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Ivanov, Y. N.
B-11 NMR study of Ho1−x Y x Al3(BO3)4 multiferroics / Y. N. Ivanov, A. A. Sukhovskii, N. V. Volkov // J. Struct. Chem. - 2013. - Vol. 54, Is. 1 : Suppl. - P. 130-136DOI 10.1134/S0022476613070135
Аннотация: The 11B NMR method is used to study the crystals of trigonal alumina borates Ho1−x Y x Al3(BO3)4 (x = 0, 0.5, 1). The temperature-field evolution of quadrupole and hyperfine interactions in these compounds is studied and described.

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Публикация на русском языке Иванов, Юрий Николаевич. Исследование мультиферроиков Ho1-xYxAl3(BO3)4 методом ЯМР 11В / Ю. Н. Иванов // Журнал структурной химии : ФГУП "Издательство Сибирского отделения Российской акдемии наук", 2013. - Т. 54, Приложение. - С. 132-138. - ISSN 0136-7463

Доп.точки доступа:
Sukhovskii, A. A.; Суховский, Андрей Андреевич; Volkov, N. V.; Волков, Никита Валентинович; Иванов, Юрий Николаевич
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Calorimetric and 23Na MAS NMR study of the phase diagram of NANB1_xTAxO3 solid solutions / I. P. Aleksandrova [et al.] // Functional Materials. - 2010. - Vol. 17, Is. 1. - P. 18-23 . - ISSN 1027-5495
Аннотация: The heat capacity of NaNb1_xTaxO3 solid solutions was measured in the temperature range 100 to 770 K. The step-like change of phase transition temperature is observed in the T-x phase diagram at concentration x = 0.55. The obtained results are in a good agreement with the data of dielectric studies. The 23Na MAS NMR spectra were obtained at Larmor frequency 79.35 MHz using a Bruker AVANCE 300 spectrometer. The quadru-polar coupling constant, (CQ=e2qQ/h) and asymmetry parameter (n) were determined by computer fitting of the NMR line shape using the DMFit software. The found parameters show that solid solution structure is NaTa03-based at 0.7<X ?1 and NaNbO3-based at 0?x?0.5. The spectra in the intermediate region (0.5<x?0.7) can be described at a reasonable accuracy when assuming the coexistence of NaTaO3 and NaNbO3 structures. В© 2010 - STC "Institute for Single Crystals".

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Держатели документа:
L. V. Kirensky Institute of Physics, Russian Academy of Sciences, Siberian Branch, 660036 Krasnoyarsk, Russian Federation
Siberian Federal University, 660041 Krasnoyarsk, Russian Federation

Доп.точки доступа:
Aleksandrova, I. P.; Александрова, Инга Петровна; Ivanov, Y. N.; Иванов, Юрий Николаевич; Bondarev, V. S.; Бондарев, Виталий Сергеевич; Sukhovskii, A. A.; Суховский, Андрей Андреевич; Voronov, V. N.; Воронов, Владимир Николаевич
}
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Chemical exchange in NH4HSeO4 single crystals studied by two-dimensional H-2 nuclear magnetic resonance / Y. N. Ivanov [et al.] // J. Phys.: Condens. Matter. - 1999. - Vol. 11, Is. 18. - P. 3751-3760, DOI 10.1088/0953-8984/11/18/310. - Cited References: 16 . - ISSN 0953-8984

РУБ Physics, Condensed Matter
Рубрики:
PHASE-TRANSITIONS
CONDUCTIVITY PROCESSES
AMMONIUM
Кл.слова (ненормированные):
Hydrogen bonds -- Nuclear magnetic resonance -- Single crystals -- Thermal effects -- Ammonium hydrogen selenate -- Ammonium compounds
Аннотация: Processes of chemical exchange of deuterons in partially deuterated ammonium hydrogen selenate, NH4HSeO4 (AHSe), crystals are investigated by means of H-2 nuclear magnetic resonance (NMR) experiments over a wide temperature range. The temperature dependencies of the quadrupole line splittings in the one-dimensional spectra of AHSe above 350 K revealed lineshape changes which are characteristic for chemical exchange processes. A detailed study of these exchange processes in AHSe is achieved by means of two-dimensional H-2 NMR experiments. In the temperature range investigated, a chemical exchange occurs only between those deuteron (proton) sites which are involved in hydrogen bonds (alpha- and beta-positions). It was established that the rates of exchange between all types of hydrogen-bound deuteron are approximately the same. Exchange between these positions and the deuterons in the ND4 groups could not be detected. On the basis of our findings, we finally discuss a model for the microscopic mechanism of hydrogen transport in AHSe.

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Держатели документа:
LV Kirensky Phys Inst, Siberian Branch, Krasnoyarsk 660036, Russia
Univ Leipzig, Fak Phys & Geowissensch, D-04103 Leipzig, Germany
ИФ СО РАН
L V Kirensky Institute of Physics, Russian Academy of Science, Siberian Branch, 660036 Krasnoyarsk, Russian Federation
Universitat Leipzig, Fakultat fur Physik und Geowissenschaften, Linnestra?e 5, D-04103 Leipzig, Germany

Доп.точки доступа:
Ivanov, Y. N.; Иванов, Юрий Николаевич; Totz, J.; Michel, D.; Klotzsche, G.; Sukhovsky, A. A.; Суховский, Андрей Андреевич; Aleksandrova, I. P.; Александрова, Инга Петровна
}
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    Crystal structure and phase transitions of a layered perovskite-like CsScF4 crystal / A. S. Krylov [et al.] // CrystEngComm. - 2016. - Vol. 18, Is. 43. - P. 8472-8486, DOI 10.1039/c6ce01144f. - Cited References:47. - The authors are grateful to Prof. I. N. Flerov for valuable support and useful discussions. This work was partly supported by the Russian Foundation for Basic Research, Project 16-02-00102. The research is partially conducted within the framework of the state task of the Ministry of Education and Science of the Russian Federation for Siberian Federal University on R&D performance in 2014 (Task 3.2534.2014/K). X-ray data from powders, Raman NMR, and IR spectra were obtained with use the analytical equipment of Krasnoyarsk Center of collective use SB RAS. . - ISSN 1466-8033
   Перевод заглавия: Кристаллическая структура и фазовые переходы в слоистом перовскитоподобном кристалле CsScF4

РУБ Chemistry, Multidisciplinary + Crystallography
Рубрики:
NEGATIVE THERMAL-EXPANSION
RAMAN-SCATTERING
LATTICE-DYNAMICS
Аннотация: This work is devoted to the complex research on temperature phase transitions in a CsScF4 crystal. The crystal structure was solved and refined at different temperatures by using the Rietveld method. Structural phase transitions were investigated by using the following spectroscopic methods, some of them for the first time: Brillouin spectroscopy, Raman spectroscopy, IR absorption spectroscopy and NMR. The symmetry analysis of the Brillouin zone center of all phases is presented. The vibrational spectra of the crystal in three phases have been calculated. The structural phase transition mechanism was determined. The transitions at T-1 = 475 K and T-2 = 317.5 K are of displacement type. The Raman soft modes have been associated with rotations of the ScF6 octahedral group.

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Держатели документа:
SB RAS, LV Kirensky Inst Phys, Krasnoyarsk 660036, Russia.
Far Eastern State Transport Univ, Dept Phys, Khabarovsk 680021, Russia.
Siberian Fed Univ, Inst Engn Phys & Radioelect, Krasnoyarsk 660041, Russia.
SB RAS, Inst Automat & Electrometry, Novosibirsk 630090, Russia.

Доп.точки доступа:
Krylov, A. S.; Крылов, Александр Сергеевич; Molokeev, M. S.; Молокеев, Максим Сергеевич; Misyul, S. V.; Krylova, S. N.; Крылова, Светлана Николаевна; Oreshonkov, A. S.; Орешонков, Александр Сергеевич; Ivanenko, A. A.; Иваненко, Александр Анатольевич; Zykova, V. A.; Ivanov, Y. N.; Иванов, Юрий Николаевич; Sukhovsky, A. A.; Суховский, Андрей Андреевич; Voronov, V. N.; Воронов, Владимир Николаевич; Safonov, I. N.; Vtyurin, A. N.; Втюрин, Александр Николаевич; Russian Foundation for Basic Research [16-02-00102]
}
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Detection of the incommensurate modulation of the hydrogen-bond double-minimum potential in the antiferroelectric phase of NH4HSEO4 / I. P. Aleksandrova [et al.] // Phys. Lett. A. - 1983. - Vol. 95, Is. 6. - P. 339-342, DOI 10.1016/0375-9601(83)90035-X. - Cited References: 15 . - ISSN 0375-9601

РУБ Physics, Multidisciplinary

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Держатели документа:
L.V. Kirensky Institute of Physics, Krasnoyarsk, 660036, Russian Federation
ИФ СО РАН
Доп.точки доступа:
Aleksandrova, I. P.; Александрова, Инга Петровна; Rosanov, O. V.; Sukhovsky, A. A.; Суховский, Андрей Андреевич; Moskvich, Y. N.; Москвич, Юрий Николаевич
}
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Dislocation instability of an incommensurate phase in connection with the floating phase in an NH4HSeO4 crystal / I. P. Aleksandrova, Yu. N. Moskvich, O. V. Rozanov [et al.] // JETP Letters. - 1984. - Vol. 40, Is. 4. - P. 879-881. - Cited References: 7 . - ISSN 0021-3640

РУБ Physics, Multidisciplinary

WOS
Доп.точки доступа:
Aleksandrova, I. P.; Александрова, Инга Петровна; Moskvich, Yu. N.; Москвич, Юрий Николаевич; Rozanov, O. V.; Sadreev, A. F.; Садреев, Алмаз Фаттахович; Sukhovskii, A. A.; Суховский, Андрей Андреевич
}
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Dislocations and time-dependent dynamics of the incommensurate phase of NH4HSEO4 / I. P. Aleksandrova [et al.] // Ferroelectr. Lett. Sect. - 1984. - Vol. 1, Is. 5-6. - P. 131-134, DOI 10.1080/07315178408202410. - Cited References: 5 . - ISSN 0731-5171

РУБ Physics, Condensed Matter

WOS
Доп.точки доступа:
Aleksandrova, I. P.; Александрова, Инга Петровна; Moskvich, Yu. N.; Москвич, Юрий Николаевич; Rozanov, O. V.; Sukhovsky, A. A.; Суховский, Андрей Андреевич
}
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Effect of impurities on the successive phase transitions in (Cs1-xRbx)(2)ZnI4 compounds / I. P. Aleksandrova [et al.] // J. Phys.: Condens. Matter. - 2002. - Vol. 14, Is. 49. - P. 13623-13634, DOI 10.1088/0953-8984/14/49/316. - Cited References: 27 . - ISSN 0953-8984

РУБ Physics, Condensed Matter
Рубрики:
X-RAY
   CS2ZNI4
   SYSTEM
   HEAT
Кл.слова (ненормированные):
Phase transitions -- Point defects -- Specific heat -- Temperature -- X ray diffraction analysis -- Zinc compounds -- Lock-in transition -- Nuclear quadrupole resonance -- Single crystals
Аннотация: The heat capacity, nuclear quadrupole resonance (NQR) and x-ray diffraction of (Cs1-xRbx)(2)ZnI4 single crystals have been measured, for x = 0, 0.001, 0.005, 0.01, 0.025 and 0.05. The normal to incommensurate (N-Inc) phase transition at T-I, the incommensurate to commensurate (Inc-C) lock-in transition at T-L and the structural commensurate monoclinic to triclinic transition at T-LT, observed in the parent compound (x = 0), takes place for x = 0, 0.001, 0.005 and 0.01. For x = 0.025 only T-I and T-L are detected, while for x = 0.05 no transitions were observable. The values of T-I and T-L increase with x while T-LT decreases and disappears at the concentration x = 0.025. The effect of defects, besides modifying the transition temperatures, is that of broadening and lowering the heat capacity anomaly at the lock-in transition until its total quenching for x = 0.05. No observable hysteresis is detected in this transition. NQR and x-ray diffraction data show the Inc-C transition up to the highest concentration. We conclude that this phenomenology is caused by weak interaction of the incommensurate modulation with point defects even in the region close to the Inc-C transition.

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Держатели документа:
Russian Acad Sci, LV Kirensky Phys Inst, Siberian Branch, Krasnoyarsk 660036, Russia
Univ Zaragoza, CSIC, Inst Ciencia Mat Aragon, E-50009 Zaragoza, Spain
ИФ СО РАН
L V Kirenski Institute of Physics, Russian Academy of Sciences, Siberian Branch, 660036 Krasnoyarsk, Russian Federation
Inst. de Ciencia de Mat. de Aragon, CSIC-Universidad de Zaragoza, 50009 Zaragoza, Spain

Доп.точки доступа:
Aleksandrova, I. P.; Александрова, Инга Петровна; Bartolome, J.; Falvello, L. R.; Torres, J. M.; Sukhovskii, A. A.; Суховский, Андрей Андреевич
}
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Experimental and theoretical methods to study structural phase transition mechanisms in K3WO3F3 oxyfluoride / A. S. Krylov [et al.] // J. Solid State Chem. - 2014. - Vol. 218. - P. 32-37, DOI 10.1016/j.jssc.2014.05.028. - Cited References: 21. - The Authors are grateful to Prof. Zinenko V.I. for constructive discussion of the results. The work has been done with financial support of the Russian Foundation for Basic Research projects nos. 4828.2012.2, 12-02-31205; Federal Special Program "Scientific and scientific-pedagogical staff of innovative Russia" project no. 8379. . - ISSN 0022-4596. - ISSN 1095-726X

РУБ Chemistry, Inorganic & Nuclear + Chemistry, Physical
Рубрики:
LATTICE-DYNAMICS
   RAMAN-SCATTERING
   ELPASOLITE
   (NH4)3WO3F3
   SPECTROSCOPY
   CRYSTALS
Кл.слова (ненормированные):
Raman spectroscopy -- IR spectroscopy -- NMR spectroscopy -- High hydrostatic pressure -- Oxyfluorides -- Lattice dynamics calculations
Аннотация: The results of structural phase transitions mechanisms study in K3WO3F3oxyfluoride are represented by different experimental and theoretical methods. The structural phase transition anomalies at T1=452 K and T2=414 K of Raman and IR spectra have been analyzed. Using vibrational spectroscopy methods, the NMR-experiment has been done to clarify the nature of found phase transitions: displacive types or order-disorder types. The model of “disordered” crystal was proposed, and the results of lattice dynamics calculation in frameworks of the generalized Gordon–Kim method of ordered (R3) and “disordered” crystals were compared. The high pressure phases were studied by the Raman technique too.

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Держатели документа:
Russian Acad Sci, Siberian Branch, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
Russian Acad Sci, Siberian Branch, VS Sobolev Inst Geol & Mineral, Novosibirsk 630090, Russia

Доп.точки доступа:
Krylov, A. S.; Крылов, Александр Сергеевич; Sofronova, S. N.; Софронова, Светлана Николаевна; Kolesnikova, E. M.; Колесникова, Евгения Михайловна; Ivanov, Y. N.; Иванов, Юрий Николаевич; Sukhovsky, A. A.; Суховский, Андрей Андреевич; Goryainov, S. V.; Ivanenko, A. A.; Иваненко, Александр Анатольевич; Shestakov, N. P.; Шестаков, Николай Петрович; Kocharova, A. G.; Кочарова, Алла Георгиевна; Vtyurin, A. N.; Втюрин, Александр Николаевич; Russian Foundation for Basic Research [4828.2012.2, 12-02-31205]; Federal Special Program "Scientific and scientific-pedagogical staff of innovative Russia" [8379]
}
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10.

H-2 NMR investigation of the transition to the proton glass state in the CS5H3(SO4)(4)center dot 0.5H(2)O crystal / Y. N. Ivanov [et al.] // Phys. Solid State. - 2007. - Vol. 49, Is. 6. - P. 1142-1148, DOI 10.1134/S1063783407060200. - Cited References: 19 . - ISSN 1063-7834

РУБ Physics, Condensed Matter
Рубрики:
DIELECTRIC-RELAXATION
MAGNETIC-RESONANCE
PHASES
Аннотация: A crystal of the CS5H3(SO4)(4) (.) xH(2)O (x approximate to 0.5) (PCHS) compound, which belongs to the family of proton conductors with a complex system of hydrogen bonds, is investigated by H-2 NMR spectroscopy. The temperature and orientation dependences of the H-2 NMR spectra are measured and analyzed. It is established that, upon transition to the glassy phase at the temperature T-g = 260 K, the parameters characterizing the proton exchange between positions in hydrogen bonds remain unchanged to within the limits of experimental error. The protons in the two-dimensional network of hydrogen bonds in the (001) plane are dynamically disordered over possible positions down to temperatures considerably lower than the glass transition point T-g. However, water molecules are fixed at particular structural positions in the phase transition range. In PCHS crystals with a nonstoichiometric water content, this circumstance can be responsible for the frustration that leads to the formation of the glassy state.

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Держатели документа:
LV Kirenskii Inst Phys, Russian Acad Sci, Siberian Div, Krasnoyarsk 660036, Russia
Russian Acad Sci, Shubnikov Inst Crystallog, Moscow 119333, Russia
ИФ СО РАН
Kirensky Institute of Physics, Siberian Division, Russian Academy of Sciences, Akademgorodok, Krasnoyarsk 660036, Russian Federation
Shubnikov Institute of Crystallography, Russian Academy of Sciences, Leninskii pr. 59, Moscow 119333, Russian Federation

Доп.точки доступа:
Ivanov, Y. N.; Иванов, Юрий Николаевич; Aleksandrova, I. P.; Александрова, Инга Петровна; Sukhovsky, A. A.; Суховский, Андрей Андреевич; Baranov, A. I.
}
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11.

Incommensurate phase in the layered hexagonal crystal Cs3Bi2I9 / I. P. Aleksandrov [et al.] // Phys. Solid State. - 1997. - Vol. 39, Is. 6. - P. 991-994, DOI 10.1134/1.1130118. - Cited References: 12 . - ISSN 1063-7834

РУБ Physics, Condensed Matter

Аннотация: An incommensurate phase is observed in a Cs3Bi2I9 crystal, which belongs to the family of layered A(3)B(2)X(9) structures. Data from I-127 NQR and x-ray powder diffraction patterns show that the second-order normal phase-incommensurate phase transition at T-i = 220 K is accompanied by a P6(3)/mmc ↔ P2(1)/m symmetry change and takes place at the center of the Brillouin zone. The nature of the instability leading to the appearance of this little-studied form of incommensurability is discussed. (C) 1997 American Institute of Physics.

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Держатели документа:
L. V. Kirenskii Physics Institute, Siberian Branch, Russian Academy of Sciences, 660036 Krasnoyarsk, Russian Federation
ИФ СО РАН

Доп.точки доступа:
Aleksandrov, I. P.; Bovina, A. F.; Бовина, Ася Федоровна; Ageev, O. A.; Sukhovskii, A. A.; Суховский, Андрей Андреевич
}
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12.

Local and average structure of relaxor Na1/2Bi1/2TiO3 from the point of view of NMR / I. P. Aleksandrova, A. A. Sukhovsky [et al.] // Ferroelectrics. - 2009. - Vol. 378. - P. 16–22. - Библиогр.: 12

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Доп.точки доступа:
Aleksandrova, I. P.; Александрова, Инга Петровна; Sukhovsky, A. A.; Суховский, Андрей Андреевич; Ivanov, Yu. N.; Иванов, Юрий Николаевич; Yablonskaya, Yu.E.; Vakhrushev, S.B.
}
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13.

Local and Average Structure of Relaxor Na1/2Bi1/2TiO3 From the Point of View of NMR / Yablonskaya Yu.E., Aleksandrova I.P., Sukhovsky A.A., Ivanov Yu.N., Vakhrushev S.B. // 9th Russai/CIS/Baltic/Japan symposium on ferroelectricity : abstracts book : June 15-19, 2008, Vilnius, Lithuania. - p. 156

Доп.точки доступа:
Yablonskaya, Yu. E.; Aleksandrova, I. P.; Александрова, Инга Петровна; Sukhovsky, A. A.; Суховский, Андрей Андреевич; Ivanov, Yu. N.; Иванов, Юрий Николаевич; Vakhrushev, S. B.; Russia/CIS/Baltic/Japan Symposium on Ferroelectricity(9 ; 2008 ; May ; Vilnus, Lithuania)
}
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14.

Local structure of disordered PbSc1/2Nb1/2O3 in the region of the diffuse tetragonal phase-rhombohedral phase transition / I. P. Aleksandrova [et al.] // Phys. Solid State. - 2012. - Vol. 54, Is. 2. - P. 316-323, DOI 10.1134/S1063783412020047. - Cited References: 16. - This study was supported by the Council on Grants from the President of the Russian Federation for Support of the Leading Scientific Schools of the Russian Federation (grant no. NSh-4645.2010.2). . - ISSN 1063-7834

РУБ Physics + Condensed Matter
Рубрики:
Neutron-diffraction
   Order
   BaTiO3
   PbNiO3
   NMR
Аннотация: The local structure of the ferroelectric-relaxor PbSc1/2Nb1/2O3 in the temperature range from 550 to 220 K has been investigated using 45Sc nuclear magnetic resonance. It has been found that, in the paraelectric phase at temperatures below 550 K, the crystal consists of regions of an ordered elpasolite structure and inclusions of the disordered tetragonal perovskite phase with displacements along directions of the [001] type. The relative weight of the tetragonal structure in the region of the paraelectric phase is approximately equal to 0.28. Below the temperature of the phase transition from the disordered modification to the polar phase, the relative weight of the tetragonal phase decreases with decreasing temperature. The tetragonal structure is replaced by the trigonal polar structure. In a wide temperature range (∼50 K), there exists a heterophase structure that is characteristic of relaxors. Note that the correlation length of displacements in the tetragonal phase should be very small to explain the absence of indications of the existence of this phase in the diffraction data.

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Публикация на русском языке Локальная структура разупорядоченного PbSc[1/2]Nb[1/2]O[3] в области размытого перехода тетрагональная фаза - тригональная фаза [Текст] / И. П. Александрова [и др.] // Физ. тверд. тела : Физико-технический институт им. А.Ф.Иоффе РАН, 2012. - Т. 54 Вып. 2. - С. 298-304

Доп.точки доступа:
Aleksandrova, I. P.; Александрова, Инга Петровна; Sukhovsky, A. A.; Суховский, Андрей Андреевич; Ivanov, Y. N.; Иванов, Юрий Николаевич; Raevsky, I. P.; Раевский И.П.
}
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15.

Measurement of the anisotropy of weak indirect interaction between magnetic nuclei in cesium tgse / O. V. Falaleev [и др.] // Fiz. Tverd. Tela. - 1981. - Vol. 23, Is. 6. - P. 1853-1857. - Cited References: 12 . - ISSN 0367-3294

РУБ Physics, Condensed Matter

WOS
Доп.точки доступа:
Falaleev, O. V.; Фалалеев, Олег Владимирович; Kriger, A. I.; Sukhovskii, A. A.; Суховский, Андрей Андреевич; Moskvich, Yu. N.
}
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16.

Measurement of the maximum content of bound water in bentonitic clay using dielectric and NMR methods / V. L. Mironov [et al.] // Russ. Phys. J. - 2011. - Vol. 54, Is. 1. - P. 71-76. - Cited References: 4 . - ISSN 1064-8887

РУБ Physics, Multidisciplinary

Кл.слова (ненормированные):
dielectric permittivity -- nuclear magnetic resonance -- bentonitic clay -- bound water
Аннотация: An investigation of moisture dependences of refractive index and spectral width of the nuclear magnetic resonance (NMR) is performed for bentonitic clay specimens at different temperatures. These moisture dependences allowed identifying two types of moisture: bound and free water. The maximum content of water in the bentonitic clay is measured.

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Держатели документа:
[Mironov, V. L.
Sukhovskii, A. A.
Lukin, Yu. I.
Aleksandrova, I. P.] Russian Acad Sci, Siberian Branch, LV Kirenskii Inst Phys, Krasnoyarsk, Russia
ИФ СО РАН

Доп.точки доступа:
Mironov, V. L.; Миронов, Валерий Леонидович; Sukhovskii, A. A.; Суховский, Андрей Андреевич; Lukin, Y. I.; Лукин, Юрий Иванович; Aleksandrova, I. P.; Александрова, Инга Петровна
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17.

Mechanism of Protonic Conductivity in an NH(4)HSeO(4) Crystal / Y. N. Ivanov [et al.] // Phys. Solid State. - 2002. - Vol. 44, Is. 6. - P. 1077-1084, DOI 10.1134/1.1485011. - Cited References: 20. - This work was supported by the Russian Foundation for Basic Research, project no. 00-15-96790. . - ISSN 1063-7834

РУБ Physics, Condensed Matter

Аннотация: The chemical exchange of deuterons in a partly deuterated ammonium hydrogen selenate crystal is investigated by deuteron magnetic resonance ((2)H NMR) spectroscopy over a wide range of temperatures. The changes observed in the line shape of the NMR spectra at temperatures above 350 K are characteristic of chemical exchange processes. The exchange processes are thoroughly examined by two-dimensional (2)H NMR spectroscopy. It is established that, over the entire temperature range, only deuterons of hydrogen bonds are involved in the exchange and the rates of exchange between deuterons of all types are nearly identical. No deuteron exchange between the ND(4) groups and hydrogen bonds is found. A new model of proton transport in ammonium hydrogen selenate is proposed on the basis of the experimental data. This model makes it possible, within a unified context, to explain all the available experimental data, including macroscopic measurements of the electrical conductivity. (C) 2002 MAIK "Nauka/Interperiodica".

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Держатели документа:
[Ivanov, Yu. N.
Sukhovsky, A. A.
Aleksandrova, I. P.] Russian Acad Sci, LV Kirensky Phys Inst, Siberian Div, Krasnoyarsk 660036, Russia
[Totz, J.
Michel, D.] Univ Leipzig, D-04103 Leipzig, Germany
ИФ СО РАН
Kirensky Institute of Physics, Siberian Division, Russian Academy of Sciences, Akademgorodok, Krasnoyarsk 660036, Russian Federation

Доп.точки доступа:
Ivanov, Y. N.; Иванов, Юрий Николаевич; Sukhovsky, A. A.; Суховский, Андрей Андреевич; Aleksandrova, I. P.; Александрова, Инга Петровна; Totz, J.; Michel, D.; Russian Foundation for Basic Research [00-15-96790]
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18.

Micromechanism of proton conduction in a KHSeO4 crystal / Y. N. Ivanov [et al.] // Phys. Solid State. - 2006. - Vol. 48, Is. 9. - P. 1698-1702, DOI 10.1134/S1063783406090125. - Cited References: 11 . - ISSN 1063-7834

РУБ Physics, Condensed Matter
Рубрики:
EXCHANGE NMR
Аннотация: The proton exchange in a potassium hydrogen selenate crystal is investigated in detail. Partial deuteration of the crystal (approximately 80% of the protons are replaced by deuterons) makes it possible to use the method of nuclear magnetic resonance (NMR) on quadrupole nuclei to perform research into proton (deuteron) transport. In addition to conventional Fourier-transform NMR spectroscopy, elementary processes of deuteron chemical exchange are studied by two-dimensional NMR spectroscopy, which provides unique information regarding these processes. Slow exchange between protons of hydrogen bond chains and dimers consisting of two SeO4 groups is revealed. It is established that this process is responsible for the proton conduction in the potassium hydrogen selenate. The NMR data are compared with the results of dielectric measurements carried out at a frequency of 1 kHz.

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Держатели документа:
Russian Acad Sci, Kirensky Inst Phys, Krasnoyarsk 660036, Russia
Univ Leipzig, D-04103 Leipzig, Germany
ИФ СО РАН
Kirensky Institute of Physics, Siberian Division, Russian Academy of Sciences, Akademgorodok, Krasnoyarsk, 660036, Russian Federation
Leipzig University, Leipzig, D-04103, Germany

Доп.точки доступа:
Ivanov, Y. N.; Иванов, Юрий Николаевич; Sukhovsky, A. A.; Суховский, Андрей Андреевич; Aleksandrova, I. P.; Александрова, Инга Петровна; Michel, D.
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19.

Na-23 NMR in the relaxor ferroelectric Na1/2Bi1/2TiO3 / I. P. Aleksandrova [et al.] // Phys. Solid State. - 2006. - Vol. 48: 17th All-Russia Conference on the Physics of Ferroelectrics (VKS-XVII) (JUN 26-JUL 01, 2005, Penza, RUSSIA), Is. 6. - P. 1120-1123, DOI 10.1134/S106378340606031X. - Cited References: 8 . - ISSN 1063-7834

РУБ Physics, Condensed Matter
Рубрики:
NEUTRON-SCATTERING
PHASE-TRANSITION
NA0.5BI0.5TIO3
Аннотация: The Na-23 NMR spectra of a Na1/2Bi1/2TiO3 crystal are studied at frequencies of 79.4 and 15.7 MHz in the temperature range 150-720 K. It is revealed that, at all temperatures, the crystal contains regions with a nearly cubic matrix and polar clusters. The temperature dependence of the local distortion of the Na environment in the clusters is determined. The dynamics of the reorientation of the local cluster polarization in the tetragonal and trigonal NBT phases is analyzed.

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Держатели документа:
Russian Acad Sci, Kirensky Inst Phys, Siberian Div, Krasnoyarsk 660036, Russia
Russian Acad Sci, Ioffe Physicotech Inst, St Petersburg 194021, Russia
ИФ СО РАН
Kirensky Institute of Physics, Siberian Division, Russian Academy of Sciences, Krasnoyarsk, 660036, Russian Federation
Ioffe Physicotechnical Institute, Russian Academy of Sciences, Politekhnicheskaya ul. 26, St. Petersburg, 194021, Russian Federation

Доп.точки доступа:
Aleksandrova, I. P.; Александрова, Инга Петровна; Ivanov, Y. N.; Иванов, Юрий Николаевич; Sukhovskii, A. A.; Суховский, Андрей Андреевич; Vakhrushev, S. B.
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20.

Na-23 NMR study of the local order in the Na1/2Bi1/2TiO3 structure in a weak magnetic field / I. P. Aleksandrova [et al.] // Phys. Solid State. - 2008. - Vol. 50, Is. 3. - P. 496-501, DOI 10.1134/S1063783408030177. - Cited References: 14 . - ISSN 1063-7834

РУБ Physics, Condensed Matter
Рубрики:
PHASE-TRANSITIONS
PEROVSKITE
Аннотация: The orientation dependences of the second-order quadrupole shifts of the central component in the Na-23 NMR spectrum were studied in the temperature range 293-760 K. The profile of the spectral distribution is calculated using various models of the Na1/2Bi1/2TiO3 structure. The calculations agree with the experimental data for the monoclinic structure of a polar cluster with two Na displacement components: a displacement along the [111](P) direction and a small displacement statistically or dynamically disordered over six equally probable [100](P)-type directions. Tetragonal-phase nuclei and monoclinic clusters with a very small displacement component along the [111](P) direction are found to coexist and have close energies over the temperature range 580-610 K. The results obtained provide new information concerning the character of the diffuse phase transition at 610 K.

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Держатели документа:
[Aleksandrova, I. P.
Sukhovskii, A. A.
Ivanov, Yu. N.
Yablonskaya, Yu. E.] Russian Acad Sci, LV Kirensky Phys Inst, Siberian Branch, Krasnoyarsk 660036, Russia
[Vakhrushev, S. B.] Russian Acad Sci, AF Ioffe Physicotech Inst, St Petersburg 194021, Russia
ИФ СО РАН

Доп.точки доступа:
Aleksandrova, I. P.; Александрова, Инга Петровна; Sukhovskii, A. A.; Суховский, Андрей Андреевич; Ivanov, Y. N.; Иванов, Юрий Николаевич; Yablonskaya, Y. E.; Vakhrushev, S. B.
}
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