBR Grants: 11-03-00610a and 11-03-12161-ofi, RSF 14-13-000025. . - ISSN 1387-1811. - ISSN 1873-3093
   Перевод заглавия: Контроль синтеза МСМ-41 с помощью рентгеновского мезоструктурного анализа

РУБ Chemistry, Applied + Chemistry, Physical + Nanoscience & Nanotechnology + Materials Science, Multidisciplinary
Рубрики:
ORDERED MESOPOROUS MATERIALS
   ORDERED MESOPOROUS MATERIALS
   IN-SITU
   POWDER DIFFRACTION
   SILICA/SURFACTANT COMPOSITES
   ELECTRON-MICROSCOPY
   MOLECULAR-SIEVES
   STABLE MCM-41
   SILICA
   ADSORPTION
Кл.слова (ненормированные):
Hydrothermal stability -- MCM-41 -- Mesostructure -- TEM -- X-ray diffraction
Аннотация: The electron density maps calculated from X-ray diffraction patterns of the mesoporous silica material MCM-41 present averaged mesostructure images which in contrast to transmission electron microscopy (TEM) images are exceptionally repeating and represent the whole sample. It was shown that the averaged mesostructure parameters such as a unit cell parameter, a pore diameter, a wall width, a pore shape estimated from the X-ray powder diffraction data in combination with the continuous electron density function approach allow monitoring continuous set of the silica framework states at different stages of the material synthesis. The mentioned technique supplemented by N 2-adsorption measurements and transmission electron microscopy was applied for consideration of the MCM-41 hydrothermal stability. Attention has been given to the variations of the synthesis conditions affecting the hydrothermal stability, in particular the maintaining the basicity of the synthesis solution as well the substitution of the synthesis solution with water or a salt solution at hydrothermal treatment. The averaged pore shape was observed to be changed from cylindrical to hexagonal-prismatic form. The observed wall thickness was in the range from 0.75 to 1.25 nm. The competition of silica polycondensation and surface hydrolysis was shown to be responsible for the variety of framework geometry and hydrothermal stability. It has been established that the pore diameter increases generally due to the osmotic pressure of water. If the pores acquire the average prismatic hexagonal shape, the sample has low hydrothermal stability. Under the conditions favorable for the polycondensation the pores have averaged cylindrical shape and material demonstrates higher hydrothermal stability. Cooperative mechanism of mesostructure destruction under hydrothermal conditions was observed using TEM data and was discussed in connection with irregular polycondensation. © 2014 Elsevier Inc. All rights reserved.

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Держатели документа:
Siberian Fed Univ, Krasnoyarsk 660041, Russia
Inst Chem & Chem Technol SB RAS, Krasnoyarsk 660036, Russia
Kirensky Inst Phys SB RAS, Krasnoyarsk 660036, Russia

Доп.точки доступа:
Parfenov, V. A.; Zharkov, S. M.; Жарков, Сергей Михайлович
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    The influence of oxygen concentration on the formation of CuO and Cu2O crystalline phases during the synthesis in the plasma of low pressure arc discharge / A. V. Uschakov [et al.] // Vacuum. - 2016. - Vol. 128. - P. 123-127, DOI 10.1016/j.vacuum.2016.03.025. - Cited References: 19. - This study was supported by the Russian Foundation for Basic Research. (Project No 15-08-02132). . - ISSN 0042-207X
   Перевод заглавия: Влияние концентрации кислорода на формирование кристаллических фаз CuO и Cu2O в процессе синтеза в плазме дугового разряда низкого давления

РУБ Materials Science, Multidisciplinary + Physics, Applied
Рубрики:
Nanoparticles
Oxide
Кл.слова (ненормированные):
Oxides -- Vapor deposition -- X-ray diffraction -- Transmission electron microscopy (TEM) -- Catalytic properties
Аннотация: This paper describes the synthesis of copper oxide nanoparticles with different percentages of CuO and Cu2O phases. It was achieved by the control of the percentage of oxygen in the gas mixture (N2 + O2) in a plasma-chemical process of evaporation-condensation by means of low-pressure arc discharge. In all the experiments, the pressure in the plasma-chemical reactor remained constant at 60 Pa. By means of X-ray diffraction (XRD), high resolution transmission electron microscopy (HRTEM), energy-dispersive X-ray spectroscopy (EDS), Fourier transform infrared spectroscopy (FTIR) it was found that the average particle size was 6 nm, and Cu2O phase content decreases with increasing oxygen content in the gas mixture. High photocatalytic properties of Cu2O powder were shown by the example of the reaction of the methyl orange dye decomposition in water solution. The problems, associated with the performance of this method and the formation of crystalline phases, are discussed.

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Держатели документа:
Siberian Federal University, Russian Federation
Reshetnev Siberian State Aerospace University, Krasnoyarsk, Russian Federation
Krasnoyarsk Scientific Center of the Siberian Branch of the Russian Academy of Science, Krasnoyarsk, Russian Federation
Kirensky Institute of Physics, Russian Academy of Sciences, Russian Federation

Доп.точки доступа:
Uschakov, A. V.; Karpov, I. V.; Lepeshev, A. A.; Zharkov, S. M.; Жарков, Сергей Михайлович
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    Synthesis, morphology, and visible magnetic circular dichroism of Ni-C nanoparticles / D. A. Petrov [et al.] // J. Sib. Fed. Univ. Math. Phys. - 2016. - Vol. 9, Is. 4. - P. 481-484 ; Журн. СФУ. Сер. "Математика и физика", DOI 10.17516/1997-1397-2016-9-4-481-484. - Библиогр.: 2. - This work was supported by the RFBR grant 14-02-01211 and MOST 102-2112-M-153-002-MY3. . - ISSN 1997-1397
   Перевод заглавия: Синтез, морфология и видимый МКД наночастиц Ni-C
Кл.слова (ненормированные):
MCD -- Nanoparticles -- Ni-C -- TEM -- наночастицы -- МКД -- электронная микроскопия
Аннотация: Ni-C nanoparticles powder (NP) was synthesized using high-temperature pyrolysis of nickel nitrate in an organic solvent. The NP was characterized by transmission electron microscopy (TEM), energy dispersive x-ray spectroscopy (EDXS) and selected-area electron diffraction (SAED). Structural characterization of the samples confirmed the formation of small, medium and large Ni nanoparticles with face-centered cubic structure (fcc) and enlarged lattice parameter. Magnetic circular dichroism (MCD) of samples with different mean particle sizes showed a red shift with decrease of mean particle size. © Siberian Federal University. All rights reserved.
Порошок наночастиц Ni-C был синтезирован с помощью высокотемпературного пиролиза нитрата никеля в органическом растворителе. Наночастицы были исследованы с помощью просвечивающей электронной микроскопии, энергодисперсионной рентгеновской спектроскопии и дифракции электронов выбранной зоны. Структурная характеризация образцов подтвердила образование маленьких, средних и больших наночастиц никеля с гранецентрированной кубической структурой и увеличенным параметром решётки. Магнитный круговой дихроизм образцов с различными средними размерами частиц показал красное смещение при уменьшении среднего размера частиц.

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Держатели документа:
Kirensky Institute of Physics SB RAS, Akademgorodok, 50/38, Krasnoyarsk, Russian Federation
Siberian Federal University, Svobodny, 79, Krasnoyarsk, Russian Federation
National Pingtung University, Pingtung City, Pingtung County, Taiwan

Доп.точки доступа:
Petrov, D. A.; Петров, Дмитрий Анатольевич; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Zharkov, S. M.; Жарков, Сергей Михайлович; Lin, C.-R.; Shu, F.-R.; Tseng, Y.-T.

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    Исследование связи согласующей цепи c входными резонаторами каналов в микрополосковом диплексере / А. О. Афонин, А. А. Лексиков, И. В. Говорун [и др.] // Журн. СФУ. Техн. и технол. - 2020. - Т. 13, № 7. - С. 871-881 ; J. Sib. Fed. Univ. Engin. Technol., DOI 10.17516/1999-494X-0272. - Библиогр.: 11 . - ISSN 1999-494X. - ISSN 2313-6057
   Перевод заглавия: The Investigation of Coupling between Matching Circuit and Input Resonators of Channels in a Microstrip Diplexer
Кл.слова (ненормированные):
микрополосковый диплексер -- согласующая цепь -- регулярный нерезонансный отрезок микрополосковой линии -- коэффициенты связи -- квазистатическое приближение -- microstrip diplexer -- matching circuit -- regular non-resonant segment of microstrip line -- coupling coefficients -- quasi-TEM approach
Аннотация: В данной статье приведены результаты исследования коэффициентов связи согласующей цепи с входными резонаторами каналов в микрополосковом диплексере. Каналы диплексера представляют собой двухзвенные фильтры, а согласующая цепь – регулярный нерезонансный отрезок микрополосковой линии, помещенной между входными резонаторами каналов. Общий порт подключен к наружному концу отрезка, а его второй конец разомкнут. Исследования проводили теоретически с помощью компьютерной программы, разработанной на основе математических выражений, полученных применением одномерных моделей и квазистатического приближения. Результаты исследования показывают, что величина связи достаточно велика и использование согласующей цепи в виде нерезонансного отрезка микрополосковой линии позволяет проектировать диплексеры с широкими полосами пропускания каналов.
This paper deals with investigation of the coupling coefficients between the matching circuit and the input resonators of channels in a microstrip diplexer. Diplexer channels are two-section filters, and matching circuit is regular non-resonant segment of a microstrip line placed between input resonators of channels. The common port is connected to outer end of the segment and its second end is opened. Research was carried out theoretically using a computer program developed on the basis of mathematical expressions obtained by means of one-dimensional models and quasi-static approximation. The results show that a value of coupling is quite large and the use of the matching circuit in a form of a non-resonant segment of a microstrip line allows to design diplexers with wide fractional bandwidth of the channels.

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Держатели документа:
Институт физики им. Л.В. Киренского СО РАН Российская Федерация, Красноярск
Сибирский федеральный университет Российская Федерация, Красноярск

Доп.точки доступа:
Афонин, Алексей Олегович; Afonin, A. O.; Лексиков, Андрей Александрович; Leksikov, An. A.; Лексиков, Александр Александрович; Leksikov, A. A.; Говорун, Илья Валерьевич; Govorun, I. V.; Сержантов, Алексей Михайлович; Serzhantov, A. M.; Угрюмов, Андрей Витальевич; Ugryumov, A. V.

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Phase stability of nanolaminated epitaxial (Cr1-xFex)2AlC MAX phase thin films on MgO(111) and Al2O3(0001) for use as conductive coatings / H. Pazniak, M. Stevens, M. Dahlqvist [et al.] // ACS Appl. Nano Mat. - 2021. - Vol. 4, Is. 12. - P. 13761-13770, DOI 10.1021/acsanm.1c03166. - Cited References: 51. - This work has been supported by the Deutsche Forschungsgemeinschaft (DFG) within CRC/TRR 270, project B02 (Project-ID 405553726). The calculations were carried out using supercomputer resources provided by the Swedish National Infrastructure for Computing (SNIC) at the National Supercomputer Centre (NSC) and the High Performance Computing Center North (HPC2N) partially funded by the Swedish Research Council through grant agreement no. 2018-05973. J.R. acknowledges funding from the Knut and Alice Wallenberg Foundation. Support by the Interdisciplinary Center for Analytics on the Nanoscale (ICAN) of the University of Duisburg-Essen (DFG RIsources reference: RI_00313), a DFG-funded core facility (Project nos. 233512597 and 324659309), is gratefully acknowledged. M.F. acknowledges co-funding by the government of the Russian Federation (agreement no. 075-15-2019-1886) . - ISSN 2574-0970
Кл.слова (ненормированные):
MAX phase -- thin film -- DFT calculations -- pulsed laser deposition -- TEM/EDX -- electrical resistivity
Аннотация: In this study, we model the chemical stability in the (Cr1-xFex)2AlC MAX phase system using density functional theory, predicting its phase stability for 0 ‹ x ‹ 0.2. Following the calculations, we have successfully synthesized nanolaminated (Cr1-xFex)2AlC MAX phase thin films with target Fe contents of x = 0.1 and x = 0.2 by pulsed laser deposition using elemental targets on MgO(111) and Al2O3(0001) substrates at 600 °C. Structural investigations by X-ray diffraction and transmission electron microscopy reveal MAX phase epitaxial films on both substrates with a coexisting (Fe,Cr)5Al8 intermetallic secondary phase. Experiments suggest an actual maximum Fe solubility of 3.4 at %, corresponding to (Cr0.932Fe0.068)2AlC, which is the highest Fe doping level achieved so far in volume materials and thin films. Residual Fe is continuously distributed in the (Fe,Cr)5Al8 intermetallic secondary phase. The incorporation of Fe results in the slight reduction of the c lattice parameter, while the a lattice parameter remains unchanged. The nanolaminated (Cr0.932Fe0.068)2AlC thin films show a metallic behavior and can serve as promising candidates for highly conductive coatings.

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Faculty of Physics, Center for Nanointegration (CENIDE), University of Duisburg-Essen, Duisburg, 47057, Germany
Materials Design, Department of Physics, Chemistry, and Biology (IFM), Linkoping University, Linkoping, SE-581 83, Sweden
Ernst Ruska-Centre for Microscopy and Spectroscopy with Electrons (ER-C), Forschungszentrum Julich, Julich, 52425, Germany
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation

Доп.точки доступа:
Pazniak, H.; Stevens, M.; Dahlqvist, M.; Zingsem, B.; Kibkalo, L.; Felek, M.; Varnakov, S. N.; Варнаков, Сергей Николаевич; Farle, M.; Фарле, Михаель; Rosen, J.; Wiedwald, U.
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    FMR and TEM Studies of Co and Ni Nanoparticles Implanted in the SiO2 Matrix / I. S. Edelman [et al.] // Appl. Magn. Reson. - 2011. - Vol. 40, Is. 3. - P363-375, DOI 10.1007/s00723-011-0218-4. - Cited Reference Count: 51. - Гранты: The work was supported in part by the Russian Foundation for Basic Research, grant no. 11-02-00972-a, Ministry of Education and Science of the Russian Federation, Federal Target Program "Scientific and scientific-pedagogical personnel of innovative Russia'', contract no. 02.740.11.0797, and State Program "Development of the Scientific Potential of the Higher Education School'', project no. 2.1.1/6038. S.M. Zharkov acknowledges the financial support of the Russian government contract no. 02.740.11.0568. The electron microscopy investigations were carried out at the Joint Center of the Siberian Federal University. - Финансирующая организация: Russian Foundation for Basic Research [11-02-00972-a]; Ministry of Education and Science of the Russian Federation [02.740.11.0797]; State Program "Development of the Scientific Potential of the Higher Education School'' [2.1.1/6038]; Russian government [02.740.11.0568] . - MAY. - ISSN 0937-9347. - ISSN 1613-7507
Рубрики:
FERROMAGNETIC-RESONANCE
   MAGNETIC-PROPERTIES
   THIN-FILMS
   COBALT NANOPARTICLES
   ION-IMPLANTATION
   FINE PARTICLES
   GRANULAR FILMS
   ANISOTROPY
   POLYIMIDES
   RUTILE
Кл.слова (ненормированные):
energy dispersive x ray spectroscopy -- face-centered cubic structure -- fused silica plates -- g factors -- hexagonal close packing -- high dose -- high-dose implantation -- implantation dose -- implanted samples -- line shape -- magnetic parameters -- matrix -- metal nanoparticles -- ni nanoparticles -- nonsymmetric -- out-of-plane -- room temperature -- spherical shape -- subsurface layer -- tem -- temperature dependence -- thin magnetic films -- uniaxial magnetic anisotropy -- cobalt -- fused silica -- magnetic anisotropy -- nanoparticles -- silica -- silicon compounds -- transmission electron microscopy -- x ray spectroscopy -- ferromagnetic resonance
Аннотация: Fused silica plates have been implanted with 40 keV Co+ or Ni+ ions to high doses in the range of (0.25-1.0) x 10(17) ions/cm(2), and magnetic properties of the implanted samples have been studied with ferromagnetic resonance (FMR) technique supplemented by transmission electron microscopy, electron diffraction and energy dispersive X-ray spectroscopy. The high-dose implantation with 3d-ions results in the formation of cobalt and nickel metal nanoparticles in the irradiated subsurface layer of the SiO2 matrix. Co and Ni nanocrystals with hexagonal close packing and face-centered cubic structures have a spherical shape and the sizes of 4-5 nm (for cobalt) and 6-14 nm (for nickel) in diameter. Room-temperature FMR signals from ensembles of Co and Ni nanoparticles implanted in the SiO2 matrix exhibit an out-of-plane uniaxial magnetic anisotropy that is typical for thin magnetic films. The dose and temperature dependences of FMR spectra have been analyzed using the Kittel formalism, and the effective magnetization and g-factor values have been obtained for Co- and Ni-implanted samples. Nonsymmetric FMR line shapes have been fitted by a sum of two symmetrical curves. The dependences of the magnetic parameters of each curve on the implantation dose and temperature are presented.

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Держатели документа:
Siberian Fed Univ, Krasnoyarsk 660041, Russia
Russian Acad Sci, Siberian Branch, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
Zavoisky Physical-Technical Institute,Russian Academy of Sciences

Доп.точки доступа:
Edelman, I. S.; Эдельман, Ирина Самсоновна; Petrakovskaja, E. A.; Петраковская, Элеонора Анатольевна; Petrov, D. A.; Петров, Дмитрий Анатольевич; Zharkov, S. M.; Жарков, Сергей Михайлович; Khaibullin, R. I.; Nuzhdin, V. I.; Stepanov, A. L.
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Synthesis and study of superhigh-concentrated organosols of silver nanoparticles / S. A. Vorobyev, M. Yu. Flerko, S. A. Novikova [et al.] // Colloid J. - 2024. - Vol. 86, Is. 2. - P. 208-217, DOI 10.1134/S1061933X23601294. - Cited References: 33. - The work was carried out with the financial support of the basic project FWES-2021-0014 of the Institute of Chemistry and Chemical Technology, Siberian Branch, Russian Academy of Sciences, and the Federal Program "Priority 2030" using the equipment of the Krasnoyarsk regional center for collective use of the Federal Research Center Krasnoyarsk Scientific Center, Siberian Branch, Russian Academy of Sciences . - ISSN 1061-933X. - ISSN 1608-3067
Кл.слова (ненормированные):
silver nanoparticles (NPs) -- concentrated silver organosols -- phase transfer of nanoparticles -- X-ray photoelectron spectroscopy (XPS) -- transmission electron microscopy (TEM) -- conductive silver films
Аннотация: Due to their unique properties, organosols of silver nanoparticles are widely used in optical and semiconductor devices, to produce electrically and thermally conductive films, as catalysts, antibacterial materials, etc. This work proposes a simple and highly productive method for the preparation of silver organosols, which have a metal concentration as high as 1800 g/L and contain spherical nanoparticles with low polydispersity and a median size of 9.1 nm. The method consists in the initial preparation of silver nanoparticle hydrosols with a concentration of higher than 30 g/L followed by the transfer of the NPs into an organic phase of o-xylene. A set of physical research methods has been employed to study the regularities of the extraction of silver nanoparticles with o-xylene in the presence of cetyltrimethylammonium bromide (CTAB) and ethanol and to determine the optimal process conditions, under which the extraction degree is as high as 62.5%. It has been found that bromine anions contained in CTAB molecules cause the aggregation of some amount of silver nanoparticles with the formation of silver metal sediment in the aqueous phase. According to X-ray photoelectron spectroscopy data, the sediment contains bromide ions (up to 4 at %) on the particle surface. Organosols synthesized under optimal conditions are stable for more than 7 months and withstand repeated cycles of drying and redispersing. Silver organosols have been used to obtain metal films with an electrical conductivity of about 68 500 S/cm, which increases to 412 000 and 509 500 S/cm (87.8% of the electrical conductivity of bulk silver) after thermal treatment at 150 and 250°C, respectively.

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Держатели документа:
Institute of Chemistry and Chemical Technology, Siberian Branch, Russian Academy of Sciences, 660036, Krasnoyarsk, Russia
Siberian Federal University, 660041, Krasnoyarsk, Russia
Kirenskii Institute of Physics, Siberian Branch, Russian Academy of Sciences, 660036, Krasnoyarsk, Russia
Tomsk National Research State University, 634050, Tomsk, Russia

Доп.точки доступа:
Vorobyev, S. A.; Flerko, M. Yu.; Novikova, S. A.; Mazurova, E. V.; Tomashevich, Ye. V.; Likhatski, M. N.; Saikova, S. V.; Samoilo, A. S.; Zolotovsky, N. A.; Золотовский, Н. А.; Volochaev, M. N.; Волочаев, Михаил Николаевич
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