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A Challenge toward novel quaternary sulfides SrLnCuS3 (Ln = La, Nd, Tm): Unraveling synthetic pathways, structures and properties / A. V. Ruseikina, M. V. Grigoriev, L. A. Solovyov [et al.] // Int. J. Mol. Sci. - 2022. - Vol. 23, Is. 20. - Ст. 12438, DOI 10.3390/ijms232012438. - Cited References: 62. - The research was funded by the Tyumen Oblast Government, as part of the West-Siberian Interregional Science and Education Center’s project No. 89-DON (3). This work was supported by state assignment of the Ministry of Science and Higher Education of the Russian Federation (Project Reg. No. 720000Φ.99.1.Б385AA13000) . - ISSN 1422-0067
Кл.слова (ненормированные):
inorganic materials -- quaternary sulfide -- synthesis -- crystal structure -- ab initio calculations -- magnetic measurements -- spectroscopy
Аннотация: We report on the novel heterometallic quaternary sulfides SrLnCuS3 (Ln = La, Nd, Tm), obtained as both single crystals and powdered samples. The structures of both the single crystal and powdered samples of SrLaCuS3 and SrNdCuS3 belong to the orthorhombic space group Pnma but are of different structural types, while both samples of SrTmCuS3 crystallize in the orthorhombic space group Cmcm with the structural type KZrCuS3. Three-dimensional crystal structures of SrLaCuS3 and SrNdCuS3 are formed from the (Sr/Ln)S7 capped trigonal prisms and CuS4 tetrahedra. In SrLaCuS3, alternating 2D layers are stacked, while the main backbone of the structure of SrNdCuS3 is a polymeric 3D framework [(Sr/Ln)S7]n, strengthened by 1D polymeric chains (CuS4)n with 1D channels, filled by the other Sr2+/Ln3+ cations, which, in turn, form 1D dimeric ribbons. A 3D crystal structure of SrTmCuS3 is constructed from the SrS6 trigonal prisms, TmS6 octahedra and CuS4 tetrahedra. The latter two polyhedra are packed together into 2D layers, which are separated by 1D chains (SrS6)n and 1D free channels. In both crystal structures of SrLaCuS3 obtained in this work, the crystallographic positions of strontium and lanthanum were partially mixed, while only in the structure of SrNdCuS3, solved from the powder X-ray diffraction data, were the crystallographic positions of strontium and neodymium partially mixed. Band gaps of SrLnCuS3 (Ln = La, Nd, Tm) were found to be 1.86, 1.94 and 2.57 eV, respectively. Both SrNdCuS3 and SrTmCuS3 were found to be paramagnetic at 20-300 K, with the experimental magnetic characteristics being in good agreement with the corresponding calculated parameters.

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Держатели документа:
Laboratory of Theory and Optimization of Chemical and Technological Processes, University of Tyumen, Tyumen, 625003, Russian Federation
Federal Research Center KSC SB RAS, Institute of Chemistry and Chemical Technology, Krasnoyarsk, 660036, Russian Federation
Institute of Natural Sciences and Mathematics, Ural Federal University named after the First President of Russia B.N. Yeltsin, Mira Str. 19, Russian Federation
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
Department of Photonics and Laser Technology, Siberian Federal University, Krasnoyarsk, 660079, Russian Federation
Institute of Physics and Technology, University of Tyumen, Volodarskogo Str. 6, Tyumen, 625003, Russian Federation
Institute of Inorganic Chemistry, University of Stuttgart, Stuttgart, D-70569, Germany
Scientific and Educational and Innovation Center for Chemical and Pharmaceutical Technologies, Ural Federal University named after the First President of Russia B.N. Yeltsin, Mira Str. 19, Russian Federation
«Advanced Materials for Industry and Biomedicine» Laboratory, Kurgan State University, Sovetskaya Str. 63/4, Kurgan, 640020, Russian Federation
University of Tyumen, Volodarskogo Str. 6, Tyumen, 625003, Russian Federation

Доп.точки доступа:
Ruseikina, A. V.; Grigoriev, M. V.; Solovyov, L. A.; Chernyshev, V. A.; Aleksandrovsky, A. S.; Александровский, Александр Сергеевич; Krylov, A. S.; Крылов, Александр Сергеевич; Krylova, S. N.; Крылова, Светлана Николаевна; Shestakov, N. P.; Шестаков, Николай Петрович; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Garmonov, A. A.; Matigorov, A. V.; Eberle, M. A.; Schleid, T.; Safin, D. A.
}
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A Raman scattering study of the phase transition in the ammonium oxyfluoride (NH4)(3)TiOF5 / Y. V. Gerasimova [et al.] // Phys. Solid State. - 2008. - Vol. 50, Is. 8. - P. 1534-1537, DOI 10.1134/S1063783408080246. - Cited References: 8 . - ISSN 1063-7834

РУБ Physics, Condensed Matter
Рубрики:
(NH4)(3)WO3F3 OXYFLUORIDE
Аннотация: Raman spectra of a polycrystalline sample of the perovskite-like oxyfluoride (NH4)(3)TiOF5 are measured in the frequency region 100-3600 cm(-1) at temperatures ranging from 91 to 370 K under hydrostatic pressures of up to 9 GPa, which include the range of the phase transition from the orientationally disordered cubic phase to the low-symmetry phase. Anomalies in the spectral parameters due to the phase transition are revealed in the range of vibrations of TiOF5 octahedral groups.

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Держатели документа:
[Gerasimova, Yu. V.
Krylov, A. S.
Vtyurin, A. N.] Russian Acad Sci, LV Kirensky Phys Inst, Siberian Branch, Krasnoyarsk 660036, Russia
[Gerasimova, Yu. V.
Krylov, A. S.
Vtyurin, A. N.] Siberian Fed Univ, Krasnoyarsk 660041, Russia
[Laptash, N. M.] Russian Acad Sci, Inst Chem, Far E Branch, Vladivostok 690022, Russia
[Goryainov, S. V.] Inst Mineral & Petrog, Siberian Branch, Novosibirsk 630090, Russia
ИФ СО РАН
Kirensky Institute of Physics, Siberian Branch, Russian Academy of Sciences, Akademgorodok 50, Krasnoyarsk 660036, Russian Federation
Siberian Federal University, Svobodnyi pr. 79, Krasnoyarsk 660041, Russian Federation
Institute of Chemistry, Far-East Branch, Russian Academy of Sciences, pr. Stoletiya Vladivostoka 159, Vladivostok 690022, Russian Federation
Institute of Mineralogy and Petrography, Siberian Branch, Universitetskii pr. 3, Novosibirsk 630090, Russian Federation

Доп.точки доступа:
Gerasimova, Y. V.; Герасимова, Юлия Валентиновна; Krylov, A. S.; Крылов, Александр Сергеевич; Vtyurin, A. N.; Втюрин, Александр Николаевич; Laptash, N. M.; Goryainov, S. V.
}
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A raman study of hydrostatic pressure induced phase transitions in Rb2KInF6 crystals / A. N. Vtyurin [et al.] // Phys. Solid State. - 2012. - Vol. 54, Is. 5. - P. 934-936, DOI 10.1134/S1063783412050472. - Cited References: 16. - This study was supported by the Russian Foundation for Basic Research (project nos. 11-02-98002-r_sibir' and 09-02-00062), the Siberian Branch of the Russian Academy of Sciences (integration project no. 101), and the Council on Grants from the President of the Russian Federation (grant no. HSh-4645.2010.2). . - ISSN 1063-7834

РУБ Physics, Condensed Matter
Рубрики:
LATTICE-DYNAMICS
ELPASOLITES
SPECTRA
Аннотация: The Raman spectra of the elpasolite (Rb2KInF6) crystal have been studied in the pressure range from 0 to 5.3 GPa at a temperature of 295 K. A phase transition at a pressure of approximately 0.9 GPa has been found. An analysis of the variations in the spectral parameters has led to the conclusion that the phase transition to a distorted phase is accompanied by the doubling of the volume of the primitive cell of the initial cubic phase. Numerical calculations of the lattice dynamics in the Rb2KInF6 crystal have been performed. The numerical simulation has established that the phase transition at a pressure of 0.9 GPa is associated with condensation of the F (lg) mode. A probable high-pressure phase is the phase with space group C2/m.

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Публикация на русском языке Исследование фазовых переходов в кристалле Rb2KInF6, индуцированных гидростатическим давлением, методом комбинационного рассеяния света // Физика твердого тела : Физико-технический институт им. А.Ф.Иоффе РАН, 2012. - Т. 54, Вып. 5. - С. 880-882. - ISSN 0367-3294

Держатели документа:
[Vtyurin, A. N.
Krylov, A. S.
Krylova, S. N.
Oreshonkov, A. S.
Voronov, V. N.] Russian Acad Sci, Siberian Branch, LV Kirensky Phys Inst, Krasnoyarsk 660036, Russia
[Goryainov, S. V.] Russian Acad Sci, Siberian Branch, Inst Mineral & Petrog, Novosibirsk 630090, Russia

Доп.точки доступа:
Vtyurin, A. N.; Втюрин, Александр Николаевич; Krylov, A. S.; Крылов, Александр Сергеевич; Goryainov, S. V.; Горяйнов, Сергей Владимирович; Krylova, S. N.; Крылова, Светлана Николаевна; Oreshonkov, A. S.; Орешонков, Александр Сергеевич; Voronov, V. N.; Воронов, Владимир Николаевич
}
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A study of phase transition in (NH4)(3)WO3F3 oxyfluoride by Raman scattering / A. S. Krylov [et al.] // Phys. Status Solidi B. - 2006. - Vol. 243, Is. 2. - P. 435-441, DOI 10.1002/pssb.200541259. - Cited References: 11 . - ISSN 0370-1972

РУБ Physics, Condensed Matter
Рубрики:
ELPASOLITE RB2KSCF6
Аннотация: Raman scattering spectra of perovskite-like (NH4)(3)WO3F3 oxyfluoride are studied in the 70-3600 cm(-1) frequency range and the 93-323 K temperature range including the transition point from orientationally disordered cubic phase into the lower symmetry one. Internal vibrations of ammonium ions and WO3F3 octahedra have been found to exhibit transition anomalies. Analysis of measurements suggests that the transition under study is due mainly to the ordering of octahedra.

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Держатели документа:
Kirensky Inst Phys, Krasnoyarsk 660036, Russia
Inst Chem, Vladivostok 690022, Russia
ИФ СО РАН
Kirensky Institute of Physics, 660036 Krasnoyarsk, Russian Federation
Institute of Chemistry, 690022 Vladivostok, Russian Federation

Доп.точки доступа:
Krylov, A. S.; Крылов, Александр Сергеевич; Gerasimova, J. V.; Герасимова, Юлия Валентиновна; Vtyurin, A. N.; Втюрин, Александр Николаевич; Fokina, V. D.; Фокина, Валентина Дмитриевна; Laptash, N. M.; Voyt, E. I.
}
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Analyzing the symmetry of the Raman spectra of crystals according to angular dependences / E. V. Golovkina, S. N. Krylova, A. N. Vtyurin, A. S. Krylov // Bull. Russ. Acad. Sci. Phys. - 2024. - Vol. 88, Is. 5. - P. 773-778, DOI 10.1134/S1062873824706573. - Cited References: 32. - This work was supported by the Russian Foundation for Basic Research, project no. 21-52-12018. The authors are grateful to Dr. Irena Senkovska for providing our DUT-8(Ni) samples . - ISSN 1062-8738. - ISSN 1934-9432
Кл.слова (ненормированные):
angular dependences of Raman scattering -- metal–organic framework crystals
Аннотация: The authors propose a way of reconstructing the Raman tensor by studying the angular dependences of the intensities of the Raman lines of unoriented microcrystals. The technique is verified using familiar calomel Hg2Cl2 crystals. It is shown that the lines on DUT-8 (Ni) crystals indicating phases with open and closed pores have different types of symmetries. The technique can be used to reconstruct the Raman tensor for any unoriented crystalline sample.

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Держатели документа:
Kirensky Institute of Physics, Krasnoyarsk Scientific Center, Siberian Branch, Russian Academy of Sciences, 660036, Krasnoyarsk, Russia
Siberian Federal University, 660041, Krasnoyarsk, Russia

Доп.точки доступа:
Golovkina, E. V.; Головкина, Елена Вячеславовна; Krylova, S. N.; Крылова, Светлана Николаевна; Vtyurin, A. N.; Втюрин, Александр Николаевич; Krylov, A. S.; Крылов, Александр Сергеевич
}
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Anharmonicity and local noncentrosymmetric regions in BaTiO3 pressed powder studied by the Raman line temperature dependence / A. M. Pugachev, I. V. Zaytseva, N. V. Surovtsev, A. S. Krylov // Ceram. Int. - 2020. - Vol. 46, Is. 14. - P. 22619-22623, DOI 10.1016/j.ceramint.2020.06.024. - Cited References: 26. - The reported study was funded by RFBR , according to the research project No. 18-02-00399 and 19-42-543-016 , Government of Novosibirsk region No. 19-42-543-016 and State assignment No AAAA-A17-117052410033-9. The experiments were performed in the multiple-access center “High-Resolution Spectroscopy of Gases and Condensed Matter” in IA&E SB RAS (Novosibirsk, Russia) and Center for Common Use of the Krasnoyarsk Scientific Center, SB RAS (Krasnoyarsk, Russia) . - ISSN 0272-8842
Кл.слова (ненормированные):
BaTiO3 -- Non-hydrostatic pressure -- Raman scattering -- Anharmonicity -- Noncentrosymmetric regions
Аннотация: The temperature dependencies of position, width, and integral amplitude the E(TO) line near 307 cm−1 in Raman spectra in barium titanate powders with different non-hydrostatic pressure and temperature treatment were studied. It was found that parameters of the E(TO) line near 307 cm−1 are different in the crystal, the untreated powder, the powder treated by the non-hydrostatic pressure, and the powder annealed after the pressure treatment. The line width (FWHM) increase with temperature according to Klemens model. It indicates that the origin of the line broadening is the anharmonicity of the E(TO) phonons. The pressure treatment changes the anharmonicity of the phonon potential. It was found that the temperature dependence of the integral intensity of the E(TO) line is similar to that of the second optical harmonic signal and reflects the presence of the local polar regions. Thus, the E(TO) line in the Raman spectrum allows one to characterize the average polarity of local regions and their anharmonicity depending on non-hydrostatic pressures and thermal treatment.

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Держатели документа:
Institute of Automation and Electrometry SB RAS, Novosibirsk, 630090, Russian Federation
Kirensky Institute of Physics Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation

Доп.точки доступа:
Pugachev, A. M.; Zaytseva, I. V.; Surovtsev, N. V.; Krylov, A. S.; Крылов, Александр Сергеевич
}
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    Anisotropic crystal of the δ-BiB3O6 investigated by vibrational spectroscopy / E. A. Strikina [et al.] // IOP Conf. Ser.: Mater. Sci. Eng. - 2016. - Vol. 155, Is. 1. - Ст. 012029, DOI 10.1088/1757-899X/155/1/012029. - Cited References: 8. - This study was partially supported by the Ministry of Education and Science of the Russian Federation, the “Krasnoyarsky regional fund of scientific support and scientific-technical activity” and the Russian Foundation for Basic Research Grant “15-42-04347 r_siberia_a".
   Перевод заглавия: Исследование анизотропного кристалла δ-BiB3O6 методом колебательной спектроскопии
Аннотация: The vibrational spectroscopy has been applied to investigate the structure the BiB3O6 (BIBO) crystal. Based on the experimental results, the total set of phonons mode of the polarized Raman spectra was proposed. To verify the obtained experimental data have been performed theoretical calculation in software package LADY.

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Доп.точки доступа:
Strikina, E. A.; Стрикина, Екатерина Андреевна; Krylov, A. S.; Крылов, Александр Сергеевич; Oreshonkov, A. S.; Орешонков, Александр Сергеевич; Vtyurin, A. N.; Втюрин, Александр Николаевич; Maximova, O. A.; International Scientific and Research Conference "Topical Issues in Aeronautics and Astronautics"(XII ; Krasnoyarsk)(11-15 April 2016)
}
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Anomalous Raman phenomenon of CuCrS2 / G. M. Abramova, G. A. Petrakovskii, A. N. Vtyurin [et al.] // J. of Ra man Spectroscopy. - 2010. - Vol. 41, Is. 12. - P1485-1488

Доп.точки доступа:
Abramova, G. M.; Абрамова, Галина Михайловна; Petrakovskii, G. A.; Петраковский, Герман Антонович; Vtyurin, A. N.; Втюрин, Александр Николаевич; Rasch, J.; Krylov, A. S.; Крылов, Александр Сергеевич; Gerasimova, Yu. V.; Герасимова, Юлия Валентиновна; Velikanov, D. A.; Великанов, Дмитрий Анатольевич; Boehm, M.; Sokolov, V.
}
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Application of DUT-4 MOF structure switching for optical and electrical humidity sensing / A. S. Krylov, S. A. Shipilovskikh, S. N. Krylova [et al.] // Dalton Trans. - 2024. - Vol. 53, Is. 8. - P. 3459-3464, DOI 10.1039/D4DT00038B. - Cited References: 37. - The authors acknowledge the support by the state assignment of the Kirensky Institute of Physics FRC KSC SB RAS, also this work was financially supported by the RFBR (Russian Foundation for Basic Research), project no. 21-52-12018. S. A. S. acknowledges the financial support by the Russian Science Foundation (chemical part, Grant No. 22-73-10069 "Design and application of flexible metal organic frameworks for photonics devices"). V.A.M. acknowledges the Priority 2030 Federal Academic Leadership Program Ivan Sergeev (student in ITMO Univ.) for supporting in IV curve analysis. Raman, FTIR and SEM experiments were performed in the Center for Common Use of the Krasnoyarsk Scientific Center SB RAS (Krasnoyarsk, Russia) . - ISSN 1477-9226. - ISSN 1477-9234
Аннотация: The threshold structural transformation of the DUT-4 metal–organic framework (MOF) from an ordered to distorted phase during exposure to ambient conditions has been revealed. The in situ X-ray diffraction analysis, in situ Raman and FTIR spectroscopy, scanning electron microscopy and synchronous thermal analysis have been used for investigation. The reversible effect of exposure time and humidity on such a phase transition has been confirmed. We also demonstrated that the observed phase transition correlated well with changes in the optical and electronic properties of DUT-4, paving the way to a new family of MOF-based phase change materials for optoelectronic applications.

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Держатели документа:
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, Russia
ITMO University, St. Petersburg, Russia
Siberian Federal University, Krasnoyarsk, Russia
South Ural State University, Chelyabinsk, Russia
Federal Research Center “Krasnoyarsk Science Center of the Siberian Branch of the Russian Academy of Sciences”, Akademgorodok 50, 660036 Krasnoyarsk, Russia
Institut Jean Lamour, Universite de Lorraine, UMR CNRS 7198, 54011 Nancy, France

Доп.точки доступа:
Krylov, A. S.; Крылов, Александр Сергеевич; Shipilovskikh, S. A.; Krylova, S. N.; Крылова, Светлана Николаевна; Slyusarenko, N. V.; Timofeeva, M.; Kenzhebayeva, Yu. A.; Bachinin, S. V.; Yushina, I. D.; Cherepakhin, A. V.; Черепахин, Александр Владимирович; Shestakov, N. P.; Шестаков, Николай Петрович; Nemtsev, I. V.; Vtyurin, A. N.; Втюрин, Александр Николаевич; Milichko, V. A.
}
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10.

    Behavior of CaBSiO4(OH) datolite at high temperatures and pressures of a water medium / S. V. Goryainov [et al.] // Bull. Russ. Acad. Sci. Phys. - 2015. - Vol. 79, Is. 6. - P. 794-797, DOI 10.3103/S1062873815060118. - Cited References: 9. - This work was supported by the Russian Foundation for Basic Research, project nos. 13-05-00185 and 4-05-00616. . - ISSN 1062-8738
Рубрики:
Constant pressures
   Constant temperature
   High temperature
   Polymorphic transitions
   T parameter
   Tectonic plates
   Water mediums
   Silicate minerals
Аннотация: The behavior of CaBSiO4(OH) datolite compressed in a water medium at simultaneous high temperatures and pressures corresponding to the cold zones of tectonic plate subduction (up to P ~5.3 GPa and T ~250°C) is studied in situ via Raman spectroscopy. Two polymorphic transitions are found: (i) upon an increase of up to 2 GPa in pressure at a constant temperature of 22°C and (ii) upon heating to ~90°C at a constant pressure of ~5–5.3 GPa. Major trends of the variations in the Raman spectra are identified for all phases of the indicated P–T parameters. No overhydration and amorphization of datolite is observed. © 2015, Allerton Press, Inc.

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Публикация на русском языке Поведение датолита CaBSiO4(OH) при высоких температурах и давлениях водной среды [Текст] / С. В. Горяйнов [и др.] // Изв. РАН. Сер. физич. - 2015. - Т. 79 № 6. - С. 880–883

Держатели документа:
Sobolev Institute of Geology and Mineralogy, Siberian Branch, Russian Academy of Sciences, Novosibirsk, Russian Federation
Kirensky Institute of Physics, Siberian Branch, Russian Academy of Sciences, Krasnoyarsk, Russian Federation
University of Saskatchewan, Saskatoon, SK, Canada

Доп.точки доступа:
Goryainov, S. V.; Krylov, A. S.; Крылов, Александр Сергеевич; Vtyurin, A. N.; Втюрин, Александр Николаевич; Pan, Y.
}
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11.

    Colloidal and deposited products of the interaction of tetrachloroauric acid with hydrogen selenide and hydrogen sulfide in aqueous solutions / S. Vorobyev [et al.] // Minerals. - 2018. - Vol. 8, Is. 11. - Ст. 492, DOI 10.3390/min8110492. - Cited References: 63. - This research was funded by the Siberian Branch of the Russian Academy of sciences, Program of Interdisciplinary Studies, grant number 64 (project 303). . - ISSN 2075-163X
   Перевод заглавия: Коллоидные и осажденные продукты взаимодействия золотохлористоводородной кислоты с селеноводородом и сероводородом в водных растворах
Кл.слова (ненормированные):
Gold selenide -- Gold sulfoselenide -- Colloids -- Nanoparticles -- Nucleation -- Liquid intermediates -- Deposition
Аннотация: The reactions of aqueous gold complexes with H2Se and H2S are important for transportation and deposition of gold in nature and for synthesis of AuSe-based nanomaterials but are scantily understood. Here, we explored species formed at different proportions of HAuCl4, H2Se and H2S at room temperature using in situ UV-vis spectroscopy, dynamic light scattering (DLS), zeta-potential measurement and ex situ Transmission electron microscopy (TEM), electron diffraction, X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), and Raman spectroscopy. Metal gold colloids arose at the molar ratios H2Se(H2S)/HAuCl4 less than 2. At higher ratios, pre-nucleation “dense liquid” species having the hydrodynamic diameter of 20–40 nm, zeta potential −40 mV to −50 mV, and the indirect band gap less than 1 eV derived from the UV-vis spectra grow into submicrometer droplets over several hours, followed by fractional nucleation in the interior and coagulation of disordered gold chalcogenide. XPS found only one Au+ site (Au 4f7/2 at 85.4 eV) in deposited AuSe, surface layers of which partially decomposed yielding Au0 nanoparticles capped with elemental selenium. The liquid species became less dense, the gap approached 2 eV, and gold chalcogenide destabilized towards the decomposition with increasing H2S content. Therefore, the reactions proceed via the non-classical mechanism involving “dense droplets” of supersaturated solution and produce AuSe1−xSx/Au nanocomposites.

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Держатели документа:
Institute of Chemistry and Chemical Technology of the Siberian Branch of the Russian Academy of Sciences, Krasnoyarsk, 660036, Russian Federation
Kirensky Institute of Physics of the Siberian Branch of the Russian Academy of Sciences, Krasnoyarsk, 660036, Russian Federation
Electron Microscopy Laboratory, Siberian Federal University, Krasnoyarsk, 660041, Russian Federation

Доп.точки доступа:
Vorobyev, S.; Likhatski, M.; Romanchenko, A.; Maksimov, N.; Zharkov, S. M.; Жарков, Сергей Михайлович; Krylov, A. S.; Крылов, Александр Сергеевич; Mikhlin, Y.
}
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12.

    Colloidal and immobilized nanoparticles of lead xanthates / S. A. Vorobyev [et al.] // ACS Omega. - 2019. - Vol. 4, Is. 7. - P. 11472-11480, DOI 10.1021/acsomega.9b00841. - Cited References: 56. - This research was supported by Russian Science Foundation, project 18-17-00135. . - ISSN 2470-1343
   Перевод заглавия: Коллоидные и иммобилизированные наночастицы ксантогенатов свинца
Аннотация: Although nanoparticles of heavy metal xanthates and their hydrosols can play important roles in froth flotation, environmental issues, analytics, and manufacturing of metal sulfide nanocomposites, they have received little attention. We studied colloidal solutions and immobilized particles prepared via interaction of aqueous lead nitrate with alkyl xanthates applying UV−vis absorption spectroscopy, dynamic light scattering, zeta potential measurement, thermogravimetry analysis, Fourier transform infrared spectroscopy, Raman scattering, X-ray photoelectron spectroscopy, atomic force microscopy, and transmission electron microscopy. The hydrodynamic diameter of colloidal particles of Pb(SSCOR)2 decreased from 500 to 50 nm with an increase in the alkyl radical length and the initial xanthate to lead ratio (X/Pb); the zeta potential magnitude varied similarly, although it remained negative. The effect of pH in the range of 4.5−11 was minor, but the colloids produced using excess of Pb2+ in alkaline media were close to PbX and decomposed much easier than PbX2. The uptake of lead xanthates on supports was generally low because of negative charges of the colloids; however, 50−100 nm thick PbX2 films were deposited on PbS and SiO2 from the media of X/Pb 2 and pH 9 because of preadsorption of Pb2+, while nanorods formed on highly oriented pyrolytic graphite.

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Institute of Chemistry and Chemical Technology, Federal Research Center “Krasnoyarsk Scientific Center”, Siberian Branch of the Russian Academy of Sciences, Akademgorodok, 50/24, Krasnoyarsk, 660036, Russian Federation
Siberian Federal University, Svobodny pr. 79, Krasnoyarsk, 660041, Russian Federation
Kirensky Institute of Physics, Federal Research Center “Krasnoyarsk Scientific Center” of, Siberian Branch of the Russian Academy of Sciences, Akademgorodok 50/38, Krasnoyarsk, 660036, Russian Federation

Доп.точки доступа:
Vorobyev, S. A.; Saikova, S. V.; Novikova, S. A.; Fetisova, O. Y.; Zharkov, S. M.; Жарков, Сергей Михайлович; Krylov, A. S.; Крылов, Александр Сергеевич; Likhatski, M. N.; Mikhlin, Y. L.
}
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13.

Condensation of a soft mode in the Raman spectrum of the second tetragonal phase of CsScF4 / A. N. Vtyurin [et al.] // Phys. Solid State. - 1997. - Vol. 39, Is. 4. - P. 632-633, DOI 10.1134/1.1129919. - Cited References: 4 . - ISSN 1063-7834

РУБ Physics, Condensed Matter

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Держатели документа:
L. V. Kirenskii Inst. of Phys., Russian Academy of Sciences, Siberian Branch, 660036 Krasnoyarsk, Russian Federation
ИФ СО РАН
Доп.точки доступа:
Vtyurin, A. N.; Втюрин, Александр Николаевич; Krylov, A. S.; Крылов, Александр Сергеевич; Shmygol, I. V.; Shebanin, A. P.
}
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14.

    Crystal and electronic structure, thermochemical and photophysical properties of europium-silver sulfate monohydrate AgEu(SO4)2·H2O / Y. G. Denisenko, A. E. Sedykh, M. S. Molokeev [et al.] // J. Solid State Chem. - 2021. - Vol. 294. - Ст. 121898, DOI 10.1016/j.jssc.2020.121898. - Cited References: 54. - This work was partially supported by the Russian Foundation for Basic Research (Grant 19-33-90258∖19 ). Use of equipment of Krasnoyarsk Regional Center of Research Equipment of Federal Research Center « Krasnoyarsk Science Center SB RAS» is acknowledged . - ISSN 0022-4596
   Перевод заглавия: Кристаллическая и электронная структура, термохимические и фотофизические свойства моногидрата сульфата европия-серебра AgEu(SO4)2·H2O
Кл.слова (ненормированные):
Structure -- Thermochemistry -- Luminescence -- Sulfates -- Europium
Аннотация: In order to synthesize single crystals of europium-silver double sulfate monohydrate, a hydrothermal reaction route was used. It was found that the crystallization cannot be performed under standard conditions. The compound AgEu(SO4)2·H2O crystallizes in the trigonal crystal system, space group P3221 (a = 6.917(1), c = 12.996(2) Å, V = 538.53(17) Å3). The structure consists of triple-capped trigonal prisms [EuO9], in which one oxygen atom belongs to crystalline water, silver octahedra [AgO6], and sulfate tetrahedra [SO4]. The hydrogen bonds in the system additionally stabilize the structure. The electronic band structure wasstudied by density functional theory calculations which show that AgEu(SO4)2·H2O is an indirect band gap dielectric. Temperature dependent photoluminescence spectroscopy shows emission bands of transitions from the 5D0 state to the spin-orbit components of the 7FJmultiplet (J = 0–6).The ultranarrow transition 5D0 - 7F0 shows a red shift with respect to other europium-containing water-free sulfates that is ascribed to the presence of OH group in the crystal structure in the close vicinity of the Eu3+ ion. An effect of abnormal sensitivity of the Ω4 intensity factor to minor distortions of the local environment is detected for the observed low local symmetry of C2.

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Institute of Chemistry, Tyumen State University, Tyumen, 625003, Russian Federation
Institute of Inorganic and Analytical Chemistry, Justus-Liebig-University of Giessen, Giessen35392, Germany
Department of General and Special Chemistry, Industrial University of Tyumen, Tyumen, 625000, Russian Federation
Center for Materials Research (LaMa), Justus-Liebig-University of Giessen, Giessen35392, Germany
Laboratory of Crystal Physics, Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
Siberian Federal University, Krasnoyarsk, 660041, Russian Federation
Department of Physics, Far Eastern State Transport University, Khabarovsk, 680021, Russian Federation
Laboratory of Molecular Spectroscopy, Kirensky Institute of Physics Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
Laboratory of Coherent Optics, Kirensky Institute of Physics Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
Institute of Nanotechnology, Spectroscopy and Quantum Chemistry, Siberian Federal University, Krasnoyarsk, 660041, Russian Federation
Komissarov Department of General Chemistry, Northen Trans-Ural Agricultural University, Tyumen, 625003, Russian Federation
Laboratory of the Chemistry of Rare Earth Compounds, Institute of Solid State Chemistry, UB RAS, Ekaterinburg, 620137, Russian Federation

Доп.точки доступа:
Denisenko, Y. G.; Sedykh, A. E.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Oreshonkov, A. S.; Орешонков, Александр Сергеевич; Aleksandrovsky, A. S.; Александровский, Александр Сергеевич; Krylov, A. S.; Крылов, Александр Сергеевич; Khritokhin, N. A.; Sal'nikova, E. I.; Andreev, O. V.; Muller-Buschbaum, K.
}
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15.

    Crystal growth and Raman spectroscopy study of Sm1-xLaxFe3(BO3)4 ferroborates / E. Moshkina [et al.] // Cryst. Growth Des. - 2016. - Vol. 16, Is. 12. - P. 6915-6921, DOI 10.1021/acs.cgd.6b01079. - Cited References: 17. - This work was supported by the Russian Foundation for Basic Research, Project No. 14-02-00307. . - ISSN 1528-7483
   Перевод заглавия: Рост кристаллов и исследование ферроборатов Sm1-xLaxFe3(BO3)4 методом спектроскопии комбинационного рассеяния света
Кл.слова (ненормированные):
Crystal lattices -- Iron compounds -- Raman spectroscopy -- Single crystals -- Crystal nucleation -- Flux methods -- Internal structure -- Magnetic phase transitions -- Magnon scattering -- Spectral region -- Temperature range -- Wave numbers -- Lanthanum
Аннотация: Sm1-xLaxFe3(BO3)4 (x = 0, 0.75) single crystals were synthesized using the flux method. The crystal nucleation procedure and flux parameters are reported. Conditions for growing the Sm1-xLaxFe3(BO3)4 (x = 0, 0.75) single crystals are described. The prepared crystals were studied by Raman spectroscopy in the temperature range of T = 10-300 K. The spectral region corresponding to temperatures of T = 10-55 K, which involves the temperatures of the magnetic phase transition TN = 32 K for x = 0 and TN = 31 K for x = 0.75, was thoroughly analyzed. Anomalies related to the magnetic ordering established in both compounds were found. The main changes occur in the low-wavenumber region (up to 100 cm-1), where the mode corresponding to magnon scattering arises. This mode is shown to have the internal structure indicative of the occurrence of unstable vibrations (40-80 cm-1). The results obtained are analyzed by calculating the empirical lattice dynamics in Sm1-xLaxFe3(BO3)4 with x = 0 and x = 1. © 2016 American Chemical Society.

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Держатели документа:
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, Russian Federation
Siberian State Aerospace University, Krasnoyarsk, Russian Federation

Доп.точки доступа:
Moshkina, E. M.; Мошкина, Евгения Михайловна; Krylov, A. S.; Крылов, Александр Сергеевич; Sofronova, S. N.; Софронова, Светлана Николаевна; Gudim, I. A.; Гудим, Ирина Анатольевна; Temerov, V. L.; Темеров, Владислав Леонидович
}
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16.

Crystal size: Versus paddle wheel deformability: Selective gated adsorption transitions of the switchable metal-organic frameworks DUT-8(Co) and DUT-8(Ni) / S. Ehrling [et al.] // J. Mater. Chem. A. - 2019. - Vol. 7, Is. 37. - P. 21459-21475, DOI 10.1039/c9ta06781g. - Cited References: 106. - The authors thank DFG (FOR 2433) for financial support. We thank HZB for the allocation of synchrotron radiation beam-time and financial support. PP, TW and TH used high performance facilities of ZIH Dresden. TW thanks the European Social Funds for Germany for a PhD fellowship. . - ISSN 2050-7488
Кл.слова (ненормированные):
Cobalt -- Crystallite size -- Density functional theory -- Dichloromethane -- Inclusions -- Nickel -- Organometallics -- Particle size -- Physisorption -- Single crystals -- Wheels -- X ray powder diffraction
Аннотация: Switchable pillared layer metal–organic frameworks M2(2,6-ndc)2(dabco) (DUT-8(M), M = Ni, Co, 2,6-ndc = 2,6-naphthalenedicarboxylate, dabco = 1,4-diazabicyclo-[2.2.2]octane, DUT – Dresden University of Technology) were synthesised in two different crystallite size regimes to produce particles up to 300 μm and smaller particles around 0.1 μm, respectively. The textural properties and adsorption-induced switchability of the materials, obtained from both syntheses, were studied by physisorption of N2 at 77 K, CO2 at 195 K and n-butane at 273 K, revealing pronounced differences in adsorption behavior for Ni and Co analogues. While the smaller nano-sized particles (50–200 nm) are rigid and show no gating transitions confirming the importance of crystallite size, the large particles show pronounced switchability with characteristic differences for the two metals resulting in distinct recognition effects for various gases and vapours. Adsorption of various vapours demonstrates consistently a higher energetic barrier for the “gate opening” of DUT-8(Co) in contrast to DUT-8(Ni), as the “gate opening” pressure for Co based material is shifted to a higher value for adsorption of dichloromethane at 298 K. Evaluation of crystallographic data, obtained from single crystal and powder X-ray diffraction analysis, showed distinct geometric differences in the paddle wheel units of the respective MOFs. These differences are further disclosed by solid-state UV-vis, FT-IR and Raman spectroscopy. Magnetic properties of DUT-8(Co) and DUT-8(Ni) were investigated, indicating a high-spin state for both materials at room temperature. Density functional theory (DFT) simulations confirmed distinct energetic differences for Ni and Co analogues with a higher energetic penalty for the structural “gate opening” transformation for DUT-8(Co) compared to DUT-8(Ni) explaining the different flexibility behaviour of these isomorphous MOFs.

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Держатели документа:
Department of Inorganic Chemistry, Technische Universitat Dresden, Bergstrasse 66, Dresden, 01069, Germany
University of Sofia, Faculty of Chemistry and Pharmacy, Sofia, 1126, Bulgaria
Leibniz Institute for Solid State and Materials Research, IFW Dresden, Helmholtz-strasse 20, Dresden, 01069, Germany
Wilhelm-Ostwald-Institute of Physical and Theoretical Chemistry, Faculty for Chemistry and Mineralogy, Leipzig University, Leipzig, 04103, Germany
Helmholtz-Zentrum Dresden-Rossendorf, Institute of Resource Ecology, Research Site Leipzig, Permoserstr. 15, Leipzig, 04318, Germany
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
Siberian Federal University, Svobodny Prospect 79, Krasnoyarsk, 660041, Russian Federation
Institute of Automation and Electrometry of the SB RAS, Novosibirsk, 630090, Russian Federation
Research Group Macromolecular Crystallography, Helmholtz-Zentrum Berlin fur Materialien und Energie, Albert-Einstein-Stra?e 15, Berlin, 12489, Germany
Department of Theoretical Chemistry, Technische Universitat Dresden, Berg-strasse 66, Dresden, 01069, Germany

Доп.точки доступа:
Ehrling, S.; Senkovska, I.; Bon, V.; Evans, J. D.; Petkov, P.; Krupskaya, Y.; Kataev, V.; Wulf, T.; Krylov, A. S.; Крылов, Александр Сергеевич; Vtyurin, A. N.; Втюрин, Александр Николаевич; Krylova, S. N.; Крылова, Светлана Николаевна; Adichtchev, S.; Slyusareva, E.; Weiss, M. S.; Buchner, B.; Heine, T.; Kaskel, S.
}
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17.

    Crystal structure and phase transitions of a layered perovskite-like CsScF4 crystal / A. S. Krylov [et al.] // CrystEngComm. - 2016. - Vol. 18, Is. 43. - P. 8472-8486, DOI 10.1039/c6ce01144f. - Cited References:47. - The authors are grateful to Prof. I. N. Flerov for valuable support and useful discussions. This work was partly supported by the Russian Foundation for Basic Research, Project 16-02-00102. The research is partially conducted within the framework of the state task of the Ministry of Education and Science of the Russian Federation for Siberian Federal University on R&D performance in 2014 (Task 3.2534.2014/K). X-ray data from powders, Raman NMR, and IR spectra were obtained with use the analytical equipment of Krasnoyarsk Center of collective use SB RAS. . - ISSN 1466-8033
   Перевод заглавия: Кристаллическая структура и фазовые переходы в слоистом перовскитоподобном кристалле CsScF4

РУБ Chemistry, Multidisciplinary + Crystallography
Рубрики:
NEGATIVE THERMAL-EXPANSION
RAMAN-SCATTERING
LATTICE-DYNAMICS
Аннотация: This work is devoted to the complex research on temperature phase transitions in a CsScF4 crystal. The crystal structure was solved and refined at different temperatures by using the Rietveld method. Structural phase transitions were investigated by using the following spectroscopic methods, some of them for the first time: Brillouin spectroscopy, Raman spectroscopy, IR absorption spectroscopy and NMR. The symmetry analysis of the Brillouin zone center of all phases is presented. The vibrational spectra of the crystal in three phases have been calculated. The structural phase transition mechanism was determined. The transitions at T-1 = 475 K and T-2 = 317.5 K are of displacement type. The Raman soft modes have been associated with rotations of the ScF6 octahedral group.

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SB RAS, LV Kirensky Inst Phys, Krasnoyarsk 660036, Russia.
Far Eastern State Transport Univ, Dept Phys, Khabarovsk 680021, Russia.
Siberian Fed Univ, Inst Engn Phys & Radioelect, Krasnoyarsk 660041, Russia.
SB RAS, Inst Automat & Electrometry, Novosibirsk 630090, Russia.

Доп.точки доступа:
Krylov, A. S.; Крылов, Александр Сергеевич; Molokeev, M. S.; Молокеев, Максим Сергеевич; Misyul, S. V.; Krylova, S. N.; Крылова, Светлана Николаевна; Oreshonkov, A. S.; Орешонков, Александр Сергеевич; Ivanenko, A. A.; Иваненко, Александр Анатольевич; Zykova, V. A.; Ivanov, Y. N.; Иванов, Юрий Николаевич; Sukhovsky, A. A.; Суховский, Андрей Андреевич; Voronov, V. N.; Воронов, Владимир Николаевич; Safonov, I. N.; Vtyurin, A. N.; Втюрин, Александр Николаевич; Russian Foundation for Basic Research [16-02-00102]
}
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18.

    Crystal structure, vibrational, spectroscopic and thermochemical properties of double sulfate crystalline hydrate [CsEu(H2O)3(SO4)2]·H2O and its thermal dehydration product CsEu(SO4)2 / Y. G. Denisenko, M. S. Molokeev, A. S. Oreshonkov [et al.] // Crystals. - 2021. - Vol. 11, Is. 9. - Ст. 1027, DOI 10.3390/cryst11091027. - Cited References: 103. - This work was partially supported by the Russian Foundation for Basic Research (grant 19-33-90258\19) . - ISSN 2073-4352
   Перевод заглавия: Кристаллическая структура, колебательные, спектроскопические и термохимические свойства двойного сульфатного кристаллического гидрата [CsEu(H2O)3(SO4)2]·H2O и продукта его термической дегидратации CsEu(SO4)2
Кл.слова (ненормированные):
sulfate -- dehydration -- crystal structure -- Raman -- thermal stability -- photoluminescence
Аннотация: Crystalline hydrate of double cesium europium sulfate [CsEu(H2O)3(SO4)2]·H2O was synthesized by the crystallization from an aqueous solution containing equimolar amounts of 1Cs+:1Eu3+:2SO42− ions. Anhydrous salt CsEu(SO4)2 was formed as a result of the thermal dehydration of the crystallohydrate. The unusual effects observed during the thermal dehydration were attributed to the specific coordination of water molecules in the [CsEu(H2O)3(SO4)2]·H2O structure. The crystal structure of [CsEu(H2O)3(SO4)2]·H2O was determined by a single crystal X-ray diffraction analysis, and the crystal structure of CsEu(SO4)2 was obtained by the Rietveld method. [CsEu(H2O)3(SO4)2]·H2O crystallizes in the monoclinic system, space group P21/c (a = 6.5574(1) Å, b = 19.0733(3) Å, c = 8.8364(2) Å, β = 93.931(1)°, V = 1102.58(3) Å3). The anhydrous sulfate CsEu(SO4)2 formed as a result of the thermal destruction crystallizes in the monoclinic system, space group C2/c (a = 14.327(1) Å, b = 5.3838(4) Å, c = 9.5104(6) Å, β = 101.979(3) °, V = 717.58(9) Å3). The vibration properties of the compounds are fully consistent with the structural models and are mainly determined by the deformation of non-rigid structural elements, such as H2O and SO42−. As shown by the diffused reflection spectra measurements and DFT calculations, the structural transformation from [CsEu(H2O)3(SO4)2]·H2O to CsEu(SO4)2 induced a significant band gap reduction. A noticeable difference of the luminescence spectra between cesium europium sulfate and cesium europium sulfate hydrate is detected and explained by the variation of the extent of local symmetry violation at the crystallographic sites occupied by Eu3+ ions, namely, by the increase in inversion asymmetry in [CsEu(H2O)3(SO4)2]·H2O and the increase in mirror asymmetry in CsEu(SO4)2. The chemical shift of the 5D0 energy level in cesium europium sulfate hydrate, with respect to cesium europium sulfate, is associated with the presence of H2O molecules in the vicinity of Eu3+ ion.

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Держатели документа:
Department of Inorganic and Physical Chemistry, Tyumen State University, Tyumen, 625003, Russian Federation
Laboratory of Crystal Physics, Federal Research Center KSC SB RAS, Kirensky Institute of Physics, Krasnoyarsk, 660036, Russian Federation
Institute of Engineering Physics and Radioelectronic, Siberian Federal University, Krasnoyarsk, 660041, Russian Federation
Department of Physics, Far Eastern State Transport University, Khabarovsk, 680021, Russian Federation
Laboratory of Molecular Spectroscopy, Federal Research Center KSC SB RAS, Kirensky Institute of Physics, Krasnoyarsk, 660036, Russian Federation
School of Engineering and Construction, Siberian Federal University, Krasnoyarsk, 660041, Russian Federation
Laboratory of Coherent Optics, Federal Research Center KSC SB RAS, Kirensky Institute of Physics, Krasnoyarsk, 660036, Russian Federation
Department of Photonics and Laser Technology, Siberian Federal University, Krasnoyarsk, 660041, Russian Federation
Laboratory of Chemistry of Compounds of Rare-Earth Elements, Institute of Solid State Chemistry, UB RAS, Ekaterinburg, 620137, Russian Federation
Laboratory of Optical Materials and Structures, Institute of Semiconductor Physics, SB RAS, Novosibirsk, 630090, Russian Federation
Research and Development Department, Kemerovo State University, Kemerovo, 650000, Russian Federation

Доп.точки доступа:
Denisenko, Y. G.; Molokeev, M. S.; Молокеев, Максим Сергеевич; Oreshonkov, A. S.; Орешонков, Александр Сергеевич; Krylov, A. S.; Крылов, Александр Сергеевич; Aleksandrovsky, A. S.; Александровский, Александр Сергеевич; Azarapin, N. O.; Andreev, O. V.; Razumkova, I. A.; Atuchin, V. V.
}
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19.

Cubic to cubic phase transition in (NH4)3SnF7 ferroelastic crystal– Raman scattering study / A. N. Vtyurin [et al.] // 3th Int. Conf. "Scanning Probe Microscopy". 4th Russia-China Workshop on Dielectric and Ferroel. Mater. (SPM-2019-RCWDFM). Int. Youth Conf. "Functional Imaging of Nanomaterials" : Abstract book of joint int. conf. - 2019. - Ст. P182. - P. 285. - Cited References: 1. - This work was supported by Russian Foundation for Basic Research (Grant N 17-02-00920) . - ISBN 978-5-9500624-2-1

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Держатели документа:
Kirensky Institute of Physics, FRC KSC SB RAS, 660036, Krasnoyarsk, Russia
Siberian Federal University
Institute of Chemistry, Far Eastern Branch of RAS

Доп.точки доступа:
Vtyurin, A. N.; Втюрин, Александр Николаевич; Gerasimova, Y. V.; Герасимова, Юлия Валентиновна; Krylov, A. S.; Крылов, Александр Сергеевич; Laptash, N. M.; Krylova, S. N.; Крылова, Светлана Николаевна; Уральский федеральный университет им. первого Президента России Б.Н. Ельцина; Scanning Probe Microscopy, International Conference(3 ; 2019 ; Aug. ; 25-28 ; Ekaterinburg); Russia-China Workshop on Dielectric and Ferroelectric Materials(4 ; 2019 ; Aug. ; 25-28 ; Ekaterinburg); "Functional Imaging of Nanomaterials", International Youth Conference(2019 ; Aug. ; 25-28 ; Ekaterinburg)
}
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20.

Determination of gruneisen parameters in δ-BiB3O6 crystal / E. A. Strikina [et al.] // Joint 13th Russia/CIS/Baltic/Japan Symp. on Ferroelectricity and Int. Workshop on Relaxor Ferroelectrics (RCBJSF-IWRF 2016) : book of abstracts. - 2016. - Ст. P-57. - References: 2

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Доп.точки доступа:
Strikina, E. A.; Стрикина, Екатерина Андреевна; Vtyurin, A. N.; Втюрин, Александр Николаевич; Krylov, A. S.; Крылов, Александр Сергеевич; Oreshonkov, A. S.; Орешонков, Александр Сергеевич; Russia/CIS/Baltic/Japan Symposium on Ferroelectricity(13 ; 2016 ; Jun. ; 19-23 ; Matsue, Japan); International Workshop on Relaxor Ferroelectrics(2016 ; Jun. ; 19-23 ; Matsue, Japan)
}
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