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Magnetic nanoparticles formed in glasses co-doped with iron and larger radius elements / I. S. Edelman [et al.] // J. Appl. Phys. - 2012. - Vol. 112, Is. 8. - Ст. 84331. - P. , DOI 10.1063/1.4759244. - Cited References: 65. - This work was partly supported by the Russian Foundation for Basic Research, Grant Nos. 07-02-92174 RFBR-CNRS and 11-02-00972, and President of Russia Federation Grant No NSh 1044.2012.2. A. Artemenko acknowledges financial support from the Marie Curie International Incoming Fellowship within the 7th European Community Framework Programme (EPREXINA, GA 255662). The synchrotron measurements were supported via the Russian federal Contract No. 16.552.11.7003. The authors thank K. P. Polyakova for the preparation of thin films. . - ISSN 0021-8979

РУБ Physics, Applied
Рубрики:
SUPERPARAMAGNETIC RESONANCE
   FERROMAGNETIC-RESONANCE
   TEMPERATURE-DEPENDENCE
   FERRITE NANOPARTICLES
   OXIDE NANOPARTICLES
   FARADAY-ROTATION
   CERAMICS
   ANISOTROPY
   PARTICLES
   SPECTRA
Аннотация: A new type of nanoparticle-containing glasses based on borate glasses co-doped with low contents of iron and larger radius elements, Dy, Tb, Gd, Ho, Er, Y, and Bi, is studied. Heat treatment of these glasses results in formation of magnetic nanoparticles, radically changing their physical properties. Transmission electron microscopy and synchrotron radiation-based techniques: x-ray diffraction, extended x-ray absorption fine structure, x-ray absorption near-edge structure, and small-angle x-ray scattering, show a broad distribution of nanoparticle sizes with characteristics depending on the treatment regime; a crystalline structure of these nanoparticles is detected in heat treated samples. Magnetic circular dichroism (MCD) studies of samples subjected to heat treatment as well as of maghemite, magnetite, and iron garnet allow to unambiguously assign the nanoparticle structure to maghemite, independently of co-dopant nature and of heat treatment regime used. Different features observed in the MCD spectra are related to different electron transitions in Fe3+ ions gathered in the nanoparticles. The static magnetization in heat treated samples has non-linear dependence on the magnetizing field with hysteresis. Zero-field cooled magnetization curves show that at higher temperatures the nanoparticles occur in superparamagnetic state with blocking temperatures above 100 K. Below ca. 20 K, a considerable contribution to both zero field-cooled and field-cooled magnetizations occurs from diluted paramagnetic ions. Variable-temperature electron magnetic resonance (EMR) studies unambiguously show that in as-prepared glasses paramagnetic ions are in diluted state and confirm the formation of magnetic nanoparticles already at earlier stages of heat treatment. Computer simulations of the EMR spectra corroborate the broad distribution of nanoparticle sizes found by "direct" techniques as well as superparamagnetic nanoparticle behaviour demonstrated in the magnetization studies. (C) 2012 American Institute of Physics. [http://dx.doi.org/10.1063/1.4759244]

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Держатели документа:
[Edelman, I.
Ivanova, O.
Ivantsov, R.
Velikanov, D.
Zabluda, V.] LV Kirensky Inst Phys SB RAS, Krasnoyarsk 660036, Russia
[Zubavichus, Y.
Veligzhanin, A.] NRC Kurchatov Inst, Moscow 123182, Russia
[Zaikovskiy, V.] Siberian Branch RAS, Boreskov Inst Catalysis, Novosibirsk 630090, Russia
[Stepanov, S.] SI Vavilov State Opt Inst, St Petersburg, Russia
[Artemenko, A.] CNRS, ICMCB, UPR 9048, F-33608 Pessac, France
[Curely, J.
Kliava, J.] Univ Bordeaux 1, CNRS, UMR 5798, LOMA, F-33405 Talence, France

Доп.точки доступа:
Edelman, I. S.; Эдельман, Ирина Самсоновна; Ivanova, O. S.; Иванова, Оксана Станиславовна; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Zabluda, V. N.; Заблуда, Владимир Николаевич; Zubavichus, Y.; Veligzhanin, A. A.; Zaikovskiy, V. I.; Stepanov, S.; Artemenko, A.; Curely, J.; Kliava, J.
}
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Microstructure and Magnetooptics of Silicon Oxide with Implanted Nickel Nanoparticles / I. S. Edel'man [et al.] // J. Exp. Theor. Phys. - 2011. - Vol. 113, Is. 6. - P. 1040-1049, DOI 10.1134/S1063776111160035. - Cited References: 44. - This work was supported by the Russian Foundation for Basic Research (project nos. 11-02-00972, 11-02-90420, 11-02-91341) and the program Research and Scientific-Pedagogical Brainpower of Innovated Russia (State contract 02.740.11.0797). . - ISSN 1063-7761

РУБ Physics, Multidisciplinary
Рубрики:
SIMPLE METAL-CLUSTERS
   OPTICAL-PROPERTIES
   ION-IMPLANTATION
   FARADAY-ROTATION
   KERR SPECTRA
   GLASS
   RESONANCE
   PHYSICS
   ENERGY
   FE
Кл.слова (ненормированные):
Disperse structure -- Effective medium model -- Implanted samples -- Irradiation dose -- Magnetic circular dichroisms -- Magnetic Nickel -- Magneto-optical Faraday effect -- Magneto-optical measurements -- matrix -- Metal nanoparticles -- Metallic nickel -- Nickel nanoparticles -- Nickel particles -- Optical range -- Spectral dependences -- Surface plasma resonances -- Tensor components -- Thin near-surface layers -- Amorphous silicon -- Crystal microstructure -- Dichroism -- Faraday effect -- Ion implantation -- Magnetoplasma -- Metallic compounds -- Nanomagnetics -- Nanoparticles -- Nickel -- Silicon compounds -- Silicon oxides -- Spectroscopy -- Tensors -- Transmission electron microscopy -- Nickel oxide
Аннотация: Metallic nickel nanoparticles of various sizes are formed in a thin near-surface layer in an amorphous SiO2 matrix during 40-keV Ni+ ion implantation at a dose of (0.25-1.0) x 10(17) ions/cm(2). The micro-structure of the irradiated layer and the crystal structure, morphology, and sizes of nickel particles formed at various irradiation doses are studied by transmission electron microscopy and electron diffraction. The magnetooptical Faraday effect and the magnetic circular dichroism in an ensemble of nickel nanoparticles are studied in the optical range. The permittivity (epsilon) over cap tensor components are calculated for the implanted samples using an effective medium model with allowance for the results of magnetooptical measurements. The spectral dependences of the tensor (epsilon) over cap components are found to be strongly different from those of a continuous metallic nickel film. These differences are related to a disperse structure of the magnetic nickel phase and to a surface plasma resonance in the metal nanoparticles.

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Держатели документа:
[Edel'man, I. S.
Petrov, D. A.
Ivantsov, R. D.
Zharkov, S. M.] Russian Acad Sci, LV Kirensky Phys Inst, Siberian Branch, Krasnoyarsk 660036, Russia
[Zharkov, S. M.] Siberian Fed Univ, Krasnoyarsk 660041, Russia
[Khaibullin, R. I.
Valeev, V. F.
Nuzhdin, V. I.
Stepanov, A. L.] Russian Acad Sci, Zavoisky Phys Tech Inst, Kazan 420029, Russia
[Stepanov, A. L.] Kazan Volga Reg Fed Univ, Kazan 420018, Russia
ИФ СО РАН
Kirensky Institute of Physics, Russian Academy of Sciences, Siberian Branch, Akademgorodok, Krasnoyarsk, 660036, Russian Federation
Siberian Federal University, Svobodnyi pr. 79, Krasnoyarsk, 660041, Russian Federation
Zavoisky Physical-Technical Institute, Russian Academy of Sciences, Sibirskii trakt 10/7, Kazan, 420029, Russian Federation
Kazan (Volga Region), Federal University, ul. Kremlevskaya 18, Kazan, 420018, Russian Federation

Доп.точки доступа:
Edel'man, I. S.; Edelman, I. S.; Petrov, D. A.; Петров, Дмитрий Анатольевич; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Zharkov, S. M.; Жарков, Сергей Михайлович; Khaibullin, R. I.; Valeev, V. F.; Nuzhdin, V. I.; Stepanov, A. L.
}
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Structure and the magnetic and magneto-optical properties of Co-Sm-O nanogranular films / I. S. Edelman [et al.] // Phys. Solid State. - 2008. - Vol. 50, Is. 11. - P. 2109-2114, DOI 10.1134/S1063783408110176. - Cited References: 15. - We would like to thank G. V. Bondarenko for the performance of the x-ray fluorescence measurements of the samples under investigation.This study was supported by the Russian Foundation for Basic Research (project no. 07-02-92174) and performed within the framework of the Program "Development of the Scientific Potential of the Higher School" (project no. 2.1.1.7376). R.D. Ivantsov acknowledges the support of the Russian Science Support Foundation. . - ISSN 1063-7834

РУБ Physics, Condensed Matter
Рубрики:
FARADAY-ROTATION
   GRANULAR FILMS
   MAGNETORESISTANCE
   CO/SIO2
Кл.слова (ненормированные):
75 -- 50 -- Tt -- 75 -- 70 -- -i -- 78 -- 20 -- Ls
Аннотация: The magnetic properties and magneto-optical effects in nanocomposites based on Co-Sm-O films prepared through pulsed plasma sputtering of a SmCo(5) target are investigated. It is shown that, depending on the technological conditions and regimes of subsequent annealing, the films can have different structures from cobalt nanoparticles distributed in the dielectric samarium oxide matrix with a magnetic phase volume of more than 60% to a continuous polycrystalline cobalt film with embedded samarium oxide nanoparticles. The evolution of the spectra of the magneto-optical Kerr effect and the field dependences of the magnetization is studied as a function of the film structure.

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Держатели документа:
[Edelman, I. S.
Zhigalov, V. S.
Ivantsov, R. D.
Seredkin, V. A.
Zharkov, S. M.
Prokof'ev, D. E.
Frolov, G. I.] Russian Acad Sci, LV Kirensky Phys Inst, Siberian Branch, Krasnoyarsk 660036, Russia
[Seredkin, V. A.
Zharkov, S. M.] Siberian Fed Univ, Krasnoyarsk 660041, Russia
[Bondarenko, G. N.] Russian Acad Sci, Inst Chem & Chem Technol, Siberian Branch, Krasnoyarsk 660036, Russia
ИФ СО РАН
ИХХТ СО РАН
Kirensky Institute of Physics, Siberian Branch, Russian Academy of Sciences, Akademgorodok, Krasnoyarsk, 660036, Russian Federation
Siberian Federal University, Svobodnyi pr. 79, Krasnoyarsk, 660041, Russian Federation
Institute of Chemistry and Chemical Technology, Siberian Branch, Russian Academy of Sciences, ul. K. Marksa 42, Krasnoyarsk, 660036, Russian Federation

Доп.точки доступа:
Edelman, I. S.; Эдельман, Ирина Самсоновна; Zhigalov, V. S.; Жигалов, Виктор Степанович; Ivantsov, R. D.; Иванцов, Руслан Дмитриевич; Seredkin, V. A.; Середкин, Виталий Александрович; Zharkov, S. M.; Жарков, Сергей Михайлович; Prokof'ev, D. E.; Frolov, G. I.; Фролов, Георгий Иванович; Bondarenko, G. N.; Бондаренко, Галина Николаевна
}
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Magnetic and optical properties and electron paramagnetic resonance of gadolinium-containing oxide glasses / J. . Kliava [et al.] // J. Phys.: Condens. Matter. - 2003. - Vol. 15, Is. 40. - P. 6671-6681, DOI 10.1088/0953-8984/15/40/005. - Cited References: 30 . - ISSN 0953-8984

РУБ Physics, Condensed Matter
Рубрики:
ABSORPTION-SPECTRA
   FARADAY-ROTATION
   SPIN-RESONANCE
   IONS
   GD3+
   SPECTROSCOPY
   BEHAVIOR
   GD-3
Кл.слова (ненормированные):
Doping (additives) -- Electronic structure -- Glass -- Lanthanum compounds -- Light absorption -- Magnetic susceptibility -- Oxides -- Paramagnetic resonance -- Positive ions -- Rate constants -- Substitution reactions -- Absorption band -- Gadolinium containing oxide glasses -- Positive Weiss constants -- Gadolinium compounds
Аннотация: Magnetic susceptibility, electron paramagnetic resonance (EPR) and optical absorption have been studied in a glass system 20La(2)O(3)-22Al(2)O(3)-23B(2)O(3)-35(SiO2 + GeO2) with a part of La2O3 substituted by Gd2O3 in different concentrations. Positive Weiss constants have been found in more heavily doped glasses and ascribed to clustering of Gd3+ ions. Computer simulations of the EPR spectra show that the short-range ordering in the environment of the Gd3+ ions is well preserved. The relative distribution widths of the ligand coordinates are less than 2%. In the more heavily doped glasses the EPR spectra are superpositions of signals arising from isolated ions and ferromagnetic clusters. The increase of Gd3+ concentration is shown to change substantially the strong optical absorption edge while only small changes of f-f absorption band characteristics are observed. This difference is associated with the different effect of the Gd ion clustering on the mechanisms of the strong absorption in the ultraviolet region and the f-f absorption.

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Держатели документа:
Univ Bordeaux 1, CPMOH, F-33405 Talence, France
SI Vavilov State Opt Inst, St Petersburg 199034, Russia
Bar Ilan Univ, Dept Chem, IL-52900 Ramat Gan, Israel
Bar Ilan Univ, Dept Phys, IL-52900 Ramat Gan, Israel
RAS, SB, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
ИФ СО РАН
CPMOH, Universite Bordeaux-I, 33405 Talence Cedex, France
L V Kirensky Inst. of Physics, SB RAS, Krasnoyarsk 660036, Russian Federation
Bar-Ilan University, Department of Physics, Ramat-Gan 52900, Israel
Bar-Ilan University, Department of Chemistry, Ramat-Gan 52900, Israel
S V Vavilov State Optical Institute, St Petersburg 199034, Russian Federation

Доп.точки доступа:
Kliava, J.; Edelman, I. S.; Эдельман, Ирина Самсоновна; Potseluyko, A. M.; Petrakovskaja, E. A.; Петраковская, Элеонора Анатольевна; Berger, R.; Bruckental, I.; Yeshurun, Y.; Malakhovskii, A. V.; Малаховский, Александр Валентинович; Zarubina, Y. V.
}
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Magnetooptic activity of f-d and f-f electron transitions in Pr3+ in the glass matrix LiB3O5 / A. M. Potseluyko [et al.] // Physica B. - 2000. - Vol. 291, Is. 1-2. - P. 89-96, DOI 10.1016/S0921-4526(99)01869-4. - Cited References: 17 . - ISSN 0921-4526

РУБ Physics, Condensed Matter
Рубрики:
FARADAY-ROTATION
OXIDE GLASSES
Кл.слова (ненормированные):
Faraday rotation -- magnetooptic activity -- praseodymium -- Electron transitions -- Faraday effect -- Light absorption -- Lithium compounds -- Praseodymium compounds -- Faraday rotation -- Transition wavelength -- Optical glass
Аннотация: The results of absorption, Faraday rotation and magnetic circular dichroism measurements for glasses with the composition of LiB3O5 + Pr2O3 are presented. The effective wavelength of the transition giving the main contribution to Faraday rotation in these glasses is determined. The contributions of several f-f transitions to Faraday rotation are separated and their magnetooptical activities are evaluated in comparison with the activity of the f-d transition. (C) 2000 Elsevier Science B.V. All rights reserved.

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Держатели документа:
SB RAS, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
ИФ СО РАН
L.V. Kirensky Institute of Physics, SB RAS, 660036, Krasnoyarsk, Russian Federation

Доп.точки доступа:
Potseluyko, A. M.; Edelman, I. S.; Эдельман, Ирина Самсоновна; Zabluda, V. N.; Заблуда, Владимир Николаевич; Bolsunovskaya, O. A.; Zamkov, A. V.; Замков, Анатолий Васильевич; Parshikov, S. A.; Zaytsev, A. I.
}
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