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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Орлов, Юрий Сергеевич, Дудников, Вячеслав Анатольевич, Соколов, Алексей Эдуардович, Овчинникова Т. М., Шестаков, Николай Петрович, Овчинников, Сергей Геннадьевич
Заглавие : Флуктуации мультиплетности ионов Co3+ и смягчение фононного спектра редкоземельных оксидов кобальта
Место публикации : Письма в ЖЭТФ. - 2022. - Т. 115, Вып. 9-10. - С. 650-655. - ISSN 0370-274X, DOI 10.31857/S1234567822100081
Примечания : Библиогр.: 25. - Работа выполнена при финансовой поддержки гранта Российского научного фонда # 18-12-00022
Аннотация: Экспериментально и теоретически исследована необычная температурная зависимость спектров инфракрасного поглощения редкоземельных оксидов кобальта LaCoO3 и GdCoO3 в интервале температур 3.2-550 K. Обнаружено достаточно сильное смягчение оптической фононной моды, которое нельзя объяснить стандартным решеточным ангарманизмом. Показано, что красное смещение фононного спектра обусловлено квадратичным по смещению решетки электрон-фононным взаимодействием и флуктуациями мультиплетности ионов Co3+.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Sokolov A. Е., Ivanova O. S., Svetlitsky E. S., Lukyanenko K. A., Shabanov A. V., Shestakov N. P., Chen Y. -Z., Tseng Y.-T., Lin C.-R.
Заглавие : Core-shell Fe3O4@C nanoparticles for magneto-mechanical destroy of Ehrlich ascites carcinoma cells
Коллективы : Asian School-Conference on Physics and Technology of Nanostructured Materials, Азиатская школа-конференция по физике и технологии наноструктурированных материалов
Место публикации : The Sixth Asian school-conference on physics and technology of nanostructured materials: Proceedings. - VLadivostok, 2022. - Ст.IV.o.08. - P.189-190. - ISBN 987-5-8044-1716-2
Примечания : Cited References: 2
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Аннотация: The core-shell magnetic nanoparticles, Fe3O4@C, were synthesized and surface aptamer-functionalized to use them as destroyers of living cancer Ehrlich's ascitic carcinoma cells. The morphology and features of the structural and magnetic properties of the obtained hybrid nanoparticles are studied.
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Ekimov A.A., Krylov A.S., Vtyurin A.N., Ivanenko A.A., Shestakov N.P., Goryainov S.V., Kocharova A.G.
Заглавие : Vibrational spectroscopy study of temperature and high pressure phase transition in K3WO3F3
Коллективы : IEEE International Symposium on Applications of Ferroelectrics, International Meeting on Ferroelectricity
Место публикации : The 12th International Meeting on Ferroelectricity and 18th IEEE International Symposium on Applications of Ferroelectrics (IMF-ISAF 2009): Xi'an, China, August 23-27, 2009 . - 2009. - Ст.AP-077
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Ronzhin N. O., Posokhina E. D., Mikhlina E. V., Shestakov N. P., Nemtsev I. V., Bondar V. S., Ryzhkov I. I.
Заглавие : The effect of copper and iron adsorption on the catalytic performance of alumina nanofiber / nanodiamond composite in sensing applications
Место публикации : J. Phys. Chem. Solids. - 2022. - Vol. 167. - Ст.110785. - ISSN 00223697 (ISSN), DOI 10.1016/j.jpcs.2022.110785
Примечания : Cited References: 68. - This work is supported by the Russian Foundation for Basic Research, Project 18–29–19078. The authors would like to express their special thanks to Krasnoyarsk Regional Center of Research Equipment of Federal Research Center «Krasnoyarsk Science Center SB RAS» for providing the equipment to ensure the accomplishment of this project
Аннотация: Phenolic compounds are common environmental pollutants, which are used in many industries and contaminate water environment due to industrial wastewater discharge. Presently, there is an increasing demand for the development and improvement of inexpensive, easy-to-use analytical tools for in-situ detection of phenolic compounds. In this work, we investigate the effect of adsorption of Cu2+ and Fe2+ ions on the catalytic activity of a composite material based on alumina nanofibers (ANF) and detonation nanodiamonds (DND) in the co-oxidation of phenols with 4-aminoantipyrine in the presence of hydrogen peroxide. We have found more than two-fold increase of the catalytic activity for ANF + DND + Cu composite, while the activity of ANF + DND + Fe composite is found to decrease by several times in comparison with the original ANF + DND material. The results of FTIR analysis indicate that the adsorption of iron ions occurs with the formation of hydroxide surface groups and hydrogen bonds, which apparently block their catalytic activity in the Fenton redox cycle. The higher catalytic performance of AND + DND composite functionalized with copper ions makes it possible to detect two times lower concentrations of analytes (phenol and 4-chlorophenol) in comparison with the original composite. It is shown that the AND + DND + Cu composite provides a linear yield of the co-oxidation reaction product in a wide range of analyte concentrations (0.25–100 μM for phenol and 0.5–25 μM for 4-chlorophenol). Model experiments demonstrate the applicability of copper-functionalized composite as a reusable sensor for the determination of phenol in aqueous samples.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Vtyurin A.N., Gerasimova J.V., Krylov A.S., Ivanenko A.A., Shestakov N.P., Laptash N.M., Voyt E.I.
Заглавие : Vibrational spectroscopy of alkaline tungsten oxyfluoride crystals: structure, lattice dynamics, ordering processes, and phase transitions
Место публикации : J. Raman Spectrosc. - MALDEN: WILEY-BLACKWELL, 2010. - Vol. 41, Is. 12. - С. 1784-1791. - DEC. - ISSN 0377-0486, DOI 10.1002/jrs.2637
Примечания : Cited Reference Count: 13. - Гранты: We would like to thank Prof. Igor Flerov for fruitful discussion. Technical assistance of Victor Ouskin is highly appreciated. This work has been supported by the Russian Foundation for Basic Researches, grant no. 08-02-00066-a.Финансирующая организация: Russian Foundation for Basic Researches [08-02-00066-a]
Предметные рубрики:
Ключевые слова (''Своб.индексиров.''): raman scattering--infrared absorption--alcaline tungsten oxyfluorides--phase transitions--alcaline tungsten oxyfluorides--infrared absorption--phasetransitions--raman scattering
Аннотация: Raman scattering (RS) and infrared absorption (IR) of ammonium oxyfluoride crystals (NH(4))(3)WO(3)F(3), (NH(4))(2)KWO(3)F(3), and Cs(2)(NH(4))WO(3)F(3) are compared. Conformation of the WO(3)F(3) octahedral groups has been established; anomalies have been found close to the transition temperatures in the internal vibrational regions of ammonium and WO(3)F(3) groups. The phase transition in (NH(4))(3)WO(3)F(3) is associated mostly with the ordering of octahedral groups and formation of W-O center dot center dot center dot H-N hydrogen bonds. In (NH(4))(2)KWO(3)F(3) crystal, the transition is not related to the ordering processes; CS(2)(NH(4))WO(3)F(3) retains its disordered structure down to 10 K. Copyright (C) 2010 John Wiley & Sons, Ltd.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Ekimov A. A., Krylov A. S., Vtyurin A. N., Ivanenko A. A., Shestakov N. P., Kocharova A. G.
Заглавие : Vibrational spectroscopy studies of temperature phase transitions in K 3WO3F3
Место публикации : Ferroelectrics. - 2010. - Т. 401, № 1. - P.168-172. - ISSN 0015-0193, DOI 10.1080/00150191003676280. - ISSN 1563-5112(eissn)
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Втюрин, Александр Николаевич, Герасимова, Юлия Валентиновна, Крылов, Александр Сергеевич, Иваненко, Александр Анатольевич, Шестаков, Николай Петрович, Лапташ Н. М., Войт Е. И.
Заглавие : Колебательная спектроскопия молекулярно-ионных кристаллов оксифторидов вольфрама – структура, динамика решетки, процессы упорядочения, фазовые переходы
Место публикации : Оптическая спектроскопия и стандарты частоты/ Под ред. Виноградова Е.А., Синицы Л.Н. - Томск: Изд-во Института оптики атмосферы СО РАН, 2009. - Т. 3. - С. 34-48
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Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Vtyurin A.N., Krylov A.S., Gerasimova Ju.V., Ivanenko A.A., Shestakov N.P., Laptash N.M.
Заглавие : Ordering processes and phase transitions in ammonium-containing crystals of A2BWO3F3 elpasolites – com?parative Raman and infrared study
Коллективы : IEEE International Symposium on Applications of Ferroelectrics, International Meeting on Ferroelectricity
Место публикации : The 12th International Meeting on Ferroelectricity and 18th IEEE International Symposium on Applications of Ferroelectrics (IMF-ISAF 2009): Xi'an, China, August 23-27, 2009 . - 2009. - Ст.OA-040
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Orlov Yu. S., Dudnikov V. A., Sokolov A. Е., Ovchinnikova T. M., Shestakov N. P., Ovchinnikov S. G.
Заглавие : Fluctuations of the multiplicity of Co3+ ions and softening of the phonon spectrum of rare-earth cobalt oxides
Место публикации : JETP Letters. - 2022. - Vol. 115, Is. 10. - P.615-619. - ISSN 00213640 (ISSN), DOI 10.1134/S0021364022100575
Примечания : Cited References: 25. - This work was supported by the Russian Science Foundation (project no. 18-12-00022)
Аннотация: An unconventional temperature dependence of infrared absorption spectra of rare-earth cobalt oxides LaCoO3 and GdCoO3 has been studied experimentally and theoretically in the temperature range of 3.2–550 K. A quite strong softening of the optical phonon mode has been detected, which cannot be explained by standard lattice anharmonicity. It has been shown that the redshift of the phonon spectrum is due to the e-lectron–phonon coupling quadratic in the lattice displacement and to fluctuations of the multiplicity of Co3+ ions.
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Ivantsov R. D., Lin C. -R., Chen Y. -Z., Ivanova O. S., Altunin R. R., Knyazev Yu. V., Molokeev M. S., Zharkov S. M., Shestakov N. P., Sukhachev A. L., Edelman I. S.
Заглавие : Effect of surfactants on the structure, phase composition, and magnetic properties of FexSy nanoparticles synthesized by thermal decomposition
Место публикации : Nanobiotechnol. Rep. - 2022. - Vol. 17, Is. 3. - P.336-344. - ISSN 26351676 (ISSN), DOI 10.1134/S2635167622030089
Примечания : Cited References: 27. - This study was supported by the Russian Foundation for Basic Research with Government of Krasnoyarsk Territory, Krasnoyarsk Regional Fund of Science, the research project no. 19-42-240005: “Features of the Electronic Structure, Magnetic Properties, and Optical Excitations in Nanocrystals of Multifunctional Magnetic Chalcogenides Fe3S4 and FeSe” and the Russian Foundation for Basic Research and the Ministry of Science and Technology of Taiwan, joint projects nos. 19-52-52002 and 109-2112-M-153-003 and 108-2923-M-153-001-MY3The electron-microscopy study was carried out at the Laboratory of Electron Microscopy of the Center for Collective Use of the Siberian Federal University within the state assignment of the Ministry of Science and Higher Education of the Russian Federation (research code FSRZ-2020-0011). The magnetic measurements were carried out on a vibrating sample magnetometer at the Krasnoyarsk Regional Center for Collective Use, Krasnoyarsk Scientific Center, Siberian Branch, Russian Academy of Sciences
Аннотация: The effect of surfactants on the structure, morphology, and magnetic properties of FexSy iron-sulfide nanoparticles synthesized by thermal decomposition is studied. Oleylamine, hexadecylamine, and octadecylamine are used as surfactants. It is established by X-ray and electron-diffraction analysis combined with Mossbauer spectroscopy that, in samples 1 and 2 prepared using oleylamine and hexadecylamine, respectively, the Fe3S4 greigite phase dominates, with an inverse spinel structure isostructural to the iron oxide Fe3O4 magnetite with minor Fe9S11 impurities. Deviations in the distribution of iron cations over the tetrahedral and octahedral sites relative to the bulk greigite crystals are observed. The nanoparticles synthesized using octadecylamine (sample 3) are found to be multiphase with a greigite fraction of ~20%. In all three cases, as showed the results of transmission electron microscopy and Fourier transform infrared spectroscopy together with thermogravimetry analysis, the magnetic nanoparticles have an organic shell chemically bonded to their magnetic core, which prevents the agglomeration of the particles. This shell is much more massive in samples 2 and 3. The magnetization values for samples 1 and 2 are similar to those of greigite nanoparticles reported in publications, while the magnetization of sample 3 is several times lower, in accordance with the greigite fraction in it. The combination of fairly high magnetization with a massive organic shell allows one to consider hexadecylamine to be a promising surfactant for the synthesis of iron-sulfide nanoparticles protected from external impact and agglomeration.
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