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Библиотека института физики им. Л.В. Киренского СО РАН
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1.
Hysteretic behavior of
the magnetoresistance and the critical current of bulk Y3/4Lu1/4Ba2CU3O7+CuOcomposites in a magnetic field / D. A. Balaev [et al.]> // Physica C. - 2007. -
Vol. 460
: 8th International Conference on Materials and Mechanisms of Superconductivity and High Temperature Superconductors (JUL 09-14, 2006, Dresden, GERMANY). - P. 1307-1308,
DOI
10.1016/j.physc.2007.03.346. - Cited References: 7 . - ISSN 0921-4534
РУБ
Physics, Applied
Рубрики:
SUPERCONDUCTORS
Кл.слова (ненормированные):
HTSC
--
resistivity
--
magnetic field
--
relaxation
--
HTSC
--
Magnetic field
--
Relaxation
--
Resistivity
--
Crystallites
--
Magnetic fields
--
Magnetic hysteresis
--
Magnetoresistance
--
Yttrium barium copper oxides
--
Superconducting
crystallites
--
Superconducting systems
--
Tunnel-type Josephson junctions
--
Josephson junction devices
Аннотация:
The hysteretic behavior of critical current j(C)(H) and magneto-resistance R(H) of composites Y-Ba-Cu-O + CuO have been studied and presented. The composites represent the network of tunnel-type Josephson junctions where copper oxide acts as a material forming barriers between superconducting (YBCO)
crystallites
. The characteristic features of R(H) and j(C)(H) dependences are discussed in the frames of the conception of "two level superconducting system" (the Josephson media and HTSC
crystallites
) which is realized in the composites under study. (c) 2007 Elsevier B.V. All rights reserved.
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Держатели документа:
LV Kirenskii Inst Phys, Krasnoyarsk 660036, Russia
ИФ СО РАН
Kirensky Institute of Physics, Krasnoyarsk, 660036, Russian Federation
Доп.точки доступа:
Balaev, D. A.; Балаев, Дмитрий Александрович; Gokhfeld, D. M.; Гохфельд, Денис Михайлович; Popkov, S. I.; Попков, Сергей Иванович; Shaykhutdinov, K. A.; Шайхутдинов, Кирилл Александрович; Petrov, M. I.; Петров, Михаил Иванович
}
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2.
Time relaxation of
residual resistance of HTSC-based composites / D. A. Balaev [et al.]> // Physica C. - 2007. -
Vol. 460
: 8th International Conference on Materials and Mechanisms of Superconductivity and High Temperature Superconductors (JUL 09-14, 2006, Dresden, GERMANY). - P. 1309-1310,
DOI
10.1016/j.physc.2007.03.347. - Cited References: 5 . - ISSN 0921-4534
РУБ
Physics, Applied
Рубрики:
SUPERCONDUCTORS
Кл.слова (ненормированные):
granular HTSC
--
resistance
--
relaxation
--
magnetic flux
--
Granular HTSC
--
Magnetic flux
--
Relaxation
--
Resistance
--
Copper oxides
--
Crystallites
--
Magnetic flux
--
Magnetic relaxation
--
Magnetization
--
Yttrium barium copper oxides
--
Anderson-like relaxation processes
--
Flux trapping
--
Residual resistance
--
Time relaxation
--
Josephson junction devices
Аннотация:
Magnetoresistance curves R(H) and time relaxation of the residual resistance of bulk YBCO + CuO composites have been studied. These composites represent the network of Josephson junctions, where CuO acts as a barrier between YBCO grains. It has been shown that hysteresis of the R(H) dependences is related to the flux trapping within the YBCO
crystallites
. This flux induces magnetic field in the intergrain media. Time relaxation of the residual resistance is caused by relaxation of the magnetization of YBCO grains. The time dependence of the residual resistance obeys a logarithmic law, which describes the Anderson-like relaxation processes in the YBCO grains. (c) 2007 Elsevier B.V. All rights reserved.
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Держатели документа:
LV Kirenskii Inst Phys, Krasnoyarsk 660036, Russia
ИФ СО РАН
Kirensky Institute of Physics, Krasnoyarsk, 660036, Russian Federation
Доп.точки доступа:
Balaev, D. A.; Балаев, Дмитрий Александрович; Dubrovskiy, A. A.; Дубровский, Андрей Александрович; Shaykhutdinov, K. A.; Шайхутдинов, Кирилл Александрович; Popkov, S. I.; Попков, Сергей Иванович; Petrov, M. I.; Петров, Михаил Иванович
}
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3.
Preparation, microstructure, magnetic
and transport properties of bulk textured Bi(1.8)Pb(0.3)Sr(1.9)Ca(2)Cu(3)O(x) and Bi(1.8)Pb(0.3)Sr(1.9)Ca(2)Cu(3)O(x)+Agceramics / M. I. Petrov [et al.]> // Supercond. Sci. Technol. - 2008. -
Vol. 21
,
Is. 10
. - Ст. 105019,
DOI
10.1088/0953-2048/21/10/105019. - Cited References: 22. - This work is supported by program of RAS 'Quantum macrophysics' No. 3.4 and integration project of SB RAS No. 3.4 and in part by Krasnoyarsk Regional Scientific Foundation (KRSF), Grants 17G057, 18G148 and 18G011. DAB and AAD acknowledge the Russian Science Support Foundation. . - ISSN 0953-2048
РУБ
Physics, Applied + Physics, Condensed Matter
Рубрики:
HIGH-TEMPERATURE SUPERCONDUCTORS
CRITICAL-CURRENT DENSITY
BI-2223 TAPES
BI2223
SILVER
DISCS
(BI
Кл.слова (ненормированные):
Building materials
--
Calcium
--
Copper
--
Crystallites
--
Diamagnetic materials
--
Lead
--
Lead alloys
--
Magnetic anisotropy
--
Magnetic properties
--
Nanocrystalline alloys
--
Silver
--
Textures
--
Transport properties
--
Bi-2223
--
Bulk samples
--
Degree of textures
--
Diamagnetic responses
--
Liquid mediums
--
Magnetic and transport properties
--
Magnetic measurements
--
Room temperatures
--
Ceramic materials
Аннотация:
A new method of preparation of bulk textured Bi2223 ceramics and Bi2223 + Ag composites, based on room temperature pressing of foamed precursor (Bi2223, Bi2223 + Ag) in a liquid medium, is proposed. SEM and XRD data prove a high degree of texture of the bulk samples obtained. Magnetic measurements performed in directions H parallel to c-axis and H parallel to a-b-planes of Bi2223
crystallites
demonstrates anisotropy of magnetization confirming the texture of the ceramics. The materials obtained possess large diamagnetic response in the direction H parallel to a-b-planes of Bi2223
crystallites
at both 77.4 and 4.2 K.
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Держатели документа:
[Petrov, M. I.
Shaikhutdinov, K. A.
Balaev, D. A.
Dubrovskii, A. A.
Popkov, S. I.
Vasil'ev, A. D.] LV Kirenskii Inst Phys, Krasnoyarsk 660036, Russia
[Belozerova, I. L.] Reshetnev Siberian State Aerosp Univ, Krasnoyarsk, Russia
[Mart'yanov, O. N.] Boreskov Inst Catalysis, Novosibirsk 630090, Russia
ИФ СО РАН
Kirensky Institute of Physics, 660036, Krasnoyarsk, Russian Federation
Reshetnev Siberian State Aerospace University, Krasnoyarsk, Russian Federation
Boreskov Institute of Catalysis, 630090, Novosibirsk, Russian Federation
Доп.точки доступа:
Petrov, M. I.; Петров, Михаил Иванович; Belozerova, I. L.; Shaikhutdinov, K. A.; Шайхутдинов, Кирилл Александрович; Balaev, D. A.; Балаев, Дмитрий Александрович; Dubrovskii, A. A.; Дубровский, Андрей Александрович; Popkov, S. I.; Попков, Сергей Иванович; Vasil'ev, A. D.; Васильев, Александр Дмитриевич; Mart'yanov, O. N.
}
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4.
Magnetoresistance hysteresis of
bulk textured Bi1.8Pb0.3Sr1.9Ca2Cu3Ox + Ag ceramics and its anisotropy / D. A. Balaev [et al.]> // Physica C. - 2010. -
Vol. 470
,
Is. 1
. - P. 61-67,
DOI
10.1016/j.physc.2009.10.007. - Cited References: 24. - Authors thanks to I.L. Belozerova for help in preparation of textured ceramics. This work was supported by program N5 of RAS, project N7, and in part in frames of young scientist projects of Siberian Federal University, project N6. . - ISSN 0921-4534
РУБ
Physics, Applied
Рубрики:
CRITICAL-CURRENT ANISOTROPY
HIGH-TEMPERATURE SUPERCONDUCTOR
CRITICAL-CURRENT DENSITY
MAGNETIC HYSTERESIS
TAPES
FLUX
YBA2CU3O7-DELTA
FIELD
Кл.слова (ненормированные):
Magnetoresistance
--
Anisotropy
--
Scaling
--
Magnetization
--
Bi2223
--
BSCCO
--
Anisotropy
--
Bi2223
--
BSCCO
--
Magnetization
--
Magnetoresistance
--
Scaling
--
Bi-2223
--
BSCCO
--
External fields
--
Granular superconductors
--
Magnetic induction
--
Parameters characterizing
--
Anisotropy
--
Calcium
--
Ceramic materials
--
Crystallites
--
Electric resistance
--
Hysteresis
--
Lead
--
Magnetic moments
--
Magnetoelectronics
--
Magnetoresistance
--
Nanocrystalline alloys
--
Silver
--
Superconducting materials
--
Superconductivity
--
Magnetic field effects
Аннотация:
Magnetoresistance of bulk textured Bi1.8Pb0.3Sr1.9Ca2Cu3Ox + Ag ceramics has been studied in the magnetic fields applied parallel and perpendicular to a-b planes of Bi2223
crystallites
. Besides well known anisotropy of magnetoresistance of textured superconductors (R-H parallel to c > RH parallel to a-b), anisotropic hysteresis of R(H) dependences was investigated. Parameters characterizing hysteretic R(H) curves differ for the cases H parallel to c and H parallel to a-b. This behavior is explained within the model of a granular superconductor where the total magnetic induction in the intercrystallite boundaries is superposition of the external field and the magnetic field induced by dipole magnetic moments of neighbor
crystallites
. (C) 2009 Elsevier B.V. All rights reserved.
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Держатели документа:
[Gokhfeld, D. M.] RAS, SD, LV Kirensky Phys Inst, High Magnet Fields Lab, Krasnoyarsk 660036, Russia
[Balaev, D. A.
Semenov, S. V.
Shaykhutdinov, K. A.] Siberian Fed Univ, Krasnoyarsk 660041, Russia
ИФ СО РАН
L.V. Kirensky Institute of Physics, Krasnoyarsk, 660036, Russian Federation
Siberian Federal University, Krasnoyarsk, 660041, Russian Federation
Доп.точки доступа:
Balaev, D. A.; Балаев, Дмитрий Александрович; Popkov, S. I.; Попков, Сергей Иванович; Semenov, S. V.; Семенов, Сергей Васильевич; Bykov, A. A.; Быков, Алексей Анатольевич; Shaykhutdinov, K. A.; Шайхутдинов, Кирилл Александрович; Gokhfeld, D. M.; Гохфельд, Денис Михайлович; Petrov, M. I.; Петров, Михаил Иванович
}
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5.
Изотов, Андрей Викторович
.
Численное моделирование магнитной микроструктуры тонких нанокристаллических пленок со случайным распределением осей / А. В. Изотов, Б. А. Беляев, Н. М. Боев> // Изв. вузов. Физика. - 2013. -
Т. 56
,
№ 8/2
. - С. 213-216. - Работа выполнена при финансовой поддержке Министерства образования и науки РФ, Госконтракт № 14.513.11.0010, и ФЦП «Научные и научно-педагогические кадры инновационной России 2009−2013 гг.»
Перевод заглавия:
Numerical modeling of the magnetic microstructure of thin nanocrystalline films with a random distribution of the easy magnetization axis in
crystallites
Кл.слова (ненормированные):
микромагнитное моделирование
--
«рябь» намагниченности
--
магнитная микроструктура
--
хаотическая анизотропия
--
нанокристаллиты
--
micromagnetic simulation
--
magnetization ripple
--
magnetic microstructure
--
random anisotropy
--
nanocrystallites
Аннотация:
На основе численного анализа микромагнитной модели нанокристаллической пленки со случайным распределением направлений одноосной магнитной анизотропии в кристаллитах исследована тонкая магнитная микроструктура типа «ряби» намагниченности. Приводится сравнение полученных результатов с результатами теоретических исследований.
The fine magnetic microstructure of the magnetization "ripple" was studied by a numerical analysis of micromagnetic model of nanocrystalline films with a random distribution of directions of the uniaxial magnetic anisotropy in
crystallites
. Obtained results were compared with the results of theoretical studies.
Держатели документа:
Институт физики им. Л.В. Киренского СО РАН
Доп.точки доступа:
Беляев, Борис Афанасьевич; Belyaev, B. A.; Боев, Н. М.; Izotov A.V.
}
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6.
Aver'yanov, E. M.
Influence of the dimension of a polycrystalline film and the optical anisotropy of
crystallites
on the effective dielectric constant of the film / E. M. Aver’yanov> // Phys. Solid State. - 2016. -
Vol. 58
,
Is. 8
. - P. 1634-1641,
DOI
10.1134/S1063783416080035. - Cited References: 41 . - ISSN 1063-7834
РУБ
Physics, Condensed Matter
Рубрики:
EFFECTIVE REFRACTIVE-INDEX
CONJUGATED POLYMER
POLY(P-PHENYLENE VINYLENE)
SPECTROSCOPIC ELLIPSOMETRY
ELECTRICAL-CONDUCTIVITY
LOCAL-FIELD
THIN-FILMS
DISPERSION
POLYFLUORENE
DEVICES
Аннотация:
The dimension D of a polycrystalline film and the optical anisotropy m = εz/εx of uniaxial
crystallites
with the principal components εx = εy and εz of the tensor of the dielectric constant have been shown to produce a strong influence on the effective dielectric constant εD* and the effective refractive index nD* = (εD*)1/2 of the film in the optical transparency region, as well as on the boundaries of the intervals BDl ≤ εD* ≤ BDu. The intervals Δ2(m) = B2l–B2u and Δ3(m) = B3l–B3u are separated by a gap for m in the range 1 m 2, whereas the theoretical dependence ε2*(m) is separated by a gap from the interval Δ3(m) for m in the range 1 m 4. This is confirmed by a comparison of the experimental (noP) and theoretical (nD*) ordinary refractive indices for uniaxial polycrystalline films of the conjugated polymer poly(p-phenylene vinylene) (PPV) with uniaxial
crystallites
and appropriate values of m. In the visible transparency region of the PPV films with a change in m(λ) in the range 2 m(λ) 3 due to the dependence of the components εx,z(λ) on the light wavelength λ, the refractive indices noP2(λ) 3 near the electronic absorption band of the
crystallites
, the values of εoP(λ) lie in the region of the overlap of the intervals Δ2(m) and Δ3(m). The boundaries mc of the range 1 m mc are determined, for which the interval Δ2(m) is separated by a gap from the dependences ε3*(m) corresponding to the effective medium theory with spherical
crystallites
and hierarchical models of a polycrystal, as well as from the proposed new dependence ε3*(m).
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Публикация на русском языке
Аверьянов, Евгений Михайлович. Влияние размерности поликристаллической пленки и оптической анизотропии кристаллитов на эффективную диэлектрическую проницаемость пленки [Текст] / Е. М. Аверьянов // Физ. тверд. тела : Физико-технический институт им. А. Ф. Иоффе РАН, 2016. - Т. 58 Вып. 8. - С. 1580–1586
Доп.точки доступа:
Аверьянов, Евгений Михайлович
}
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7.
Ivanov, A. A.
On features of magnetization self-organization in 1D stochastic ferromagnetic systems / A. A. Ivanov, V. A. Orlov> // Eur. Phys. J. B. - 2017. -
Vol. 90
,
Is. 3
. - Ст. 40,
DOI
10.1140/epjb/e2017-70531-0. - Cited References: 31. - Sections 2, 4–6 of the work was supported by Russian Foundation for Basic Research (RFBR), Project No. 17-02-00254-a. Section 3 was supported by Russian Science Foundation, Project No. 14-15-00805. . - ISSN 1434-6028
Перевод заглавия:
Об особенностях самоорганизация намагниченности в 1D ферромагнитных стохастических системах
Кл.слова (ненормированные):
Anisotropy
--
Crystallites
--
Crystallography
--
Magnetization
--
Magnetostatics
--
Characteristic length
--
Crystallographic anisotropy
--
Experimental techniques
--
Ferromagnetic systems
--
Magnetostatic interactions
--
Polycrystalline nanowires
--
Self organizations
--
Stochastic domains
--
Stochastic systems
Аннотация:
The magnetic structure of a polycrystalline nanowire at the weak or missing magnetostatic interaction exhibits the special self-organization of magnetization. As is known, the magnetization structure forming in a random crystallographic anisotropy field has a characteristic length range, which involves tens and hundreds of
crystallites
. This leads to the occurrence of stochastic domains. The induced uniform anisotropy of magnetostatic nature or the texture co-directed with the crystallite anisotropy axes masks the picture of stochastic domains. Nevertheless, as we show, the information on stochastic domains remains in the magnetization structure. The experimental techniques for obtaining information on the magnetic properties of stochastic domains are proposed.
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Держатели документа:
Siberian Federal University, pr. Svobodny 79, Krasnoyarsk, Russian Federation
Kirensky Institute of Physics Federal Research Center KSC Siberian Branch Russian Academy of Sciences, Krasnoyarsk, Russian Federation
Krasnoyarsk State Pedagogical University named after V.P. Astafev, ul. Ady Lebedevoi 89, Krasnoyarsk, Russian Federation
Доп.точки доступа:
Orlov, V. A.; Орлов, Виталий Александрович
}
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8.
Magnetic resonance studies
of mixed chalcospinel CuCr2SxSe4−x (x = 0; 2) and CoxCu1−xCr2S4 (x = 0.1; 0.2) nanocrystals with strong interparticle interactions / A. I. Pankrats [et al.]> // J. Magn. Magn. Mater. - 2018. -
Vol. 452
. - P. 297-305,
DOI
10.1016/j.jmmm.2017.12.092. - Cited References: 31. - The authors thank D.A. Balaev for fruitful and useful discussions. The work at the University of Alabama was supported by the National Science Foundation, United States under Grant No. CHE-1508259. . - ISSN 0304-8853
Кл.слова (ненормированные):
Freezing temperatures
--
Individual nanoparticles
--
Inhomogeneous broadening
--
Inter-particle interaction
--
Magnetic dipolar field
--
Magnetic resonance spectra
--
Nano-sized
crystallites
--
Resonance characteristic
Аннотация:
Magnetic resonance characteristics of mixed chalcospinel nanocrystals CuCr2SxSe4−x (x = 0 and 2) and CoxCu1−xCr2S4 (x = 0.1 and 0.2) have been investigated. It has been established based on TEM, SEM and resonance data that all the samples contain both blocks with sizes from 1 to 50 m of compacted nanosized
crystallites
and individual nanoparticles with sizes from 10 to 30 nm. The studies provide evidence of strong interparticle interaction in all the samples leading to high values of the blocking temperature. Magnetic dipolar field arise in the boundary regions of interacting adjacent nanocrystals below the blocking temperature. This results in inhomogeneous broadening of the magnetic resonance spectrum along with appearance of additional absorption lines. With increase in magnetic anisotropy at low temperatures, a shift of the resonance field along with line broadening are observed for all the studied compounds due to freezing of the moments in the nanoparticles, both in the individual and compacted ones. A gapped characteristic of the resonance spectrum is established below the freezing temperature Tfr, with the energy gap defined by the averaged magnetic anisotropy
. Anionic substitution of sulfur by selenium results in a decrease in the magnetic anisotropy. In contrast, cationic substitution of copper by cobalt increases the magnetic anisotropy due to a strong contribution from the latter ion.
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Держатели документа:
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, Russian Federation
Siberian Federal University, Krasnoyarsk, Russian Federation
UbiQD, LLC, 134 Eastgate Dr, Los Alamos, NM, United States
MINT Center, The University of Alabama, Tuscaloosa, AL, United States
Доп.точки доступа:
Pankrats, A. I.; Панкрац, Анатолий Иванович; Vorotynov, A. M.; Воротынов, Александр Михайлович; Tugarinov, V. I.; Тугаринов, Василий Иванович; Zharkov, S. M.; Жарков, Сергей Михайлович; Zeer, G. M.; Ramasamy, K.; Gupta, A.
}
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9.
Orlov, V. A.
Interaction of a Magnetic Vortex with Magnetic Anisotropy Nonuniformity / V. A. Orlov, G. S. Patrin, I. N. Orlova> // J. Exp. Theor. Phys. - 2020. -
Vol. 131
,
Is. 4
. - P. 589-599,
DOI
10.1134/S1063776120090071. - Cited References: 51. - This study was supported by the Russian Foundation for Basic Research (project no. 18-02-00161) . - ISSN 1063-7761
Кл.слова (ненормированные):
Crystallites
--
Defects
--
Equations of motion
--
Magnetism
--
Plasma theory
--
Vortex flow
Аннотация:
The problem of propagation of a magnetic inhomogeneity in the form of a magnetic vortex near a defect simulated by a crystallite with uniaxial anisotropy has been solved theoretically. The defect (crystallite) is implanted into a homogeneous 2D ferromagnetic matrix. Apart from the anisotropy energy, the term responsible for the existence of a centrosymmetric potential is included into the total energy. For calculations, we have used the method of collective variables (Thiele equation). We have considered the variants of bidirectional and unidirectional anisotropy of the crystallite. Analysis of the equations of motion for different directions of the anisotropy axis of the implanted defect has revealed the variety in the behavior of the vortex core as a quasiparticle. The vortex core can be trapped by the defect with equilibrium position of the vortex at rest directly on the crystallite or during its motion at a certain distance from it. It is shown that for a small damping parameter and in the case when the defect anisotropy axis lies in the plane of the magnet, the vortex moves so as if its core experiences the action of the repulsive axially symmetric potential.
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Публикация на русском языке
Орлов, Виталий Александрович. Взаимодействие магнитного вихря с неоднородностью магнитной анизотропии [Текст] / В. А. Орлов, Г. С. Патрин, И. Н. Орлова // Журн. эксперим. и теор. физ. - 2020. - Т. 158 Вып. 4. - С. 672-683
Держатели документа:
Siberian Federal University, Krasnoyarsk, 660041, Russian Federation
Kirensky Institute of Physics, Federal Research Center “Krasnoyarsk Scientific Center,” Siberian Branch, Russian Academy of Sciences, Krasnoyarsk, 660036, Russian Federation
Astaf’ev Krasnoyarsk State Pedagogical University, Krasnoyarsk, 660049, Russian Federation
Доп.точки доступа:
Patrin, G. S.; Патрин, Геннадий Семёнович; Orlova, I. N.; Орлов, Виталий Александрович
}
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10.
Moiseenko, E. T.
In situ electron diffraction and resistivity characterization of solid state reaction process in Cu/Al bilayer thin films / E. T. Moiseenko, R. R. Altunin, S. M. Zharkov> // Metall. Mat. Trans. A. - 2020. -
Vol. 51
,
Is. 3
. - P. 1428-1436,
DOI
10.1007/s11661-019-05602-5. - Cited References: 52. - The authors wish to thank the financial support from the Russian Science Foundation (Grant #18-13-00080) . - ISSN 1073-5623
Перевод заглавия:
In situ исследования процесса твердофазной реакции в двухслойных тонких пленках Cu/Al методами дифракции электронов и изменения электросопротивления
Кл.слова (ненормированные):
Aluminum alloys
--
Binary alloys
--
Crystallites
--
Electric conductivity
--
Electron diffraction
--
Intermetallics
--
Solid state reactions
--
Thin films
Аннотация:
Solid state reaction processes in Cu/Al thin films have been studied using the methods of in situ electron diffraction and electrical resistivity measurements. The solid state reaction in the Cu/Al thin films has been found to begin already at 88 °C with the formation of the Al2Cu phase in the process of thermal heating in vacuum. The phase sequence at the solid state reaction in the films under study has been determined to be the following: Al2Cu → AlCu → Al4Cu9. A model has been suggested for describing the initial formation stage of intermetallic compounds at the solid state reaction in Cu/Al thin films. According to this model, at the initial stage, the intermetallic compounds are formed as separate
crystallites
at the interface in the Cu/Al thin films. The suggested model can be applied both to the formation of the first phase, Al2Cu, and to the subsequent phases: AlCu and Al4Cu9. For the Al4Cu9 phase the temperature coefficient of the electrical resistivity has been determined to be equal to αAl4Cu9= 1.1 × 10−3 K−1.
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Держатели документа:
Siberian Federal University, 79 Svobodny pr., Krasnoyarsk, 660041, Russian Federation
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Akademgorodok 50/38, Krasnoyarsk, 660036, Russian Federation
Доп.точки доступа:
Altunin, R. R.; Zharkov, S. M.; Жарков, Сергей Михайлович
}
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11.
Superparamagnetic blocking and
magnetic interactions in nanoferrihydrite adsorbed on biomineralized nanorod-shaped F3S4
crystallites
/ Y. V. Knyazev, O. P. Ikkert, S. V. Semenov [et al.]> // J. Alloys Compd. - 2022. -
Vol. 923
. - Ст. 166346,
DOI
10.1016/j.jallcom.2022.166346. - Cited References: 109. - This study was supported by the Russian Science Foundation, project no. 22-24-00601 (https://rscf.ru/project/22–24–00601/). - The electron microscopy and Mössbauer spectroscopy studies were carried out on the equipment of the Krasnoyarsk Territorial Center for Collective Use, Krasnoyarsk Scientific Center, Siberian Branch of the Russian Academy of Sciences. We thank Dr. Ivan Nemtsev for the SEM images. The contribution of M. P. (development of methodology of sample preparation for EXAFS measurements) was partially supported by the Russian Ministry of Science and Higher Education via the budget project of SRF SKIF, Boreskov Institute of Catalysis . - ISSN 0925-8388
Кл.слова (ненормированные):
Biomineralization
--
Superparamagnetic nanoparticles
--
Interparticle interactions
--
Iron sulfide
--
Ferrihydrite
Аннотация:
A composite based on nanorod-shaped greigite (Fe3S4)
crystallites
with adsorbed ferrihydrite (Fe2O3 ‧ nH2O) nanoparticles has been synthesized. The synthesis has been performed by biomineralization of the bacterial wall of a sulfate-reducing Desulfovibrio sp. A2 bacteria. The phase composition of the synthesized composite has been investigated by X-ray powder and electron diffraction, as well as Fourier-transform infrared, extended X-ray absorption fine structure, and Mössbauer spectroscopy. The magnetic measurement data have shown that the sample under study contains two magnetic phases: multidomain nanorod-shaped greigite and ultrasmall ferrihydrite nanoparticles. The constant atomic fraction of the greigite crystalline phase in the range of 4–300 K (~20%) revealed by Mössbauer spectroscopy is indicative of a blocked magnetic moment of nanorod-shaped Fe3S4. It is shown that nanorod-shaped Fe3S4
crystallites
are strongly magnetically bound with adsorbed Fe2O3 ‧ nH2O (Eint ~ 1200kB) nanoparticles. This significantly slows down the superparamagnetic relaxation of the magnetic moments of ferrihydrite nanoparticles. Therefore, the blocking temperature noticeably increases and attains, according to the Mössbauer spectroscopy data, a value of TB = 140 K (the magnetic measurements yield TB = 72 K). The processes of superparamagnetic blocking of the magnetic moments of ferrihydrite nanoparticles manifest themselves in the evolution of the magnetic properties of the investigated sample (a significant increase in the coercivity and remanent magnetization). In support of the Mössbauer spectroscopy data, a sufficiently high superparamagnetic blocking temperature has been established, which discloses the effect of magnetizing of ferrihydrite nanoparticles by coarser greigite formations, analogously to the effect of interparticle magnetic interactions.
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Держатели документа:
Kirensky Institute of Physics, Federal Research Center KSC SB RAS, Krasnoyarsk, 660036, Russian Federation
Department of Plant Physiology, Biotechnology, and Bioinformatics, Tomsk State University, Tomsk, 634050, Russian Federation
Siberian Federal University, Krasnoyarsk, 660041, Russian Federation
Synchrotron radiation facility SKIF, Boreskov Institute of Catalysis SB RAS, Kol'tsovo, 630559, Russian Federation
National Research Center “Kurchatov Institute”, Moscow, 123182, Russian Federation
Доп.точки доступа:
Knyazev, Yu. V.; Князев, Юрий Владимирович; Ikkert, O. P.; Semenov, S. V.; Семёнов, Сергей Васильевич; Volochaev, M. N.; Волочаев, Михаил Николаевич; Molokeev, M. S.; Молокеев, Максим Сергеевич; Platunov, M. S.; Платунов, Михаил Сергеевич; Khramov, E. V.; Dubrovskiy, A. A.; Дубровский, Андрей Александрович; Shestakov, N. P.; Шестаков, Николай Петрович; Smorodina, E. D.; Karnachuk, O. V.; Balaev, D. A.; Балаев, Дмитрий Александрович
}
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