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Synthesis and structural properties of cubic G0-Rb2KMoO3F3 oxyfluoride / V. V. Atuchin [et al.] // Ceram. Int. - 2012. - Vol. 38, Is. 3. - P. 2455-2459, DOI 10.1016/j.ceramint.2011.11.013. - Cited References: 23. - This study was partly supported by RFBR (Grant 09-02-00062) and SB RAS (Grant 34). . - ISSN 0272-8842

РУБ Materials Science, Ceramics
Рубрики:
PHASE-TRANSITIONS
   FERROELECTRIC K3WO3F3
   (NH4)(3)MOO3F3
   TEMPERATURE
   PEROVSKITE
   ELPASOLITE
   CRYSTALS
   BEHAVIOR
   High temperature
   Melt solidification
   Micromorphologies
   Melt solidification
   Microstructure-final
   Oxyfluorides
   Space Groups
   Oxyfluorides
   X ray methods
Кл.слова (ненормированные):
Powders: solid state reaction -- Microstructure-final -- X-ray methods -- Alkali oxides -- Halides
Аннотация: High-temperature G0 polymorph of Rb2KMoO3F3 has been prepared by melt solidification. Micromorphology and chemical properties of the final product were evaluated by scanning electron microscopy (SEM) and X-ray photoelectron spectroscopy (XPS). The elpasolite-related crystal structure of G0-Rb2KMoO3F3 has been refined by Rietveld method at T = 298 K (space group Fm-3m, a = 8.92446(8) Å, V = 710.76(1) Å3; RB = 3.55%). Ferroelectric G1-Rb2KMoO3F3 polymorph, earlier reported at T˂328 K, is not found at T = 298 K.

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Держатели документа:
[Atuchin, V. V.] SB RAS, Inst Semicond Phys, Lab Opt Mat & Struct, Novosibirsk 630090 90, Russia
[Gavrilova, T. A.] SB RAS, Inst Semicond Phys, Lab Nanolithog & Nanodiagnost, Novosibirsk 630090 90, Russia
[Isaenko, L. I.
Zhurkov, S. A.] SB RAS, Inst Geol & Mineral, Lab Crystal Growth, Novosibirsk 530090 90, Russia
[Kesler, V. G.] SB RAS, Inst Semicond Phys, Lab Phys Principles Integrated Microelect, Novosibirsk 630090 90, Russia
[Molokeev, M. S.] SB RAS, Inst Phys, Lab Crystal Phys, Krasnoyarsk 660036 36, Russia

Доп.точки доступа:
Atuchin, V. V.; Gavrilova, T. A.; Isaenko, L. I.; Kesler, V. G.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Zhurkov, S. A.
}
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Golovnev, N. N.
Enrofloxacinium citrate monohydrate: Preparation, crystal structure, thermal stability and IR-characterization / N. N. Golovnev, A. D. Vasiliev, S. D. Kirik // J. Mol. Struct. - 2012. - Vol. 1021. - P. 112-117, DOI 10.1016/j.molstruc.2012.04.059. - Cited References: 22. - The authors are grateful to the Ministry of Education and Science (Government Contracts # 02.740.11.0629) for the financial support of the investigation. . - ISSN 0022-2860

РУБ Chemistry, Physical
Рубрики:
COCRYSTAL
   ANTIBACTERIAL
   BEHAVIOR
   STATE
   ACID
Кл.слова (ненормированные):
Enrofloxacin -- Citric acid -- Crystal structure -- IR spectra -- Thermal analysis
Аннотация: Enrofloxacinium citrate monohydrate (I), C19H 23FN3O3+В·C6H7O7- В·H2O, [C19H22FN3O3 - enrofloxacin, EnrH] has been crystallized from the mutual solution of citric acid and enrofloxacin in ambient conditions. The colorless crystals have been investigated using X-ray single crystal and powder techniques, and characterized by differential scanning calorimetry, thermogravimetry and infrared spectroscopy. The obtained compound can be considered as a salt with enrofloxacinium in the role of a cation and citrate as an anion. The ions ratio equals to 1:1. The compound crystallizes in the triclinic lattice with a = 9.0489(8) A, b = 9.6531(8) A, c = 14.913(1) A, ? = 98.813(1)В°, ? = 92.029(1)В°, ? = 91.013(1)В°, Z = 2, V = 1286.1(2) A3, S.G. P1?. The crystal structure determination reveals the importance of inter- and intramolecular interactions in the crystal formation. The EnrH2+andH3Cit- molecular ions are packed in alternating layers with water molecules inserted into the citrate layers. A citrate ion in the layer is linked via H-bondings with two adjacent ones and three water molecules. Enrofloxacinium cations are packaged by means of a benched mode and every cation is linked by three intermolecular thymus type H-bondings with nitrogens of adjacent cations and by two links with the oxygen of the citrate ions. The infrared spectra gave the evidence of H-bonding formation in the obtained salt. The ?-stacking interactions are observed between the aromatic cycles of the adjacent cations which are located in an antiparallel style in a layer. В© 2012 Elsevier B.V. All rights reserved.

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Держатели документа:
Siberian Federal University, Svobodny Ave. 79, Krasnoyarsk 660041, Russian Federation
Kirensky Institute of Physics SB RAS, Krasnoyarsk 660036, Russian Federation
Institute of Chemistry and Chemical Technology SB RAS, Krasnoyarsk 660036, Russian Federation

Доп.точки доступа:
Vasiliev, A. D.; Васильев, Александр Дмитриевич; Kirik, S. D.; Головнёв, Николай Николаевич
}
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Synthesis and magnetic states of cobalt in three-layer Co/Ge/Co films / G. S. Patrin [et al.] // Phys. Solid State. - 2014. - Vol. 56, Is. 2. - P. 302-309, DOI 10.1134/S1063783414020255. - Cited References: 13. - This study was supported by the Russian Foundation for Basic Research (project no. 11-02-00675-a). . - ISSN 1063-7834. - ISSN 1090-6460

РУБ Physics, Condensed Matter
Рубрики:
FERROMAGNETIC LAYER THICKNESS
   NANOSTRUCTURES
   BEHAVIOR
   SPACER
Аннотация: The magnetic properties of three-layer Co-Ge magnetic films have been studied experimentally as a function of technological conditions of their deposition. It has been found that the films deposited at a high deposition rate have a granular structure, and the films obtained at a low deposition rate have an X-ray amorphous structure. Electron microscopy and nuclear magnetic resonance studies have demonstrated that, at the same cobalt layer thickness, the semiconductor granule sizes depend on the average semiconductor layer thickness and correlate with the formation of different cobalt phases (amorphous, cubic, and hexagonal). The thermomagnetic properties of the films have been investigated. © 2014 Pleiades Publishing, Ltd.

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Публикация на русском языке Синтез и магнитные состояния кобальта в трехслойных пленках Co/Ge/Co [] / Г. С. Патрин [и др.] // Физ. тверд. тела : ФТИ РАН, 2014. - Т. 56 Вып. 2. - С. 301-307

Держатели документа:
Russian Acad Sci, LV Kirensky Phys Inst, Siberian Branch, Krasnoyarsk 660036, Russia
Siberian Fed Univ, Inst Engn Phys & Radio Elect, Krasnoyarsk 660074, Russia

Доп.точки доступа:
Patrin, G. S.; Патрин, Геннадий Семёнович; Turpanov, I. A.; Турпанов, Игорь Александрович; Kobyakov, A. V.; Кобяков, Александр Васильевич; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Patrin, K. G.; Патрин, Константин Геннадьевич; Li, L. A.; Ли, Людмила Алексеевна; Maltsev, V. K.; Мальцев, Вадим Константинович; Zharkov, S. M.; Жарков, Сергей Михайлович; Yushkov, V. I.; Юшков, Василий Иванович
}
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Raman spectroscopy of natural cordierite at high water pressure up to 5?GPa / A. Y. Likhacheva [et al.] // J. Raman Spectrosc. - 2012. - Vol. 43, Is. 4. - P. 559-563, DOI 10.1002/jrs.3060. - Cited References: 38. - We greatly appreciate the critical comments of Prof. R. Kaindl and an anonymous reviewer on this work, and we thank Dr G. Lepezin for providing the cordierite sample. This work was supported by RFBR grant 11-05-01121-a. . - ISSN 0377-0486

РУБ Spectroscopy
Рубрики:
SINGLE-CRYSTAL STRUCTURE
   X-RAY
   CHANNEL H2O
   BEHAVIOR
   SPECTRA
   CO2
   POLYMORPHISM
   DIFFRACTION
   CHEMISTRY
   CAVITIES
Кл.слова (ненормированные):
cordierite -- Raman spectroscopy -- high pressure -- phase transition
Аннотация: The high-pressure behaviour of cordierite, a widespread ring aluminosilicate with channels incorporating fluid compounds (H2O, CO2), is characterized by the absence of phase transitions up to 2.5 GPa. However, the distortion of the ring tetrahedra observed previously at 2.3 GPa is supposed to introduce a phase transition at higher pressure, which has not been checked so far. This work presents a high-pressure Raman spectroscopic study of natural cordierite compressed in water medium up to 4.7 GPa in a diamond anvil cell. At P > 4 GPa, a disordering of both the framework and intrachannel H2O subsystem is apparent from significant broadening of Raman peaks and the evolution of short-range order parameters. This is followed by abrupt shifts of the framework and O–H stretching modes at about 4.5 GPa, indicating a first-order phase transition. Its reversibility is seen from the recovery of the initial spectrum at P < 3 GPa. The shift amplitudes of different framework modes indicate the predominance of distortion over contraction of the framework polyhedra upon this transition. The disordering of the H2O subsystem in the high-pressure phase is likely a consequence of distortion of the channel-forming framework elements, which is supposed to be a driving force of this transition. Copyright © 2011 John Wiley & Sons, Ltd.

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Держатели документа:
[Likhacheva, Anna Yu.
Goryainov, Sergey V.
Bul'bak, Taras A.] RAS, SB, Sobolev Inst Geol Mineral, Novosibirsk 630090 90, Russia
[Krylov, Aleksandr S.] RAS, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
[Prasad, Pinnelli S. R.] Natl Geophys Res Inst, Council Sci & Ind Res, Hyderabad 500007, Andhra Pradesh, India

Доп.точки доступа:
Likhacheva, A. Y.; Goryainov, S. V.; Krylov, A. S.; Крылов, Александр Сергеевич; Bul'bak, T. A.; Prasad, PSR
}
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Caloric characteristics of PbTiO3 in the temperature range of the ferroelectric phase transition / E. A. Mikhaleva [et al.] // Phys. Solid State. - 2012. - Vol. 54, Is. 9. - P. 1832-1840, DOI 10.1134/S1063783412090181. - Cited References: 31. - This study was supported by the Russian Foundation for Basic Research (project no. 12-08-00079) and the Council on Grants from the President of the Russian Federation for Support of Leading Scientific Schools of the Russian Federation (grant no. NSh-4828.2012.2). . - ISSN 1063-7834

РУБ Physics, Condensed Matter
Рубрики:
SINGLE-CRYSTALS
   LEAD TITANATE
   DIELECTRIC PROPERTIES
   SOLID-SOLUTIONS
   PRESSURE
   PEROVSKITES
   DEPENDENCE
   BEHAVIOR
   HEAT
Аннотация: The heat capacity and thermal expansion of the PbTiO3 ceramic sample have been measured in the temperature range 80–970 K. The electrocaloric and barocaloric efficiencies of lead titanate in the ferroelectric phase transition range have been investigated by analyzing the experimental data in terms of the thermodynamic theory of phase transitions, the electrical equation of state P(T, E), the Pippard equation, and the S(T, p) diagram.

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Публикация на русском языке Калорические характеристики PbTiO3 в области сегнетоэлектрического фазового перехода [Текст] / Е. А. Михалева [и др.] // Физ. тверд. тела : Физико-технический институт им. А.Ф.Иоффе РАН, 2012. - Т. 54 Вып. 9. - С. 1719-1726

Держатели документа:
[Mikhaleva, E. A.
Flerov, I. N.
Gorev, M. V.] Siberian Fed Univ, Inst Engn Phys & Radio Elect, Krasnoyarsk 660074, Russia
[Mikhaleva, E. A.
Flerov, I. N.
Gorev, M. V.
Molokeev, M. S.
Cherepakhin, A. V.
Kartashev, A. V.
Mikhashenok, N. V.
Sablina, K. A.] Russian Acad Sci, Siberian Branch, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia

Доп.точки доступа:
Mikhaleva, E. A.; Михалева, Екатерина Андреевна; Flerov, I. N.; Флёров, Игорь Николаевич; Gorev, M. V.; Горев, Михаил Васильевич; Molokeev, M. S.; Молокеев, Максим Сергеевич; Cherepakhin, A. V.; Черепахин, Александр Владимирович; Kartashev, A. V.; Карташев, Андрей Васильевич; Mikhashenok, N. V.; Михашенок, Наталья Владимировна; Sablina, K. A.; Саблина, Клара Александровна
}
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Determination of the magnetic structure of SmFe3(BO3)4 by neutron diffraction: comparison with other RFe3(BO3)4 iron borates / C. Ritter [et al.] // J. Phys.: Condens. Matter. - 2012. - Vol. 24, Is. 38. - Ст. 386002, DOI 10.1088/0953-8984/24/38/386002. - Cited References: 40. - This work was supported by RFBR, grant No. 10-02-00765. . - ISSN 0953-8984

РУБ Physics, Condensed Matter
Рубрики:
SPIN REORIENTATION
   EARTH
   GDFE3(BO3)4
   BEHAVIOR
Аннотация: Temperature dependent neutron diffraction studies were performed on SmFe3(BO3)4. The crystallographic structure was determined to stay as R32 over the whole studied temperature range of 2 K ‹ T ‹ 300 K. A magnetic phase transition characterized by the magnetic propagation vector κ = [0 0 3/2] takes place at TN = 34 K. The magnetic structure sees an easy-plane arrangement within the trigonal basal a–b-plane of ferromagnetic layers of iron and samarium having a canting angle of about 70° relative to each other. Neighbouring layers in the c-direction are antiferromagnetically coupled; at 2 K the magnetic moment values amount to μFe = 4.2(1) μB and μSm = 0.8(2) μB. The non-Brillouin type increase of the iron magnetic moment below TN points to a strong Fe–Sm exchange and to the simultaneous appearance of long range magnetic order on both sublattices.

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Держатели документа:
[Ritter, C.] Inst Max Von Laue Paul Langevin, F-38042 Grenoble, France
[Pankrats, A.
Gudim, I.
Vorotynov, A.] RAS, Siberian Branch, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia

Доп.точки доступа:
Ritter, C.; Pankrats, A.I.; Панкрац, Анатолий Иванович; Gudim, I. A.; Гудим, Ирина Анатольевна; Vorotynov, A.M.; Воротынов, Александр Михайлович
}
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Aver'yanov, E. M.
New features of a smectic-A-crystal-B phase transition in a homologous series of liquid crystals / E. M. Aver'yanov // JETP Letters. - 2014. - Vol. 99, Is. 3. - P. 158-163, DOI 10.1134/S0021364014030047. - Cited References: 21 . - ISSN 0021-3640. - ISSN 1090-6487

РУБ Physics, Multidisciplinary
Рубрики:
POLARIZABILITY
   POLYMORPHISM
   ANISOTROPY
   MOLECULES
   BEHAVIOR
Аннотация: The components L j of the Lorentz tensor and the polarizability density of molecules G in the smectic-A and crystalline-B phases have been determined for homologues of the series of alkyl-p-(4-alkoxybenzylideneamino-)cinnamates. The quantity L j (G) in both phases is a linear (quadratic) function of the orientational order parameter of molecules S, which is invariant (noninvariant) with respect to the A-B transition, which is manifested in the form of jumps δL j and δG and enhancement of the G(S) dependence. An increase in the length of terminal molecular chains and weakening of interlayer correlation of molecules are accompanied by strengthening of the A-B transition of the first order and G(S) dependences in both phases together with an increase in δL j and δG. Change δG and dependence G(S) in the B phase are related to change in the conformation (flattening) of aromatic molecular cores.

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Публикация на русском языке Аверьянов, Евгений Михайлович. Новые особенности фазового перехода смектик-A-кристалл-B в гомологическом ряду жидких кристаллов [Текст] / Е. М. Аверьянов // Письма в Журн. эксперим. и теор. физ. : Наука, 2014. - Т. 99 Вып. 3-4. - С. 179-184

Доп.точки доступа:
Аверьянов, Евгений Михайлович
}
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Balaev, D. A.
Correlation between magnetoresistance and magnetization hysteresis in a granular high-T C superconductor: Impact of flux compression in the intergrain medium / D. A. Balaev, S. V. Semenov, M. I. Petrov // J. Supercond. Nov. Magn. - 2014. - Vol. 27, Is. 6. - P. 1425-1429, DOI 10.1007/s10948-014-2491-6. - Cited References: 27 . - ISSN 1557-1939. - ISSN 1557-1947

РУБ Physics, Applied + Physics, Condensed Matter
Рубрики:
HIGH-TEMPERATURE SUPERCONDUCTOR
   JOSEPHSON MEDIUM
   CRITICAL-STATE
   YBA2CU3O7-DELTA
   FIELDS
   BEHAVIOR
   HTSC
   COMPOSITES
   RESISTANCE
   MOTION
Кл.слова (ненормированные):
Granular superconductor -- Josephson medium -- Effective field -- Magnetoresistance -- Magnetization hysteresis
Аннотация: The correlation between experimental magnetic field dependences of magnetoresistance and magnetization hysteresis in granular YBa2Cu3O7 is established. Within the proposed approach, magnetoresistance is assumed to be determined by the effective field in the intergrain boundaries the ensemble of which is considered to be a Josephson medium. The effective field in the intergrain medium can be written in the form B (eff)(H)=H-4 pi M(H)x alpha, where alpha is the parameter of averaged demagnetizing factors of grains and the degree of flux compression. A comparison of experimental magnetoresistance R(H) and magnetization M(H) hysteresis dependences obtained at different external magnetic field sweep rates yields the value alpha similar to 10, which is caused by the flux compression between grains. The proposed model describes well most of the features of the magnetoresistance hysteresis in granular high-T (C) superconductors.

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Доп.точки доступа:
Semenov, S. V.; Семёнов, Сергей Васильевич; Petrov, M. I.; Петров, Михаил Иванович; Балаев, Дмитрий Александрович
}
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Direct and inverse magnetoelectric effects in HoAl3(BO3)4 single crystal / A. L. Freydman [et al.] // J. Appl. Phys. - 2014. - Vol. 115, Is. 17. - Ст. 174103, DOI 10.1063/1.4874270. - Cited References: 34. - This work was supported by Russian Foundation for Basic Research (Project Nos. 13-02-12442ofi_m2 and 14-02-00307). The authors are grateful to V. N. Ilyushchenko for the help in preparing of this manuscript. . - ISSN 0021-8979. - ISSN 1089-7550

РУБ Physics, Applied
Рубрики:
POLARIZATION
BEHAVIOR
ORDER
Аннотация: The direct (MEH-) and inverse (MEE-) magnetoelectric effects in the HoAl3(BO3)4 single crystal are studied. Temperature and magnetic field dependences of permittivity of the crystal are investigated. A relation between the investigated effects was established. It was found that the magnetoelectric effect can exist in crystals without magnetic order or spontaneous polarization. It was shown that the phenomena investigated are due to magnetostriction or magnetoelastic effect. The thermodynamic potential was considered for describing magnetoelectric effect at low magnetic fields. The results obtained are explained within a proposed qualitative microscopic model, based on interplay of configuration of 4f- electron subshell of the rare-earth element and applied magnetic or electric field.
Изучаются прямой (MEH-) и обратный (МЭА-) магнитоэлектрические эффекты в монокристалле HoAl3(BO3)4 . Зависимости диэлектрической проницаемости кристалла от температуры и магнитного поля исследованы. Была создана связь между исследованными эффектами. Было обнаружено, что магнитоэлектрический эффект может существовать в кристаллах без магнитного порядка или спонтанной поляризации. Было показано, что исследуемые явления происходят из-за магнитострикции или магнитоупругого эффекта. Термодинамический потенциал рассчитывался для описания магнитоэлектрический эффект в слабых магнитных полях. Полученные результаты объясняются в рамках предложенной качественной микроскопической модели, основанной на взаимодействии конфигурации 4f-электронов в подоболочке редкоземельного элемента и внешнего магнитного или электрического поля.

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Доп.точки доступа:
Freydman, A. L.; Фрейдман, Александр Леонидович; Balaev, A. D.; Балаев, Александр Дмитриевич; Dubrovskiy, A. A.; Дубровский, Андрей Александрович; Eremin, E. V.; Еремин, Евгений Владимирович; Temerov, V. L.; Темеров, Владислав Леонидович; Gudim, I. A.; Гудим, Ирина Анатольевна; Russian Foundation for Basic Research [13-02-12442ofi_m2, 14-02-00307]
}
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10.

Studies of ferroelectric and magnetic phase transitions in multiferroic PbFe0.5Ta0.5O3-PbTiO3 solid solution ceramics / I. P. Raevski [et al.] // J. Mater. Sci. - 2014. - Vol. 49, Is. 18. - P. 6459-6466, DOI 10.1007/s10853-014-8376-z. - Cited References: 35. - This study is partially supported by the Russian Foundation for Basic Research (RFBR) Project 12-08-00887_a and Research Committee of the University of Macau under Research and Development Grant for Chair Professor. . - ISSN 0022-2461. - ISSN 1573-4803

РУБ Materials Science, Multidisciplinary
Рубрики:
MOSSBAUER
   CRYSTALS
   BEHAVIOR
   NIOBATE
Аннотация: Dielectric, X-ray, Mossbauer and magnetization studies of (1 − x)PbFe0.5Ta0.5O3–(x)PbTiO3 ceramics with 0 ≤ x ≤ 0.3 have been carried out to determine the compositional evolution of ferroelectric and magnetic phase transition temperatures. Addition of PbTiO3 to PbFe0.5Ta0.5O3 increases the temperature T m of the dielectric permittivity maximum, decreases both the diffusion of this maximum and its frequency dependence. However, the Curie–Weiss temperature exceeds T m for all the compositions studied, indicating that the phase transition still remains diffused. Dilution of the (Fe, Ta)-sublattice by Ti lowers the Neel temperature T N but above a certain compositional threshold (x ≈ 0.1) fast lowering of T N stops and a new magnetic state stable in a rather wide compositional range appears. Large difference between the zero-field-cooled (ZFC) and FC magnetization–temperature curves as well as between the temperatures of magnetic phase transition determined from Mossbauer and magnetization studies for compositions with x 0.1 implies that this state is a spin-glass phase.

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Держатели документа:
Southern Fed Univ, Fac Phys, Rostov Na Donu 344090, Russia
Russian Acad Sci, Kirensky Inst Phys, Siberian Branch, Krasnoyarsk 660036, Russia
Univ Macau, Fac Sci & Technol, Taipa, Peoples R China
Natl Taiwan Univ Sci & Technol, Taipei 106, Taiwan

Доп.точки доступа:
Raevski, I. P.; Titov, V. V.; Malitskaya, M. A.; Eremin, E. V.; Еремин, Евгений Владимирович; Kubrin, S. P.; Blazhevich, A. V.; Chen, H.; Chou, C.-C.; Raevskaya, S. I.; Zakharchenko, I. N.; Sarychev, D. A.; Shevtsova, S. I.; Russian Foundation for Basic Research (RFBR) [12-08-00887_a]; Research Committee of the University of Macau
}
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