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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Aleksandrov K. S., Flerov I. N., Bovina A. F., Voronov V. N., Горев, Михаил Васильевич, Melnikova S. V., Misjul S. V.
Заглавие : Study of phase transitions in single crystals with elpasolite structure
Коллективы : European Meeting on Ferroelectricity
Место публикации : European Meeting on Ferroelectricity (5 ; 1983 ; Sept. ; 26-30 ; Malaga, Sp). Ferroelectrics. - 1983. - Vol. 54, Is. 1. - P.577-580. - ISSN 0015-0193
Ключевые слова (''Своб.индексиров.''): crystals - structure--elpasolite structure--phase transistions--ferroelectric materials
Аннотация: Structural distortions and physical properties of some fluorides with the elpasolite structure were studied. Different types of distortions at ferroelastic phase transitions for fluorides and chlorides are discussed.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Aleksandrov K. S., Flerov I. N., Bovina A. F., Voronov V. N., Gorev M. V., Melnikova S. V., Misjul S. V.
Заглавие : The study of phase-transitions in single-crystals with elpasolite structure
Разночтения заглавия :Загл. в ист.: The study op phase transitions
Место публикации : Ferroelectrics: GORDON BREACH SCI PUBL LTD, 1984. - Vol. 54, Is. 1. - P.237/577-240/580. - ISSN 0015-0193, DOI 10.1080/00150198408215859
Примечания : Cited References: 7. - В WoS указаны стр. 577-580
Аннотация: Structural distortions and physical properties of some fluorides with the elpasolite structure were studied. Different types of distortions at ferroelastic phase transitions for fluorides and chlorides are discussed.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Aleksandrov K. S., Melnikova S. V., Misyul S. V.
Заглавие : Successive phase-transitions in ferroelastic cs2rbdyf6 with elpasolite-type structure
Место публикации : Phys. Status Solidi A. - 1987. - Vol. 104, Is. 2. - P.545-548. - ISSN 0031-8965, DOI 10.1002/pssa.2211040205
Примечания : Cited References: 6
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Flerov I. N., Gorev M. V., Melnikova S. V., Misyul S. V., Voronov V. N., Aleksandrov K. S.
Заглавие : Phase-transitions in elpasolite Rb2KSCF6
Место публикации : Fiz. Tverd. Tela. - 1992. - Vol. 34, Is. 7. - P.2185-2195. - ISSN 0367-3294
Примечания : Cited References: 24
Предметные рубрики: RB2KMIIIF6 ELPASOLITES
CS2NANDCL6
SCATTERING
RB2NADYF6
CS2RBDYF6
RB2KDYF6
CRYSTAL
MODE
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Zinenko V. I., Zamkova N. G., Sofronova S. N.
Заглавие : Lattice dynamics of K2NaAlF6, K3AlF6, and Na3AlF6 crystals with the elpasolite structure
Место публикации : J. Exp. Theor. Phys.: AMER INST PHYSICS, 1998. - Vol. 87, Is. 5. - P944-951. - ISSN 1063-7761, DOI 10.1134/1.558743
Примечания : Cited References: 10
Аннотация: This paper presents the results of a nonempirical calculation of the static and dynamic properties of K2NaAlF6, K3AlF6, and Na3AlF6 crystals with the elpasolite structure. The calculation is based on a microscopic model of an ionic crystal that allows for the deformability and polarizability of the ions. The deformability parameters of the ions are determined by minimizing the total energy of the crystal. The total energy is regarded as a functional of the electron density, using the local Thomas-Fermi approximation and taking into account exchange (correlation) effects. The results of the calculations of the equilibrium lattice parameters and of the permittivities are in good agreement with the experimental data. Unstable vibrational modes are found in the spectrum of the lattice vibrations, with these modes occupying the phase space in the entire Brillouin zone. (C) 1998 American Institute of Physics. [S1063-7761(98)01311-0].
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Flerov I. N., Gorev M. V., Sciau P.
Заглавие : Specific heat of the elpasolite Pb2MgWO6
Место публикации : Phys. Solid State: AMER INST PHYSICS, 1999. - Vol. 41, Is. 9. - P1544-1546. - ISSN 1063-7834, DOI 10.1134/1.1131020
Примечания : Cited References: 12
Предметные рубрики: PEROVSKITE PB2MGWO6
Аннотация: The specific heat of Pb2MgWO6 has been measured in the temperature interval 83-370 K. An anomaly in the specific heat associated with the phase transition at T-0=312.8 K has been discovered. The thermodynamic parameters of the structural phase transition Fm3m-Pmcn have been determined. (C) 1999 American Institute of Physics. [S1063-7834(99)03209-8].
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Flerov I. N., Gorev M. V., Afanas'ev M. L., Ushakova T. V.
Заглавие : Thermodynamic properties of (NH4)(2)KGaF6 elpasolite
Разночтения заглавия :авие SCOPUS: Thermodynamic properties of (NH4)2KGaF6 elpasolite
Место публикации : Phys. Solid State: AMER INST PHYSICS, 2001. - Vol. 43, Is. 12. - P2301-2306. - ISSN 1063-7834, DOI 10.1134/1.1427960
Примечания : Cited References: 19
Предметные рубрики: NUCLEAR MAGNETIC-RESONANCE
PHASE-TRANSITIONS
CRYOLITE (NH4)(3)SCF6
MOTIONS
F-19
H-1
Аннотация: The heat capacity of (NH4)(2)KGaF6 elpasolite is measured in the temperature range from 80 to 350 K. A sequence of three phase transitions at T-1 = 288.5 K, T-2 = 250 K, and T-3 = 244.5 K is revealed, and the thermodynamic characteristics of these transitions are determined. The influence of hydrostatic pressure on the phase transition temperature is investigated. The results obtained are discussed within the model of orientational ordering of NH4+ and GaF63- ionic groups. (C) 2001 MAIK "Nauka/Interperiodica".
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Vtyurin A. N., Bulou A., Krylov A. S., Voronov V. N.
Заглавие : Soft-mode condensation in Raman spectra of the Rb2KScF6 elpasolite
Место публикации : Phys. Solid State: AMER INST PHYSICS, 2001. - Vol. 43, Is. 11. - P2154-2157. - ISSN 1063-7834, DOI 10.1134/1.1417197
Примечания : Cited References: 11
Предметные рубрики: STRUCTURAL PHASE-TRANSITION
SCATTERING
Аннотация: This paper reports on the first observation of soft-mode condensation in the Raman spectra of the Rb2KScF6 elpasolite crystal below the transition points from the cubic to tetragonal and, subsequently, monoclinic phase. (C) 2001 MAIK "Nauka/Interperiodica".
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Gorev M. V., Flerov I. N., Sciau P.
Заглавие : Heat capacity and the p-T phase diagram of Pb2MgTeO6 elpasolite
Место публикации : Phys. Solid State: AMER INST PHYSICS, 2001. - Vol. 43, Is. 2. - P345-349. - ISSN 1063-7834, DOI 10.1134/1.1349486
Примечания : Cited References: 17
Предметные рубрики: ORDERED PEROVSKITE PB2MGTEO6
CRYSTAL-STRUCTURE
PB2COWO6
PB2MGWO6
Аннотация: The heat capacity of Pb2MgTeO6 is measured in the temperature range 80-300 K. It is found that the heat capacity exhibits an anomaly associated with the phase transition at T-0 = 186.9 K. The thermodynamic parameters of the structural transformation are determined. The effect of hydrostatic pressure up to 0.5 GPa on the phase transition temperature is examined. (C) 2001 MAIK "Nauka/Interperiodica".
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Gorev M. V., Flerov I. N., Tressaud A., Durand E.
Заглавие : The p-T phase diagram of ammonium hexafluoroaluminate
Место публикации : J. Phys.: Condens. Matter: IOP PUBLISHING LTD, 2002. - Vol. 14, Is. 25. - P6447-6453. - ISSN 0953-8984, DOI 10.1088/0953-8984/14/25/312
Примечания : Cited References: 17
Предметные рубрики: NUCLEAR MAGNETIC-RESONANCE
TRANSITIONS
MOTIONS
F-19
H-1
Ключевые слова (''Своб.индексиров.''): entropy--hydrostatic pressing--mathematical models--order disorder transitions--phase diagrams--specific heat of solids--ammonium hexafluoroaluminate--crolite--elpasolite--ammonium compounds
Аннотация: The heat capacity and the effect of hydrostatic pressure on structural phase transitions in ammonium hexafluoroaluminate, (NH4)(3)AlF6, have been studied. Two heat capacity anomalies have been found with maxima at T-1 = 218.5 +/- 0.5 K and T-2 = 179 +/- 2 K. Respective entropy changes of phase transitions are DeltaS(1) = 15.3 +/- 0.5 J mol(-1) K-1 and DeltaS(2) = 2.5 +/- 0.5 J mol(-1) K-1. It is shown that the p-T phase diagram of this compound is rather complex and contains a triple point (p(tp) = 0.12 GPa, T-tp = 221 K) and high-pressure phase. The mechanism of transformations and generalized p-T phase diagram for compounds of the (NH4)(3)(MF6)-F-III family are discussed within the framework of the rotational order-disorder model.
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11.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Flerov I. N., Burriel R., Gorev M. V., Isla P., Voronov V. N.
Заглавие : Low-temperature specific heat of the Rb2KScF6 elpasolite
Место публикации : Phys. Solid State: AMER INST PHYSICS, 2003. - Vol. 45, Is. 1. - P167-170. - ISSN 1063-7834, DOI 10.1134/1.1537430
Примечания : Cited References: 9
Предметные рубрики: PHASE-TRANSITIONS
CRYOLITE (NH4)(3)SCF6
DISTORTED PHASES
SYMMETRY
Аннотация: The specific heat of single-crystal Rb2KScF6 is measured using ac calorimetry in the range 4-280 K. The results are discussed in the context of a group-theoretical analysis of possible distortions of the elpasolite structure and of experimental data obtained earlier with an adiabatic calorimeter in a narrower temperature region. (C) 2003 MAIK "Nauka/Interperiodica".
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12.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Krylov A. S., Vtyurin A. N., Bulou A., Voronov V. N.
Заглавие : Raman spectra and phase transitions in the Rb2KScF6 elpasolite
Коллективы : Russian-CIS-Baltic-Japanese symposium on ferroelectricity
Место публикации : Ferroelectrics: Taylor & Francis LTD, 2003. - Vol. 284. - P221-238. - ISSN 0015-0193, DOI 10.1080/00150190390204709
Примечания : Cited References: 13
Предметные рубрики: LIGHT-SCATTERING
OPTICAL PHONONS
MODE
Ключевые слова (''Своб.индексиров.''): rb2kscf6--phase transitions--raman scattering--soft modes
Аннотация: Raman spectra of Rb2KScF6 elpasolite crystal have been studied in a wide temperature range, including two transition points: from cubic to tetragonal, and then-to the monoclinic phase. For the first time both for this crystal and for fluoride elpasolites in general soft modes restoration has been found below transition points; in agreement with selection rules a splitting of degenerate modes has been observed as well both for lattice vibrations and internal modes of ScF6 octahedrons. Parameters of Raman lines have been quantitatively analyzed and found in good agreement with known thermodynamic characteristics of these transitions; in particular, lines widths are shown to be determined by tree-phonons anharmonic interactions. A wide region of pretransitional fluctuations was found above the upper transition point.
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13.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Krylova S. N., Vtyurin A. N., Bulou A., Krylov A. S., Zamkova N. G.
Заглавие : Lattice dynamics and raman scattering spectrum of elpasolite Rb2KScF6: Comparative analysis
Разночтения заглавия :авие SCOPUS: Lattice dynamics and Raman scattering spectrum of elpasolite Rb 2KScF6: Comparative analysis
Место публикации : Phys. Solid State: MAIK NAUKA/INTERPERIODICA/SPRINGER, 2004. - Vol. 46, Is. 7. - P1311-1319. - ISSN 1063-7834, DOI 10.1134/1.1778457
Примечания : Cited References: 18
Предметные рубрики: STRUCTURAL PHASE-TRANSITION
LIGHT-SCATTERING
OPTICAL PHONONS
SOFT-MODE
CRYSTAL
Аннотация: Raman scattering spectra of elpasolite Rb2KScF6 are studied in a wide temperature range including two phase transitions: from the cubic to the tetragonal phase and then to the monoclinic phase. The experimental Raman scattering spectrum is compared with the lattice vibration spectra of these phases calculated using an ab initio approach. A number of anomalies (caused by structural rearrangement during the phase transitions) are revealed and quantitatively analyzed in the ranges of both the intramolecular vibrations of the octahedron molecular ScF6 ions and low-frequency intermolecular lattice vibrations. The interaction between low-frequency intramolecular vibrations and the intermolecular modes is found to be significant, and strong resonance interaction of the rotational soft modes (which are recovered below the phase transition points) with hard low-frequency vibrations of the rubidium ion sublattice is detected. These interactions are shown to substantially complicate the spectra. (C) 2004 MAIK "Nauka / Interperiodica".
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14.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Flerov I. N., Gorev M. V., Fokina V. D., Bovina A. F., Laptash N. M.
Заглавие : Calorimetric and x-ray diffraction studies of the (NH4)(3)WO3F3 and (NH4)(3)TiOF5 perovskite-like oxyfluorides
Разночтения заглавия :авие SCOPUS: Calorimetric and X-ray diffraction studies of the (NH4)3WO 3F3 and (NH4)3TiOF5 perovskite-like oxyfluorides
Место публикации : Phys. Solid State: AMER INST PHYSICS, 2004. - Vol. 46, Is. 5. - P915-921. - ISSN 1063-7834, DOI 10.1134/1.1744971
Примечания : Cited References: 11
Предметные рубрики: PHASE-TRANSITIONS
ELPASOLITE
K3MOO3F3
Аннотация: The heat capacity and unit cell parameters of the (NH4)(3)WO3F3 and (NH4)(3)TiOF5 perovskite-like oxyfluorides were measured in the temperature interval from 80 to 300 K; the existence of two and one phase transitions in these compounds, respectively, was demonstrated, and their thermodynamic parameters were determined. The effect of a hydrostatic pressure of up to 0.5 GPa on the phase transition temperatures was studied. Triple points and high-pressure phases were found in the T vs. p diagrams. An analysis of entropy changes suggests that all the structural transformations revealed are associated with the ordering of structural blocks. (C) 2004 MAIK "Nauka / Interperiodica".
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15.

16.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Flerov I. N., Gorev M. V., Aleksandrov K. S., Tressaud A., Fokina V. D.
Заглавие : Ferroelastic phase transitions in fluorides with cryolite and elpasolite structures
Место публикации : Crystallogr. Rep. - 2004. - Vol. 49, Is. 1. - P.100-107. - ISSN 1063-7745, DOI 10.1134/1.1643969
Примечания : Cited References: 43
Предметные рубрики: NUCLEAR MAGNETIC-RESONANCE
THERMODYNAMIC PROPERTIES
RB2KMIIIF6 ELPASOLITES
NEUTRON-DIFFRACTION
CRYSTALS
PEROVSKITES
DIAGRAM
SC
RB2KGAXSC1-XF6
SCATTERING
Аннотация: The ferroelastic phase transitions are investigated in several series of fluoride crystals belonging to the elpasolite and cryolite families (space group Fm (3) over barm) with the general formula A(2)BB'F-6. The influence of the size and shape of cations and anions on the entropy and the mechanism of structural distortions is discussed. (C) 2004 MAIK "Nauka/Interperiodica".
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17.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Flerov I. N., Gorev M. V., Fokina V. D., Bovina A. F., Molokeev M. S., Boiko Y. V., Voronov V. N., Kocharova A. G.
Заглавие : Structural phase transition in elpasolite-like (NH4)(2)KWO3F3
Разночтения заглавия :авие SCOPUS: Structural phase transition in elpasolite-like (NH4) 2KWO3F3
Место публикации : Phys. Solid State: SPRINGER, 2006. - Vol. 48, Is. 1. - P106-112. - ISSN 1063-7834, DOI 10.1134/S1063783406010215
Примечания : Cited References: 16
Аннотация: A new chemical compound, (NH4) 2KWO3 F-3, was synthesized. The Rietveld-refined crystal structure was found to be cubic at room temperature and to belong to the elpasolite family (space group). The heat capacity and unit cell parameters were studied within a broad temperature range. A second-order phase transition was found to occur at 235.4 K and to be well described in terms of phenomenological theory. Hydro-static pressure broadens the temperature interval of stability of the cubic phase (dT(0)/dp = -10.8K GPa(-1)). A possible model of structural ordering based on a comparison of the entropy parameters and electron density distribution in oxygen and fluorine atoms is discussed.
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18.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Krylov A. S., Gerasimova J. V., Vtyurin A. N., Fokina V. D., Laptash N. M., Voyt E. I.
Заглавие : A study of phase transition in (NH4)(3)WO3F3 oxyfluoride by Raman scattering
Разночтения заглавия :авие SCOPUS: A study of phase transition in (NH4)3WO 3F3 oxyfluoride by Raman scattering
Место публикации : Phys. Status Solidi B. - 2006. - Vol. 243, Is. 2. - P.435-441. - ISSN 0370-1972, DOI 10.1002/pssb.200541259
Примечания : Cited References: 11
Предметные рубрики: ELPASOLITE RB2KSCF6
Аннотация: Raman scattering spectra of perovskite-like (NH4)(3)WO3F3 oxyfluoride are studied in the 70-3600 cm(-1) frequency range and the 93-323 K temperature range including the transition point from orientationally disordered cubic phase into the lower symmetry one. Internal vibrations of ammonium ions and WO3F3 octahedra have been found to exhibit transition anomalies. Analysis of measurements suggests that the transition under study is due mainly to the ordering of octahedra.
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19.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Flerov I. N., Gorev M. V., Fokina V. D., Bovina A. F., Molokeev M. S., Pogorel'tsev E. I., Laptash N. M.
Заглавие : Heat capacity, structure, and p-T phase diagram of elpasolite (NH4)(2)KMoO3F3
Разночтения заглавия :авие SCOPUS: Heat capacity, structure, and p-T phase diagram of elpasolite (NH 4)2KMoO3F3
Место публикации : Phys. Solid State: MAIK NAUKA/INTERPERIODICA/SPRINGER, 2007. - Vol. 49, Is. 1. - P141-147. - ISSN 1063-7834, DOI 10.1134/S1063783407010234
Примечания : Cited References: 8
Предметные рубрики: TRANSITIONS
Аннотация: Thermophysical and structural studies of an (NH4)(2)KMoO3F3 crystal show that this crystal belongs to the family of elpasolites (space group Fm (3) over barm) and undergoes an order-disorder phase transition at To 241.5 K. Under hydrostatic pressure, this phase transition splits into two consecutive transitions at the tricritical point with parameters T-tr = 232.5 K and p(tr)= 0.21 GPa. It was found that anomalous hysteresis and relaxation phenomena accompany the transitions from the cubic to both distorted phases. The results are analyzed taking into account the data on the phase transition in the related elpasolite (NH4)(2)KWO3F3.
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20.

Вид документа : Статья из сборника (однотомник)
Шифр издания :
Автор(ы) : Fokina V. D., Laptash N. M., Flerov I. N.
Заглавие : Oxyfluorides with Elpasolite-Cryolite Structure as Materials of Fundamental and Practical Interests
Коллективы : "Advanced inorganic fluorides", International Siberian workshop
Место публикации : Advanced inorganic fluorides: the Third International Siberian workshop Intersibfluorine - 2008, September 01-06, 2008, Vladivostok, Russia : proceedings of ISIF-2008. - Vladivostok, 2008. - p.29-30. - ISBN 978-5-98128-036-8
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