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1.
Ultrafine particles derived
from mineral processing: A case study of the Pb-Zn sulfide ore with emphasis on lead-bearing colloids / Y. Mikhlin [et al.]> // Chemosphere. - 2016. -
Vol. 147
. - P. 60-66,
DOI
10.1016/j.chemosphere.2015.12.096. - Cited References: 47. - This research was supported by the Russian Science Foundation, Grant No. 14-17-00280. . - ISSN 0045-6535
Перевод заглавия:
Ультрадисперсные частицы, полученные при переработке минерального сырья: комплексный анализ колчеданной руды Pb-Zn и коллоидных частиц, содержащих свинец
РУБ
Environmental Sciences
Рубрики:
GALENA DISSOLUTION
METALLIC COPPER
NANOPARTICLES
SOIL
ENVIRONMENT
SEPARATION
TRANSPORT
FLOTATION
WATER
SIZE
Кл.слова (ненормированные):
Lead sulfide
--
Lead-zinc ore
--
Lead sulfide
--
Ultrafine particles
--
Aquatic nanoparticles
Аннотация:
Although mining and mineral processing industry is a vast source of heavy metal pollutants, the formation and behavior of micrometer- and nanometer-sized particles and their aqueous colloids entered the environment from the technological media has received insufficient attention to date. Here, the yield and characteristics of ultrafine mineral entities produced by routine grinding of the Pb-Zn sulfide ore (Gorevskoe ore deposit, Russia) were studied using laser diffraction analysis (LDA), dynamic light scattering (DLS) and zeta potential measurement, microscopy, X-ray photoelectron spectroscopy, with most attention given to toxic lead species. It was revealed, in particular, that the fraction of particles less that 1 ?m in the ground ore typical reaches 0.4 vol. %. The aquatic particles in supernatants were micrometer size aggregates with increased content of zinc, sulfur, calcium as compared with the bulk ore concentrations. The hydrodynamic diameter of the colloidal species decreased with time, with their zeta potentials remaining about -12 mV. The colloids produced from galena were composed of 20-50 nm PbS nanoparticles associated with lead sulfate and thiosulfate, while the surface oxidation products at precipitated galena were largely lead oxyhydroxides. The size and zeta potential of the lead-bearing colloids decreased with time down to about 100 nm and from -15 mV to -30 mV, respectively. And, conversely, lead sulfide nanoparticles were mobilized before the aggregates during redispersion of the precipitates in fresh portions of water. The potential environmental impact of the metal-bearing colloids, which is due to the large-scale production and relative stability, is discussed. © 2015 Elsevier Ltd.
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Держатели документа:
Inst. of Chemistry and Chemical Technology, Siberian Branch of the Russian Academy of Sciences, Akademgorodok, 50/24, Krasnoyarsk, Russian Federation
Siberian Federal University, Svobodny pr. 79, Krasnoyarsk, Russian Federation
Kirensky Institute of Physics, Siberian Branch of the Russian Academy of Sciences, Akademgorodok 50/38, Krasnoyarsk, Russian Federation
Доп.точки доступа:
Mikhlin, Y.; Vorobyev, S.; Romanchenko, A.; Karasev, S.; Karacharov, A.; Zharkov, S. M.; Жарков, Сергей Михайлович
}
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2.
Preparation and characterization
of colloidal copper xanthate nanoparticles / Y. Mikhlin [et al.]> // New J. Chem. - 2016. -
Vol. 40
,
Is. 4
. - P. 3059-3065,
DOI
10.1039/c6nj00098c. - Cited References:50. - This research was supported by the Russian Science Foundation grant 14-17-00280. We thank Dr Roberto Felix Duarte (HZB) and bilateral program "German-Russian laboratory at BESSY II" for assistance with the X-ray absorption experiments. . - ISSN 1144-0546. - ISSN 1369-9261
Перевод заглавия:
Получение и исследование коллоидных наночастиц ксантогената меди
РУБ
Chemistry, Multidisciplinary
Рубрики:
X-ray-absorption
Self-assembled monolayers
Sulfide nanoparticles
Electronic-structure
Waste-water
Complexes
Flotation
Spectroscopy
Adsorption
Oxidation
Аннотация:
Despite the important role of metal xanthates in a number of industrial processes and emerging applications, no attempts have been made to prepare the metal xanthate nanoparticles and to study colloidal solutions of insoluble heavy metal xanthates. Here, we examined the formation of colloidal copper xanthate particles during the reactions of aqueous solutions of cupric sulfate and various potassium xanthates, which occur in
flotation
and water treatment slurries and can be used to manufacture nanoparticles for materials science (e.g., as precursors for copper sulfide nanoparticles and biomedicine). The products were characterized using UV-vis absorption, dynamic light scattering, zeta potential measurements, transmission electron microscopy (TEM), electron diffraction, Fourier transform infrared spectroscopy, thermogravimetry, X-ray photoelectron spectroscopy, and X-ray absorption spectroscopy (XANES). Colloidal copper xanthates with compositions of ROCSSCu (R = ethyl, isopropyl, butyl, isobutyl, and amyl groups), disordered structures and average diameters of 20–80 nm easily formed and aggregated and were stable for at least several hours, especially if excessive xanthate was used. The hydrodynamic diameters of the nanoparticles were smaller at lower temperatures. Dixanthogens, which were produced in the reactions along with ROCSSCu, seemed to promote nanoparticle aggregation and precipitated with the copper xanthate, affecting their thermal decomposition. The TEM micrographs and S K- and Cu K-edge XANES spectra revealed core/shell particle morphologies, likely with Cu(I) bonded to four S atoms in the core and reduced copper coordination in the shell.
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Держатели документа:
Russian Acad Sci, Inst Chem & Chem Technol, Siberian Branch, Akad 50-24, Krasnoyarsk 6600036, Russia.
Siberian Fed Univ, Svobodny Pr 79, Krasnoyarsk 660041, Russia.
Russian Acad Sci, Siberian Branch, Kirensky Inst Phys, Akad 50-38, Krasnoyarsk 660036, Russia.
Доп.точки доступа:
Mikhlin, Y. L.; Михлин, Юрий Леонидович; Vorobyev, S.; Saikova, S. V.; Сайкова, С. В.; Tomashevich, Y.; Fetisova, O.; Kozlova, S.; Zharkov, S. M.; Жарков, Сергей Михайлович; Russian Science Foundation [14-17-00280]
}
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3.
Analysis of function
of copper sulfide nanoparticles as sphalerite
flotation
activator / S. A. Vorob’ev, E. A. Burdakova, A. A. Sarycheva [et al.]> // J. Min. Sci. - 2021. -
Vol. 57
,
Is. 1
. - P. 144-153,
DOI
10.1134/S1062739121010154. - Cited References: 22. - This study was supported by the Russian Science Foundation, project no. 18-17-00135 . - ISSN 1062-7391
Кл.слова (ненормированные):
nanoparticles
--
copper sulfide
--
flotation
--
sphalerite
--
activators
--
dynamic light scattering
--
X-ray photoelectron spectroscopy
Аннотация:
The authors compare the effect exerted by copper ions and sulphide copper nanoparticles on
flotation
of Gorevka deposit sphalerite using potassium n-butyl xanthate and in reagent-less regime. Covelline-like colloid particles 4–8 nm in size, obtained in interaction of copper (II) and sulfide ions in aqueous solutions, are characterized using the methods of dynamic light scattering, electron microscopy and diffraction. Sphalerite surface after reaction with copper ions and CuS dispersoid solutions are described by zeta-potential measurements and X-ray photoelectron spectroscopy. It is found that sphalerite
flotation
after activation with nanoparticles is lower than with copper ion solutions of the same concentrations, and improves with increasing duration of activation and
flotation
processes. The mechanism of CuS nanoparticles consists in creation of active centers for the collector to attach to, which intensifies the hydrophobic behavior and adsorption of the collector. Moreover, CuS nanoparticles promote formation of a special microrelief of the solid–liquid interface, which ensures rupture of liquid film and attachment of sphalerite particles to air bubbles when they collide.
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Публикация на русском языке
Изучение действия наночастиц сульфида меди как активатора флотации сфалерита [Текст] / С. А. Воробьев, Е. А. Бурдакова, И. В. Сарычева [и др.] // Физ.-техн. проблемы разраб. полез. ископаемых. - 2021. - № 1. - С. 159-168
Держатели документа:
Institute of Chemistry and Chemical Technology, Siberian Branch, Russian Academy of Sciences, Krasnoyarsk Science Center, Siberian Branch, Russian Academy of Sciences, Krasnoyarsk, 660036, Russian Federation
Siberian Federal University, Krasnoyarsk, 660041, Russian Federation
Kirensky Institute of Physics, Siberian Branch, Russian Academy of Sciences, Krasnoyarsk Science Center, Siberian Branch, Russian Academy of Sciences, Krasnoyarsk, 660036, Russian Federation
Reshetnev Siberian State University of Science and Technology, Krasnoyarsk, 660037, Russian Federation
Доп.точки доступа:
Vorob’ev, S. A.; Burdakova, E. A.; Sarycheva, A. A.; Volochaev, M. N.; Волочаев, Михаил Николаевич; Karacharov, A. A.; Likhatskii, M. N.; Mikhlin, Y. L.
}
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