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Synthesis, structural, magnetic, and electronic properties of cubic CsMnMoO3F3 oxyfluoride / V. V. Atuchin [et al.] // J. Phys. Chem. C. - 2012. - Vol. 116, Is. 18. - P. 10162-10170, DOI 10.1021/jp302020f. - Cited References: 64. - We thank Dr. A.M. Ziatdinov for the electron paramagnetic resonance measurements. This study was partly supported by SB RAS (Grant 28). . - ISSN 1932-7447

РУБ Chemistry, Physical + Nanoscience & Nanotechnology + Materials Science, Multidisciplinary
Рубрики:
RAY PHOTOELECTRON-SPECTROSCOPY
   PHASE-TRANSITIONS
   CORE LEVELS
   SURFACE CHARACTERIZATION
   CRYSTAL-STRUCTURE
   CLEAVED SURFACE
   MIXED-VALENCE
   OXIDES
   MN
   MOLYBDENUM
   Chemical bondings
   Cubic phase
   Energy differences
   Heat capacity measurements
   Oxyfluorides
   Powder samples
   Solid-state synthesis
   Space Groups
   Temperature range
   Valence electron
   Binding energy
   Chemical bonds
   Electronic structure
   Fluorine compounds
   Magnetic properties
   Metal ions
   Photoelectrons
   Rietveld method
   X ray photoelectron spectroscopy
   Electronic properties
Аннотация: A powder sample of CsMnMoO3F3 oxyfluoride has been prepared by solid state synthesis. The pyrochlore-related crystal structure of CsMnMoO3F3 has been refined by the Rietveld method at T = 298 K (space group Fd-3m, a = 10.59141(4) angstrom, V = 1188.123(8) angstrom(3); R-B = 3.44%). The stability of the cubic phase has been obtained over the temperature range T = 110-293 K by heat capacity measurements. Magnetic properties have been measured over the range of T = 2-300 K. The electronic structure of CsMnMoO3F3 has been evaluated by X-ray photoelectron spectroscopy. Chemical bonding effects have been discussed for all metal ions using binding energy difference parameters and wide comparison with related oxides and fluorides. The competition between O-2(-) and F- ions for metal valence electrons has been found.

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Держатели документа:
Atuchin, Victor V.
Gavrilova, Tatyana A.
Kesler, Valery G.] SB RAS, Inst Semicond Phys, Novosibirsk 630090, Russia
Molokeev, Maxim S.
Yurkin, Gleb Yu.
Flerov, Igor N.
Patrin, Gennadii S.] SB RAS, Inst Phys, Krasnoyarsk 660036, Russia
Laptash, Natalia M.] FEB RAS, Inst Chem, Vladivostok 690022, Russia
Flerov, Igor N.
Patrin, Gennadii S.] Siberian Fed Univ, Inst Engn Phys & Radio Elect, Krasnoyarsk 660074, Russia

Доп.точки доступа:
Atuchin, V. V.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Yurkin, G. Yu.; Юркин, Глеб Юрьевич; Gavrilova, T. A.; Kesler, V. G.; Laptash, N. M.; Flerov, I. N.; Флёров, Игорь Николаевич; Patrin, G. S.; Патрин, Геннадий Семёнович
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    Magnetism and structure of Ni2MnBO5 ludwigite / E. Moshkina [et al.] // J. Magn. Magn. Mater. - 2016. - Vol. 402. - P. 69-75, DOI 10.1016/j.jmmm.2015.11.033. - Cited References: 23. - The authors are grateful to Professor N.V. Volkov and Professor A.N. Vasiliev for valuable discussions. This work was supported by Russian Foundation for Basic Research (grants No. 16-02-00055, 16-32-00318) . - ISSN 0304-8853
   Перевод заглавия: Магнетизм и структура людвигита Ni2MnBO5

РУБ Materials Science, Multidisciplinary + Physics, Condensed Matter
Рубрики:
CRYSTAL-STRUCTURE
   DIELECTRICS
   IFEFFIT
   Mn
Кл.слова (ненормированные):
Ludwigites -- Crystal structure -- Antiferromagnetic -- Indirect coupling model
Аннотация: Single crystals of ludwigite Ni2MnBO5 were synthesized by flux growth technique. The detailed structural and magnetic characterizations of the synthesized samples have been carried out. The cations composition of the studied crystal was determined using X-ray diffraction and EXAFS technique, the resulting composition is differ from the content of the initial Mn2O3–NiO components of flux. Magnetic susceptibility measurements and the calculations of the exchange integrals in frameworks of indirect coupling model revealed strong antiferromagnetic interactions and appearance of magnetic ordering phase at the temperature T=85 K. The hypothesis of the existence of several magnetic subsystems was supposed.

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Держатели документа:
L.V. Kirensky Institute of Physics SB RAS, Krasnoyarsk, Russian Federation
Siberian State Aerospace University Named after Academician M.F. Reshetnev, Krasnoyarsk, Russian Federation
National Research Centre Kurchatov Institute, Moscow, Russian Federation
Far Eastern State Transport University, Khabarovsk, Russian Federation
Siberian Federal University, Krasnoyarsk, Russian Federation

Доп.точки доступа:
Moshkina, E. M.; Мошкина, Евгения Михайловна; Sofronova, S. N.; Софронова, Светлана Николаевна; Veligzhanin, A.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Nazarenko, I. I.; Назаренко, Илья Иванович; Eremin, E. V.; Еремин, Евгений Владимирович; Bezmaternykh, L. N.; Безматерных, Леонард Николаевич
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Ferromagnetism and strong magnetic anisotropy of the PbMnBO4 orthoborate single crystals / A. Pankrats [et al.] // J. Magn. Magn. Mater. - 2016. - Vol. 414. - P. 82-89, DOI 10.1016/j.jmmm.2016.04.042. - Cited References: 20. - We acknowledge the assistance of A. Dubrovsky in magnetic measurements. - This work was supported by the Russian Foundation for Basic Research, Projects nos. 13-02-00897 and 16-02-00563. MVE thanks for support the Russian Government Program of Competitive Growth of the Kazan Federal University, decision no. 930_p, May 22, 2015. . - ISSN 0304-8853

РУБ Materials Science, Multidisciplinary + Physics, Condensed Matter
Рубрики:
PbMBO4 M
   Resonance
   Symmetry
   Mn
   Fe
   Cr
Кл.слова (ненормированные):
Strong ferromagnetic anisotropy -- Ferromagnetic resonance -- Exchange interactions
Аннотация: The PbMnBO4 orthoborate single crystals were first grown and their magnetic properties and ferromagnetic resonance were studied. It was found that the ferromagnetic state below the Curie temperature TC=31 K is characterized by the strong magnetic anisotropy. The significant effective anisotropy fields of PbMnBO4 determine the energy gap in the FMR spectrum, which is extraordinary large for ferromagnets (112 GHz at T=4.2 K). It was shown that the static Jahn-Teller effect characteristic of the Mn3+ ion leads to both the ferromagnetic ordering and the strong magnetic anisotropy in the crystal. In the strong external magnetic field the induced ferromagnetic ordering is retained in the crystal above the Curie temperature up to the temperatures multiply higher than TC. A weak anomaly of the dielectric permittivity was observed in PbMnBO4 at the Curie temperature at which the long-range ferromagnetic order is established. © 2016 Elsevier B.V. All rights reserved.

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Держатели документа:
Kirensky Institute of Physics, Russian Academy of Sciences, Siberian Branch, Krasnoyarsk, Russian Federation
Siberian Federal University, Krasnoyarsk, Russian Federation
Institute of Physics, Kazan Federal University, Kazan, Russian Federation

Доп.точки доступа:
Pankrats, A. I.; Панкрац, Анатолий Иванович; Sablina, K. A.; Саблина, Клара Александровна; Eremin, M.; Balaev, A. D.; Балаев, Александр Дмитриевич; Kolkov, M.; Колков, Максим Игоревич; Tugarinov, V. I.; Тугаринов, Василий Иванович; Bovina, A. F.; Бовина, Ася Федоровна
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