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Chemistry of vinylidene complexes. XXIII. Binuclear rhenium-palladium vinylidene bridged complexes, their reactions with diiron nonacarbonyl / V. V. Verpekin [et al.]> // J. Organomet. Chem. - 2014. - Vol. 770. - P. 42-50, DOI 10.1016/j.jorganchem.2014.07.024. - Cited References: 56. - This article is dedicated to the memory of Alla B. Antonova.
. - ISSN 0022-328X. - ISSN 1872-8561РУБ Chemistry, Inorganic & Nuclear + Chemistry, Organic Рубрики: TRANSITION-METAL-COMPLEXES CATIONIC CARBYNE COMPLEXES RAY CRYSTAL-STRUCTURE MOLECULAR-STRUCTURE HETEROBIMETALLIC COMPLEXES LIGANDS MANGANESE CLUSTERS DINUCLEAR PD2CL2(MU-PH2PCH2PPH2)2 Кл.слова (ненормированные): Rhenium -- Palladium -- Iron -- Vinylidene complexes -- Heterometallic complexes Аннотация: The reaction of [Cp(CO)2ReCCHPh] (1) with [Pd(PPh3)4] followed by the treatment of resulting [Cp(CO)2RePd(μ-CCHPh)(PPh3)2] (2) with diphosphines (dppe, dppp) gave new complexes [Cp(CO)2RePd(μ-CCHPh)(dppe)] (3) and [Cp(CO)2RePd(μ-CCHPh)(dppp)] (4). Treatment of the synthesized complexes with [Fe2(CO)9] led to mixtures of [Cp(CO)2ReFe(μ-CCHPh)(CO)4] (5), [(dppe)PdFe2(CO)8] (6), [CpReFe2(μ3-CCHPh)(CO)8] (7), [CpReFePd(μ3-CCHPh)(CO)5(dppe)] (8) and of 5, [(dppp)PdFe2(CO)8] (9), [CpReFePd(μ3-CCHPh)(CO)5(dppp)] (10), respectively. The main products of both reactions were trinuclear μ3-vinylidene clusters 8 and 10. Reactions of the trinuclear μ3-vinylidene ReFePd clusters 8 and 10 with Fe2(CO)9 were also studied. New complexes were characterized by IR, 1H, 13C, 31P NMR spectroscopy and cyclic voltammetry. The structure of [CpReFe2(μ3-CCHPh)(CO)8] was determined by single-crystal X-ray diffraction.
Смотреть статью, Scopus, WOS, Читать в сети ИФ Держатели документа: Russian Acad Sci, Inst Chem & Chem Technol, Siberian Branch, Krasnoyarsk 660036, Russia Russian Acad Sci, Inst Phys, Siberian Branch, Krasnoyarsk 660036, Russia RAS, Siberian Branch, Krasnoyarsk Sci Ctr, Krasnoyarsk 660036, Russia Siberian Fed Univ, Krasnoyarsk 660041, Russia Доп.точки доступа: Verpekin, V. V.; Верпекин В. В.; Kondrasenko, A. A.; Кондрасенко, Александр Александрович; Chudin, O. S.; Чудин О. С.; Vasiliev, A. D.; Васильев, Александр Дмитриевич; Burmakina, G. V.; Бурмакина Г. В.; Pavlenko, N. I.; Павленко, Нина Ивановна; Rubaylo, A. I.; Рубайло, Анатолий Иосифович } Найти похожие
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