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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Churilov G. N., Popov A. A., Vnukova N. G., Dudnik A. I., Glushchenko G. A., Samoylova N. A., Dubinina I. A., Gulyaeva U. E.
Заглавие : A method and apparatus for high-throughput controlled synthesis of fullerenes and endohedral metal fullerenes
Место публикации : Tech. Phys. Lett.: MAIK Nauka-Interperiodica / Springer, 2016. - Vol. 42, Is. 5. - P.475-477. - ISSN 10637850 (ISSN), DOI 10.1134/S1063785016050072
Примечания : Cited References: 9. - This work was supported by a grant of the Ministry of Science and Education of the Russian Federation, ID RFMEFI61314X0010, project no. 14.613.21.0010.
Предметные рубрики: Metallofullerenes
Plasma
Аннотация: A method for synthesis of carbon nanostructures in a high-frequency arc discharge in the flow of helium (3–4 L/min) is presented. It is shown that the plasma-chemical synthesis of fullerenes and endohedral metal fullerenes (EMFs) can be controlled by changing helium pressure in the chamber. Temperature and electron concentration along the line normal to the discharge axis decrease upon moving away from the axis to the periphery; the larger the pressure, the sharper is the decrease in these parameters. The optimal helium pressure of 98 kPa was found in obtaining the Gd@C82 EMF which corresponds to the maximal EMF yield of 5 wt %. © 2016, Pleiades Publishing, Ltd.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Churilov G. N., Nikolaev N. S., Shichalin K. V., Lopatin V. A.
Заглавие : A Plasma Generator with Magnetic Vortex Stabilization and Possibilities of Its Use
Место публикации : Tech. Phys. Lett. - 2018. - Vol. 44, Is. 12. - P.1226-1229. - ISSN 1063-7850, DOI 10.1134/S106378501901005X. - ISSN 1090-6533(eISSN)
Примечания : Cited References: 8
Аннотация: A design of a plasma generator, the parameters of the resulting plasma, and the possibilities of its use for the synthesis of nanosized powders and optical emission spectroscopy are described. The device operation is based on the arc discharge of alternating current (66 kHz) in an argon jet between water-cooled metal electrodes. The discharge is stabilized by a flow of isolating gas (helium, nitrogen, air) and an axial magnetic field. The gas flow is fed tangentially to the discharge axis. The plasma between the electrodes has the shape of a cylinder remote from the chamber walls. The temperature and electron concentration in the cross section of the plasma cylinder vary along the radius and take the maximum and minimum values.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Petrakovskaya E. A., Bulina N. V., Churilov G. N., Puzyr' A. P.
Заглавие : A study of the synthesis products of fullerenes with nickel and cobalt
Место публикации : Tech. Phys.: AMER INST PHYSICS, 2001. - Vol. 46, Is. 1. - P42-46. - ISSN 1063-7842, DOI 10.1134/1.1340883
Примечания : Cited References: 15
Предметные рубрики: COMPLEXES
SPECTRA
Аннотация: Qualitative analysis of the products of plasmochemical synthesis of fullerenes with metallic nickel and cobalt has been carried out using electron paramagnetic resonance (EPR) and electron microscopy. These studies show that the synthesis products are mainly fullerenes, metallic nanoparticles coated with an insulating layer, and isolated atomic clusters. (C) 2001 MAIK "Nauka/Interperiodica".
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Fedorov A. S., Churilov G. N., Kuzubov A.A., Serjantova M.V.
Заглавие : Ab-initio investigation of hydrogen absorption by magnesium nanoparticles
Коллективы : "Carbon Nanomaterials in Clean-Energy Hydrogen Systems", national conference
Место публикации : Carbon Nanomaterials in Clean-Energy Hydrogen Systems: Proceedings of the NATO Advanced Research Workshop on Using Carbon Nanomaterials in Clean-Energy Hydrogen Systems Sudak, Crimea, Ukraine 22–28 September 2007/ red. Baranowski, B.; Zaginaichenko, S.; Schur, D.; Skorokhod, V.; Veziroglu, A.: Springer, 2008. - С. 603-610. - (SNATO Science for Peace and Security Series Subseries: NATO Science for Peace and Security Series C: Environmental Security). - ISBN 1874-6519, DOI 10.1007/978-1-4020-8898-8_75
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Bulina N. V., Bondarenko G. V., Marachevsky A.V., Chekanova L. A., Prokof'ev D. E., Churilov G. N., Gromyko A. I.
Заглавие : About iron globules formed at cooling of iron-contained plasma
Место публикации : Phys. Metals Metallogr. - New York: MAIK Nauka/Interperiodica/Springer, 2006. - Vol. 102. - С. S94-S95. - ISSN 0031-918X, DOI 10.1134/S0031918X06140249
Примечания : Cited Reference Count: 4
Аннотация: This paper is devoted to the investigation of iron globules that are formed during cooling of the iron-carbon-helium plasma and as a result of destruction of a natural ball lightning. Scanning electron microscopy, X-ray fluorescence, X-ray diffraction, and ferromagnetic resonance investigations were carried out. The magnetization values of the samplers were determined.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Kovel E. S., Sachkova A. S., Vnukova N. G., Churilov G. N., Knyazeva E. M., Kudryasheva N. S.
Заглавие : Antioxidant Activity and Toxicity of Fullerenols via Bioluminescence Signaling: Role of Oxygen Substituents
Место публикации : Int. J. Mol. Sci. - 2019. - Vol. 20, Is. 9. - Ст.2324. - ISSN 14220067 (ISSN) , DOI 10.3390/ijms20092324
Примечания : Cited References: 74. - This work was supported by PRAN-32, Program: 'Nanostructures: physics, chemistry, biology, technological basis'; RFBR 18-29-19003; RFBR-Krasnoyarsk Regional Foundation 18-44-240004, Tomsk Polytechnic University CE Program.
Аннотация: Fullerenols are nanosized water-soluble polyhydroxylated derivatives of fullerenes, a specific allotropic form of carbon, bioactive compounds, and perspective basis for drug development. Our paper analyzes the antioxidant activity and toxicity of a series of fullerenols with different number of oxygen substituents. Two groups of fullerenols were under investigation: (1) C60Oy(OH)(x), C60,70Oy(OH)(x), where x+y = 24-28 and (2) C60,70Oy(OH)(x), Fe0,5C60Oy(OH)(x), Gd@C82Oy(OH)(x), where x+y = 40-42. Bioluminescent cellular and enzymatic assays (luminous marine bacteria and their enzymatic reactions, respectively) were applied to monitor toxicity in the model fullerenol solutions and bioluminescence was applied as a signaling physiological parameter. The inhibiting concentrations of the fullerenols were determined, revealing the fullerenols' toxic effects. Antioxidant fullerenol' ability was studied in solutions of model oxidizer, 1,4-benzoquinone, and detoxification coefficients of general and oxidative types (D-GT and D-OxT) were calculated. All fullerenols produced toxic effect at high concentrations (0.01 g L-1), while their antioxidant activity was demonstrated at low and ultralow concentrations (0.001 g L-1). Quantitative toxic and antioxidant characteristics of the fullerenols (effective concentrations, concentration ranges, D-GT, and D-OxT) were found to depend on the number of oxygen substituents. Lower toxicity and higher antioxidant activity were determined in solutions of fullerenols with fewer oxygen substituents (x+y ⋍ 24-28). The differences in fullerenol properties were attributed to their catalytic activity due to reversible electron acceptance, radical trapping, and balance of reactive oxygen species in aqueous solutions. The results provide pharmaceutical sciences with a basis for selection of carbon nanoparticles with appropriate toxic and antioxidant characteristics. Based on the results, we recommend, to reduce the toxicity of prospective endohedral gadolinium-fullerenol preparations Gd@C82Oy(OH)(x), decreasing the number of oxygen groups to x+y ⋍ 24-28. The potential of bioluminescence methods to compare toxic and antioxidant characteristics of carbon nanostructures were demonstrated.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Bulina N. V., Lopatin V. A., Vnukova N. G., Osipova I. V., Churilov G. N., Krtschmer W.
Заглавие : Arc synthesis of silicon-doped heterofullerenes in plasma at atmospheric pressure
Место публикации : Fullerenes Nanotubes and Carbon Nanostructures: Marcel Dekker Inc., 2007. - Т. 15, № 5. - С. 395-400. - ISSN 1536-383X, DOI 10.1080/15363830701512229. - ISSN 1536-4046(eissn)
ГРНТИ : 31
РИНЦ
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Sachkova A. S., Kovel E. S., Churilov G. N., Stom D. I., Kudryasheva N. S.
Заглавие : Biological activity of carbonic nano-structures—comparison via enzymatic bioassay
Место публикации : J. Soils Sed. - 2019. - Vol. 19, Is. 6. - P.2689–2696. - ISSN 14390108 (ISSN) , DOI 10.1007/s11368-018-2134-9
Примечания : Cited References: 38. - This work was supported by the state budget allocated to the fundamental research at the Russian Academy of Sciences, project 0356-2017-0017; PRAN-32, Program: “Nanostructures: physics, chemistry, biology, technological basis.” Study of ROS involvement to antioxidant activity of humic substances was supported by the Russian Science Foundation, grant 16-14-10115.
Аннотация: Purpose: The aim of the work is to compare the biological activity of carbonic nano-structures of natural and artificial origination, namely, humic substances (HS) and fullerenols. Materials and methods: The representative of the fullerenol group, С60Оy(OH)x where у + x = 20–22, was chosen. Enzyme-based luminescent bioassay was applied to evaluate toxicity and antioxidant properties of HS and fullerenol (F); chemiluminescent luminol method was used to study a content of reactive oxygen species (ROS) in the solutions. Toxicity of the bioactive compounds was evaluated using effective concentrations ЕС50; detoxification coefficients DOxT were applied to study and compare antioxidant activity of the compounds. Antioxidant activity and ranges of active concentrations of the bioactive compounds were determined in model solutions of organic and inorganic oxidizers—1,4-benzoquinone and potassium ferricianide. Results and discussion: Values of ЕС50 revealed higher toxicity of HS than F (0.005 and 0.108 g L−1, respectively); detoxifying concentrations of F were found to be lower. Antioxidant ability of HS was demonstrated to be time-dependent; the 50-min preliminary incubation in oxidizer solutions was suggested as optimal for the detoxification procedure. On the contrary, F’ antioxidant effect demonstrated independency on time. Antioxidant effect of HS did not depend on amphiphilic characteristics of the media (values of DOxT were 1.3 in the solutions of organic and inorganic oxidizers), while this of F was found to depend: it was maximal (DOxT = 2.0) in solutions of organic oxidizer, 1,4-benzoquinone. Conclusions: Both HS and F demonstrated toxicity and low-concentration antioxidant ability; however, quantitative characteristics of their effects were different. The differences were explained with HS polyfunctionality, higher ability to decrease ROS content, non-rigidity, and diffusion restrictions in their solutions. Antioxidant effect of the bioactive compounds was presumably attributed to catalytic redox activity of their π-fragments. The paper demonstrates a high potential of luminescent enzymatic bioassay to study biological activity of nano-structures of natural and artificial origination.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Sushko E. S., Sachkova A. S., Внукова, Наталья Григорьевна, Чурилов, Григорий Николаевич, Stepin E. A., Kicheeva A. G., Kudryasheva N. S.
Заглавие : Biological activity of fullerenols of various structure. The role of reactive oxygen species. Bioluminescent monitoring
Коллективы : Congress of Biophysicists of Russia
Место публикации : Biophysical reviews: 7th Congress of Biophysicists of Russia : conference proceedings. - 2023. - Vol. 15, Is. 5. - Ст.S7.437. - P.1663. - DOI 10.1007/s12551-023-01150-w
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Kudryasheva, Nadezhda S., Kovel, Ekaterina S., Sachkova, Anna S., Vorobeva, Anna A., Isakova V. G., Churilov G. N.
Заглавие : Bioluminescent enzymatic assay as a tool for studying antioxidant activity and toxicity of bioactive compounds
Коллективы : Russian Foundation for Basic Research [15-03-06786, 15-43-04377-sibir]; Russian Academy of Sciences [01201351504]
Место публикации : Photochem. Photobiol.: Wiley, 2017. - Vol. 93, Is. 2. - P.536-540. - ISSN 0031-8655, DOI 10.1111/php.12639. - ISSN 1751-1097(eISSN)
Примечания : Cited References:40. - The work was supported by the Russian Foundation for Basic Research, Grants 15-03-06786 and 15-43-04377-sibir; the state budget allocated to the fundamental research at the Russian Academy of Sciences (project 01201351504).
Предметные рубрики: LUMINOUS MARINE-BACTERIA
HUMIC SUBSTANCES
DETOXIFICATION PROCESSES
Аннотация: A bioluminescent assay based on a system of coupled enzymatic reactions catalyzed by bacterial luciferase and NADH:FMN-oxidoreductase was developed to monitor toxicity and antioxidant activity of bioactive compounds. The assay enables studying toxic effects at the level of biomolecules and physicochemical processes, as well as determining the toxicity of general and oxidative types. Toxic and detoxifying effects of bioactive compounds were studied. Fullerenols, perspective pharmaceutical agents, nanosized particles, water-soluble polyhydroxylated fullerene-60 derivatives were chosen as bioactive compounds. Two homologous fullerenols with different number and type of substituents, C60O2–4(OH)20–24 and Fe0.5C60(OH) xOy (x + y = 40–42), were used. They suppressed bioluminescent intensity at concentrations 0.01 g L−1 and 0.001 g L−1 for C60O2–4(OH)20-24 and Fe0.5C60(OH)xOy, respectively; hence, a lower toxicity of C60O2–4(OH)20–24 was demonstrated. Antioxidant activity of fullerenols was studied in model solutions of organic and inorganic oxidizers; changes in toxicities of general and oxidative type were determined; detoxification coefficients were calculated. Fullerenol C60O2–4(OH)20–24 revealed higher antioxidant ability at concentrations 10−17−10−5 g L−1. The difference in the toxicity and antioxidant activity of fullerenols was explained through their electron donor/acceptor properties and different catalytic activity. Principles of bioluminescent enzyme assay application for evaluating the toxic effect and antioxidant activity of bioactive compounds were summarized and the procedure steps were described.
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11.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Vnukova N. G., Dudnik A. I., Komogortsev S. V., Velikanov D. A., Nemtsev I. V., Volochaev M., Osipova I. V., Churilov G. N.
Заглавие : Carbon coated nickel nanoparticles produced in high-frequency arc plasma at ambient pressure
Коллективы : Euro-Asian Symposium "Trends in MAGnetism", "Trends in MAGnetism", Euro-Asian Symposium, Институт физики им. Л.В. Киренского Сибирского отделения РАН
Место публикации : J. Magn. Magn. Mater.: Elsevier Science, 2017. - Vol. 440: EURO-Asian Symposium on Trends in Magnetism (EASTMAG) (AUG 15-19, 2016, Siberian Fed Univ, Krasnoyarsk, RUSSIA). - P.164-166. - ISSN 0304-8853, DOI 10.1016/j.jmmm.2016.12.142. - ISSN 1873-4766(eISSN)
Примечания : Cited References:10. - The work was supported by Ministry of Education and Science of Russia (Russian-Japanese joined project, Agreement No 14.613.21.0010, ID RFMEFI61314X0010).
Предметные рубрики: FULLERENES
NI3C
Ключевые слова (''Своб.индексиров.''): nanoparticles--carbon--nickel
Аннотация: The nickel particles with the mean size about 10-20 nm coated with carbon were extracted by the treatment of the carbon condensate with nitric and hydrochloric acids. The initial carbon condensate containing nickel nanoparticles with a graphite conversion was synthesized in the high-frequency carbon-helium arc plasma at ambient pressure with the nickel nanoparticles as a catalyst. The nickel content in the nanoparticles was 84.6 wt %. Magnetic properties of the nanoparticles are characterized by the high hysteresis and thermal stability. The sample of compacted nanoparticles is characterized by electrical resistance much higher than it in of compacted initial condensate.
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12.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Churilov G. N., Fedorov A. S., Novikov P. V.
Заглавие : Fullerene C-60 formation in partially ionized carbon vapor
Разночтения заглавия :авие SCOPUS: Fullerene C60 formation in partially ionized carbon vapor
Место публикации : JETP Letters. - 2002. - Vol. 76, Is. 8. - P.522-526. - ISSN 0021-3640, DOI 10.1134/1.1533779
Примечания : Cited References: 15
Предметные рубрики: TOTAL-ENERGY CALCULATIONS
WAVE BASIS-SET
CLUSTERS
GROWTH
Аннотация: The assembling rate of a fullerene C-60 molecule has been theoretically studied as a function of electron concentration and temperature in partially ionized carbon vapor. For C-60 formation via one or two intermediate stages of cluster collisions, it has been shown that there is a region of plasma parameters (the temperature and electron concentration) in which fullerene C-60 is formed more efficiently. The C-60 formation rate versus temperature and electron concentration relationships have been found to correlate with the trends in the collision cross-section of carbon clusters as functions of these parameters. (C) 2002 MAIK "Nauka/Interperiodica".
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13.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Churilov G. N.
Заглавие : Synthesis of fullerenes and other nanomaterials in arc discharge
Место публикации : Fullerenes Nanotubes and Carbon Nanostructures: Marcel Dekker Inc., 2008. - Т. 16, № 5-6. - С. 395-403. - ISSN 1536-383X, DOI 10.1080/15363830802281641. - ISSN 1536-4046(eissn)
ГРНТИ : 31
РИНЦ
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14.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Churilov G. N.
Заглавие : Two new discharges for production of fullerenes and nanotubes
Коллективы : International Winterschool on Electronic Properties of Novel Materials
Место публикации : Progress in fullerene research/ ed. H. Kuzmany [et al.]. - Singapore ; New Jersey ; London: World Scientific, 1994. - P.135-138. - ISBN 978-9810218874 (Шифр -292987024). - ISBN 981-02-1887-7
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15.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Dudnik A. I., Osipova I. V., Nikolaev N. S., Churilov G. N.
Заглавие : Comparative analysis of two methods for synthesis of fullerenes at different helium pressures
Коллективы : RFBRRussian Foundation for Basic Research (RFBR) [18-32-20011]
Место публикации : Fuller. Nanotub. Carbon Nanostruct. - 2020. - Vol. 28, Is. 9. - P.697-701. - ISSN 1536-383X, DOI 10.1080/1536383X.2020.1746281. - ISSN 1536-4046(eISSN)
Примечания : Cited References: 16. - The reported study was funded by RFBR according to the research project No 18-32-20011
Предметные рубрики: PLASMA
YIELD
DISCHARGE
PARAMETERS
DEPENDENCE
C60
Аннотация: The results of the effect of helium pressure in the chamber on the amount and composition of the produced fullerenes (C60, C70, etc.) synthesized in the arc plasma with graphite electrodes are presented. The findings obtained when the arc is powered by a direct (DC) and alternating (AC) currents of low frequency were compared in the same chamber with the electrodes located at the same angle to each other. These two methods are drastically different. The complete conversion of graphite into fullerene soot in AC occurs, but a part of the graphite is converted into a cathode deposit that does not contain fullerenes in DC, the relative amount of which increases when decreasing the helium pressure in the chamber. The highest fullerene content in fullerene soot of 10.2 wt.% is produced at a pressure of 127.5 kPa in AC arc, but in DC arc, the highest content of fullerenes in fullerene soot of 8.3 wt.% is produced at a pressure of 33.3 kPa.
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16.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Внукова, Наталья Григорьевна, Лопатин, Владислав Александрович, Осипова, Ирина Владимировна, Чурилов, Григорий Николаевич
Заглавие : Comparative characteristics of alternating current light source with copper and silver electrodes under power samples analysis
Коллективы : "Современный атомно-эмиссионный анализ и науки о земле", семинар, Российская академия наук, Сибирское отделение РАН, Иркутский научынй центр СО РАН, Институт геохимии им. А. П. Виноградова СО РАН
Место публикации : Современный атомно-эмиссионный анализ и науки о земле: программа и тезисы докл. науч. семинара с междунар. участием, посвящ. 150-летию создания Кирхгофом и Бунзеном основ атом. спектроскопии, 30 июня - 4 июля 2009 г., г. Иркутск/ [отв. ред.: Е. В. Шабанова, О. В. Зарубина]. - 2009. - С. 17-18. - ISBN 978-5-94797-139-2
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17.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Churilov G. N., Dudnik A. I., Vnukova N. G., Dubinina I. A.
Заглавие : Comparative characteristics of metallofullerenes, clusterfullerenes with carbide and nitride synthesized under high and low pressure
Коллективы : "Advanced carbon nanostructures", International conference
Место публикации : International Conference Advanced Carbon Nanostructures: abstracts of invited lectures & contributed papers. - 2015. - Ст.P1-03. - P.62
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18.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Vnukova N. G., Churilov G. N., Popov Yu. M., Glushenko G. A.
Заглавие : Comparative characteristics of Sc2C2@C82 and C84 polymerization under high pressure
Коллективы : "Advanced carbon nanostructures", International conference, Физико-технический институт им. А.Ф. Иоффе РАН, Национальный исследовательский центр "Курчатовский институт", Санкт-Петербургский государственный технологический институт (технический университет), Санкт-Петербургский национальный исследовательский Академический университет имени Ж.И. Алфёрова Российской академии наук
Место публикации : 15th International Conference "Advanced carbon nanostructures": book of abstracts. - 2021. - Fullerenes. - Ст.O4-4-10. - P.195. - ISBN 978-5-93634-069-7
Примечания : Cited References: 3. - The reported study was funded by RFBR according to the research project № 18-29-190080
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19.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Dubinina I. A., Dudnik A. I., Vnukova N. G., Churilov G. N.
Заглавие : Comparative study of antioxidant activity of fullerenols including higher and endohedral fullerenols by inhibition of adrenaline autoxidation
Коллективы : "Advanced carbon nanostructures", International conference
Место публикации : International Conference Advanced Carbon Nanostructures: abstracts of invited lectures & contributed papers. - 2015. - P.63
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20.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Churilov G. N., Osipova I. V., Maslennikov A. N., Glushchenko G. A., Drokin N. A.
Заглавие : Composites based on superhigh-molecular poly(ethylene) and carbon nanostructures
Коллективы : "Advanced Carbon Nanostructures", Joint International Conference, Красноярский государственный педагогический университет им. В.П. Астафьева
Место публикации : Joint International Conference "Advanced Carbon Nanostructures" (ACN 2011): Abstracts. - 2011. - Ст.P6.08. - С. 324
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