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Electrocaloric and barocaloric effects in some ferroelectric hydrosulfates and triglycinesulfate / E. A. Mikhaleva [et al.] // Ferroelectrics. - 2012. - Vol. 430. - P. 78-83, DOI 10.1080/00150193.2012.677717. - Cited References: 14. - This work was supported by the Council on Grants from the President of the Russian Federation for Support of Leading Scientific Schools (project no, Nsh - 4645.2010.2). . - ISSN 0015-0193

РУБ Materials Science, Multidisciplinary + Physics, Condensed Matter
Рубрики:
PHASE-TRANSITIONS
AMMONIUM
RbHSO4
Кл.слова (ненормированные):
Ferroelectrics -- phase transitions -- electrocaloric and barocaloric effects
Аннотация: A comparative analysis of electrocaloric and barocaloric efficiency of order-disorder ferroelectrics Rbx(NH4)1-xHSO4 and TGS is performed. A good agreement was found between intensive electrocaloric effects measured experimentally and calculated using electric equation of state. Barocaloric effects were evaluated analyzing the experimental data on heat capacity and T-p phase diagrams. In some crystals under study the same adiabatic temperature change can be produced by low pressure and rather high electric field.

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Доп.точки доступа:
Mikhaleva, E. A.; Михалева, Екатерина Андреевна; Flerov, I. N.; Флёров, Игорь Николаевич; Bondarev, V. S.; Бондарев, Виталий Сергеевич; Gorev, M. V.; Горев, Михаил Васильевич; Vasiliev, A. D.; Васильев, Александр Дмитриевич; Davydova, T. N.; Давыдова, Тамара Николаевна; European Meeting on Ferroelectricity(12 ; 2011 ; 26 June - 1 July ; Bordeaux, France)
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Thermal, structural, optical, dielectric and barocaloric properties at ferroelastic phase transition in trigonal (NH4)2SnF6: A new look at the old compound / I. N. Flerov [et al.] // J. Fluor. Chem. - 2016. - Vol. 183. - P. 1-9, DOI 10.1016/j.jfluchem.2015.12.010. - Cited References: 25. - The reported study was partially supported by RFBR, research project No. 15-02-02009a. . - ISSN 0022-1139

РУБ Chemistry, Inorganic & Nuclear + Chemistry, Organic
Рубрики:
Heat-capacity
   Ammonium
   (NH4)3TiF7
   Pressure
Кл.слова (ненормированные):
Fluorides -- Structural disorder -- Phase transitions -- Entropy -- Barocaloric effect
Аннотация: Structural phase transition P-3m1 → P-1 of the first order and nonferroelectric nature was found in (NH4)2SnF6 at about 110 K in the process of thermal, optical, dielectric and X-ray studies. Order-disorder transformation is accompanied by large changes of entropy (ΔS0 = 16.4 J/mol K) and volume (ΔV0/V ≈ 1%). The structural model associated with three orientations of NH4 tetrahedra in P-3m1 phase and their complete ordering in P-1 phase was suggested with the entropy change (ΔS0 = 18.3 J/mol K) close to the experimental value. A good agreement between baric coefficients measured in a direct way (dT0/dp = -157 K/GPa) and evaluated using entropy and volume changes at phase transition (-170 K/GPa) was found. Barocaloric effects in (NH4)2SnF6 are comparable with those of known solid state refrigerants and are characterised by a low-pressure need for realising their maximum values. © 2015 Elsevier B.V. All rights reserved.

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Держатели документа:
Kirensky Institute of Physics, Siberian Branch of RAS, Akademgorodok 50, Krasnoyarsk, Russian Federation
Institute of Engineering Physics and Radioelectronics, Siberian State University, Krasnoyarsk, Russian Federation
Astafijev Krasnoyarsk State Pedagogical University, Krasnoyarsk, Russian Federation
Krasnoyarsk State Agrarian University, Krasnoyarsk, Russian Federation
Far Eastern State Transport University, Khabarovsk, Russian Federation
Institute of Chemistry, Far Eastern Branch of RAS, Vladivostok, Russian Federation

Доп.точки доступа:
Flerov, I. N.; Флёров, Игорь Николаевич; Kartashev, A. V.; Карташев, Андрей Васильевич; Gorev, M. V.; Горев, Михаил Васильевич; Bogdanov, E. V.; Богданов, Евгений Витальевич; Mel'nikova, S. V.; Мельникова, Светлана Владимировна; Molokeev, M. S.; Молокеев, Максим Сергеевич; Pogoreltsev, E. I.; Погорельцев, Евгений Ильич; Laptash, N. M.
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Chemical exchange in NH4HSeO4 single crystals studied by two-dimensional H-2 nuclear magnetic resonance / Y. N. Ivanov [et al.] // J. Phys.: Condens. Matter. - 1999. - Vol. 11, Is. 18. - P. 3751-3760, DOI 10.1088/0953-8984/11/18/310. - Cited References: 16 . - ISSN 0953-8984

РУБ Physics, Condensed Matter
Рубрики:
PHASE-TRANSITIONS
CONDUCTIVITY PROCESSES
AMMONIUM
Кл.слова (ненормированные):
Hydrogen bonds -- Nuclear magnetic resonance -- Single crystals -- Thermal effects -- Ammonium hydrogen selenate -- Ammonium compounds
Аннотация: Processes of chemical exchange of deuterons in partially deuterated ammonium hydrogen selenate, NH4HSeO4 (AHSe), crystals are investigated by means of H-2 nuclear magnetic resonance (NMR) experiments over a wide temperature range. The temperature dependencies of the quadrupole line splittings in the one-dimensional spectra of AHSe above 350 K revealed lineshape changes which are characteristic for chemical exchange processes. A detailed study of these exchange processes in AHSe is achieved by means of two-dimensional H-2 NMR experiments. In the temperature range investigated, a chemical exchange occurs only between those deuteron (proton) sites which are involved in hydrogen bonds (alpha- and beta-positions). It was established that the rates of exchange between all types of hydrogen-bound deuteron are approximately the same. Exchange between these positions and the deuterons in the ND4 groups could not be detected. On the basis of our findings, we finally discuss a model for the microscopic mechanism of hydrogen transport in AHSe.

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Держатели документа:
LV Kirensky Phys Inst, Siberian Branch, Krasnoyarsk 660036, Russia
Univ Leipzig, Fak Phys & Geowissensch, D-04103 Leipzig, Germany
ИФ СО РАН
L V Kirensky Institute of Physics, Russian Academy of Science, Siberian Branch, 660036 Krasnoyarsk, Russian Federation
Universitat Leipzig, Fakultat fur Physik und Geowissenschaften, Linnestra?e 5, D-04103 Leipzig, Germany

Доп.точки доступа:
Ivanov, Y. N.; Иванов, Юрий Николаевич; Totz, J.; Michel, D.; Klotzsche, G.; Sukhovsky, A. A.; Суховский, Андрей Андреевич; Aleksandrova, I. P.; Александрова, Инга Петровна
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    Effect of a restricted geometry on thermal and dielectric properties of NH4HSO4 ferroelectric / E. A. Mikhaleva [et al.] // Ferroelectrics. - 2017. - Vol. 513, Is. 1. - P. 44-50, DOI 10.1080/00150193.2017.1350436. - Cited References:17. - The reported study was partially supported by the Russian Foundation for Basic Research (RFBR), research project No. 16-32-00092 mol_a. . - ISSN 0015-0193. - ISSN 1563-5112
   Перевод заглавия: Влияние ограниченной геометрии на тепловые и диэлектрические свойства сегнетоэлектриков NH4HSO4

РУБ Materials Science, Multidisciplinary + Physics, Condensed Matter
Рубрики:
PHASE-TRANSITIONS
   AMMONIUM
   CAPACITY
   SULFATE
   KH2PO4
Кл.слова (ненормированные):
Ferroelectric -- phase transition -- porous glass -- nanocomposite
Аннотация: Heat capacity, thermal dilatation, sensitivity to pressure and permittivity of NH4HSO4 embedded into glass matrices with a pore size of 320 nm and 46 nm were studied. Large difference in the thermal expansion of both glass and ferroelectric leads to a "clamped" state of NH4HSO4 in nanocomposites and to the phase transition temperatures change. The restricted geometry does not effect on the order of successive transformations in NH4HSO4 but is accompanied by a significant reduction in entropy of phase transitions. The behavior of DTA-signal and permittivity show the expansion of the temperature range of the ferroelectric phase under hydrostatic pressure.

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Доп.точки доступа:
Mikhaleva, E. A.; Михалева, Екатерина Андреевна; Flerov, I. N.; Флёров, Игорь Николаевич; Kartashev, A. V.; Карташев, Андрей Васильевич; Gorev, M. V.; Горев, Михаил Васильевич; Bogdanov, E. V.; Богданов, Евгений Витальевич; Bondarev, V. S.; Бондарев, Виталий Сергеевич; Korotkov, L. N.; Rysiakiewicz-Pasek, E.; Russian Foundation for Basic Research (RFBR) [16-32-00092 mol_a]; Russia/CIS/Baltic/Japan Symposium on Ferroelectricity(13 ; 2016 ; Jun. ; 19-23 ; Matsue, Japan)
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