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Труды сотрудников ИФ СО РАН

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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Usmanov O. V., Ovsianikov A. K., Zobkalo I. A., Shaykhutdinov K. A., Terentjev K. Yu., Semenov S. V.
Заглавие : Crystal field parameters and magnetic properties correlations in rare-earth orthoferrite HoFeO3
Место публикации : J. Surf. Invest. - 2022. - Vol. 16, Is. 6. - P.1041-1047. - ISSN 10274510 (ISSN), DOI 10.1134/S1027451022060258. - ISSN 18197094 (eISSN)
Примечания : Cited References: 28. - This work was supported by the Russian Foundation for Basic Research grant no. 19-52-12 047, and DFG grant no. SA 3688/1-1
Аннотация: The crystal structure and magnetic properties investigations of holmium orthoferrite compound HoFeO3 were performed in temperature range 7–300 K. Obtained XRD data confirm that HoFeO3 retains the orthorhombic perovskite structure of Pbnm space group. The crystal electric field (CEF) parameters of Ho3+ ion subsystem has been revealed numerically on the base of point charge model in the same temperature range. By this set of parameters CEF the splitting of Ho3+ energy levels was calculated and their temperature evolution was obtained. Modelling of isothermal magnetization M(H) with obtained set of parameters was carried out. Ho3+ single ion anisotropy due to CEF effects was demonstrated. Bulk magnetization evaluated from CEF was compared to experimental data.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Smirnova E. S., Alekseeva O. A., Dudka A. P., Khmelenin D. N., Frolov K. V., Lyubutina M. V., Gudim I. A., Lyubutin I. S.
Заглавие : Crystal structure and structural phase transition in bismuth-containing HoFe3(BO3)4 in the temperature range 11–500 K
Место публикации : Acta Crystallogr. B. - 2019. - Vol. 75. - P.954-968. - ISSN 20525192 (ISSN), DOI 10.1107/S2052520619010473
Примечания : Cited References: 37. - The authors are grateful to D. Yu. Chernyshov (SNBL, ESRF, Grenoble) for his assistance in obtaining the experimental data. This work was performed using the equipment of the Shared Research Center FSRC ‘Crystallography and Photonics’ RAS and was supported by the Russian Ministry of Education and Science (project RFMEFI62119X0035)This work was supported by the Ministry of Science and Higher Education within the State assignment FSRC ‘Crystallography and Photonics’ RAS and partially by the Russian Foundation for Basic Research (grant No. 17-02-00766)
Аннотация: An accurate single-crystal X-ray diffraction study of bismuth-containing HoFe3(BO3)4 between 11 and 500 K has revealed structural phase transition at Tstr = 365 K. The Bi atoms enter the composition from Bi2Mo3O12-based flux during crystal growth and significantly affect Tstr. The content of Bi was estimated by two independent methods, establishing the composition as (Ho0.96Bi0.04)Fe3(BO3)4. In the low-temperature (LT) phase below Tstr the (Ho0.96Bi0.04)Fe3(BO3)4 crystal symmetry is trigonal, of space group P3121, whereas at high temperature (HT) above 365 K the symmetry increases to space group R32. There is a sharp jump of oxygen O1 (LT) and O2 (LT) atomic displacement parameters (ADP) at Tstr. O1 and O2 ADP ellipsoids are the most elongated over 90–500 K. In space group R32 specific distances decrease steadily or do not change with decreasing temperature. In space group P3121 the distortion of the polyhedra Ho(Bi)O6, Fe1O6 and Fe2O6, B2O3 and B3O3 increases with decreasing temperature, whereas the triangles B1O3 remain almost equilateral. All BO3 triangles deviate from the ab plane with decreasing temperature. Fe–Fe distances in Fe1 chains decrease, while distances in Fe2 chains increase with decreasing temperature. The Mössbauer study confirms that the FeO6 octahedra undergo complex dynamic distortions. However, all observed distortions are rather small, and the general change in symmetry during the structural phase transition has very little influence on the local environment of iron in oxygen octahedra. The Mössbauer spectra do not distinguish two structurally different Fe1 and Fe2 positions in the LT phase. The characteristic temperatures of cation thermal vibrations were calculated using X-ray diffraction and Mössbauer data.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Petrakovsky G. A., Patrin G. S.
Заглавие : Effect of optical-excitation of impurity holmium ions on magnetic-resonance in yttrium-iron-garnet
Место публикации : Zhurnal Eksperimentalnoi Teor. Fiz.: MEZHDUNARODNAYA KNIGA, 1986. - Vol. 90, Is. 5. - P1769-1780. - ISSN 0044-4510
Примечания : Cited References: 27
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Erofeev D. A., Chukalina E. P., Popova M. N., Malkin B. Z., Bezmaternykh L. N., Gudim, I. A.
Заглавие : Holmium iron borate: high-resolution spectroscopy and crystal-field parameters
Коллективы : Congress on Spectroscopy
Место публикации : XXV Congress on Spectroscopy: E D P Sciences, 2017. - Vol. 132. - Ст.03013. - (EPJ Web of Conferences). - ISSN 2100-014X, DOI 10.1051/epjconf/201713203013
Примечания : Cited References:4
Аннотация: High-resolution transmission spectra of HoFe3(BO3)(4) single crystals were measured in broad spectral (5000-23000 cm(-1)) and temperature (1.7-300 K) ranges. Crystal-field energies of the Ho3+ ions were determined for a paramagnetic and easy-axis antiferromagnetic phases of the compound. On the basis of these data and of preliminary crystal-field calculations in the frame of the exchange-charge model, crystal-field parameters were found. A parameter of the isotropic Ho-Fe exchange interaction was estimated.Спектры пропускания высокого разрешения монокристаллов HoFe3(BO3)4 измерялись в широком спектральном диапазоне (5000-23000 см-1) при температурах от 1,7 до 300 К. Определены энергии кристаллического поля ионов Ho3+ для парамагнитной и легкоосной антиферромагнитных фаз соединения. На основе этих данных и предварительных расчетов кристаллического поля в рамках модели обменного заряда были найдены параметры кристаллического поля. Оценен параметр изотропного обменного взаимодействия Ho-Fe.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Sitnikov M. N., Kharkov A. M., Aplesnin S. S., Romanova O. B.
Заглавие : Influence of the Magnetic Field on Transprt Properties of Holmium-Manganese Sulfide
Место публикации : Sib. J. Sci. Technol. - 2020. - Vol. 21, Is. 3. - P.451-458. - ISSN 2587-6066, DOI 10.31772/2587-6066-2020-21-3-451-458; \b Сибирский журнал науки и технологий
Примечания : Cited References: 33. - The work was supported by the Siberian State University youth grant, SibGU, 2020
Аннотация: Holmium-manganese silfide with giant magnetoresistance refers to new magnetic sulfide compounds of holmium and manganese that have the effect of giant magnetoresistance (i. e., with special magnetoelectric properties), which can be used as components of sensor technology, magnetic memory, and spintronics. The technology of manufacturing polycrustals HoxMn1-xS grown by crystallization from the melt of the obtained powdered sulfides with a putity not lower then 99,9%, in glass-carbon crucibles and a quartz reactor in an argon atmosphere is presented. According to the results of x-ray diffracton analysis, HoxMn1-xS holmium-manganese sulfides have a HCC structure of the NaCl type. As the degree of cationic substitution increases, the unit cell parameter increases linearly with the concentration. No concomitant impurity phases are detected in the synthesized samples. Tj determine the state of the spin glass, mahnetic moment measurements are conducted at several frequencies ω = 1 KHz, 10 KHz and 100 kHz. The dependence of magnetic characteristics on the frequency of measurements is found. The damping of the magnetic moment and its increase with a decrease in temperature is reviled, which is connected with the formation of metastable states. Measurements of electrical resistance without a field and in a magnetic field are conducted. Anomalies in the remperature dependence of the conductivity are found. A change in the magnetoresistance sign is detected with the increase of temperature below and above room temperature.Гольмий-марганцевый сульфид с гигантским магнитосопротивлением относится к новым магнитным сульфидным соеднениям гольмия и марганца, обладающим эффектом гигантского магнитоспопротивления, то есть с особыми магнитоэлектрическими свойствами, которые могут быть использованы в качестве составляющих компонент сенсорной техники, магнитной памяти для спинтроники. Приведена технология изготовления поликристаллов HoxMn1-xS, выращенных кристаллизацией из расплава полученных порошковых сульфидов чистотой не ниже 99,9% в стеклоуглеродных тиглях и кварцевом реакторе в атмосфере аргона. Согласно результатам рентгеноструктурного анализа, гольмий-марганцевые сульфиды HoxMn1-xS имеют ГЦК структуру типа NACl. С увеличением степени катионного замещения параметр элементарной ячейки линейно увеличивается с концентрацией. Сопутствующих примесных фаз в синтезированных образцах не обнаружено. Для установления состояния спинового стекла проуедены измерения магнитного момента на нескольких частотах ω = 1, 10 и 100 KHz. Обнаружена зависимость характеристик от частоты измерений. Найдено затухание магнитного момента и его увеличение с понижением температуры, что связывается с образованием метастабильных состояний. Проведены измерения электросопротивления без поля и в магнитном поле. Найдены аномалии в температурной зависимости проводимости. Обнаружена смена знака магнитосопротивления с ростом температуры ниже и выше комнатной температуры.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Sofronova S. N., Gerasimova Y. V., Vtyurin A. N., Gudim, I. A., Shestakov N. P., Ivanenko A. A.
Заглавие : Infrared absorption spectrum of HoFe3(BO3)4 crystal
Коллективы : RFBR [13-02-00825, 13-02-98041, SS-4828.2012.2]
Место публикации : Vib. Spectrosc.: Elsevier Science, 2014. - Vol. 72. - P.20-25. - ISSN 0924-2031, DOI 10.1016/j.vibspec.2014.02.005. - ISSN 1873-3697
Примечания : Cited References: 18. - The work was partially supported by the RFBR through Grants No. 13-02-00825 and 13-02-98041, SS-4828.2012.2.
Предметные рубрики: MAGNETOELASTIC INTERACTIONS
IRON
GDFE3(BO3)4
Ключевые слова (''Своб.индексиров.''): holmium ferroborate--infrared absorption
Аннотация: Infrared (IR) absorption spectra of HoFe3(BO3)4 crystal have been obtained in spectral range 30–7000 cm−1 at temperatures from 4 to 423 K. Vibrational frequencies have been simulated with ‘Lady’ software package both for high-temperature and low-temperature phases. The experimental spectra have been analyzed on the basis of calculated data, and interpreted within the framework of internal vibrations of ionic complexes of HoFe3(BO3)4 crystal lattice. The spectral range under study was observed to have no Davydov splitting of internal vibrational modes due to unit cell multiplication. No effects of magnetic ordering on the IR spectra of the crystal under study were observed in the low-temperature range.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Pankrats A. I., Petrakovskii G. A., Kartashev A., Eremin E. V., Temerov V. L.
Заглавие : Low-temperature magnetic phase diagram of HoFe3(BO3)(4) holmium ferroborate: a magnetic and heat capacity study
Разночтения заглавия :авие SCOPUS: Low-temperature magnetic phase diagram of HoFe3(BO 3)4 holmium ferroborate: A magnetic and heat capacity study
Место публикации : J. Phys.: Condens. Matter: IOP PUBLISHING LTD, 2009. - Vol. 21, Is. 43. - Ст.436001. - ISSN 0953-8984, DOI 10.1088/0953-8984/21/43/436001
Примечания : Cited References: 20
Предметные рубрики: SINGLE-CRYSTAL
DYFE3(BO3)(4)
ND3+
Ключевые слова (''Своб.индексиров.''): antiferromagnetic state--applied magnetic fields--characteristic temperature--crystal axis--heat capacities--low temperatures--magnetic field parallel--magnetic phase diagrams--magnetic phase transitions--magnetization jump--schottky anomaly--spin reorientation transitions--thermal measurements--antiferromagnetic materials--antiferromagnetism--holmium--magnetic fields--phase diagrams--single crystals--specific heat--phase transitions
Аннотация: We present the results of the magnetic and heat capacity study of a magnetic phase diagram of a HoFe3(BO3)(4) single crystal. Two magnetic phase transitions are found in the low-temperature region. The transition from the paramagnetic to easy-plane antiferromagnetic state occurs at T-N = 37.4 K and is independent of an applied magnetic field. The sharp heat capacity peaks and magnetization jumps corresponding to the spontaneous and field-induced spin-reorientation transitions between the easy-axis and easy-plane states are observed below 4.7 K. Also, the additional heat capacity peaks, which can be attributed to the Schottky anomalies with the field-dependent characteristic temperatures, are found. According to the magnetic and thermal measurement data, the magnetic phase diagrams of HoFe3(BO3)(4) for the magnetic field parallel and perpendicular to the crystal axis are constructed.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Aleksandrovsky A. S., Krylov A. S., Malakhovskii A. V., Voronov V. N.
Заглавие : Luminescence spectra of Ho3+ in distorted parity-breaking HoF63− octahedra
Место публикации : J. Lumines.: Elsevier Science BV, 2012. - Vol. 132, No. 3. - P.690-692. - ISSN 0022-2313, DOI 10.1016/j.jlumin.2011.11.005
Примечания : The work has been supported by Ministry of Education and Science of Russian Federation (Contract 16.740.11.0150), by Russian Foundation for Basic Research (Grant no. 11-02-98002-r-sibir-a), by Grant of President of Russian Federation for support of leading scientific schools No. SS-4645.2010.2, Grant No. RNP.21.1.3455, Project 3.9.1 of PSB RAS, and Projects No. 21.1 and No. 5 of SB RAS.
Ключевые слова (''Своб.индексиров.''): distorted octahedra--holmium--luminescence--monoclinic crystals
Аннотация: Low temperature luminescence spectrum of holmium ions in monoclinic Rb2KHoF6 crystal was found to be well analyzable by the comparison with earlier studied cubic Cs2NaHoF6. The manifestation of the local symmetry influence on the strength of individual lines is found to be distinctive. In the absence of structural data, the local symmetry of holmium in Rb2KHoF6 is proved to be a non-centrosymmetric one. The concentration quenching of holmium luminescence in Rb2KHoF6 is found to be rather modest.
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Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Romanova O. B., Aplesnin S. S., Sitnikov M. N., Udod L. V., Kharkov A. M.
Заглавие : Magnetoresistance and magnetoimpedance in holmium manganese sulfides
Коллективы : Russian Foundation for Fundamental InvestigationsRussian Foundation for Basic Research (RFBR) [20-42-243002]
Место публикации : Appl. Phys. A. - 2022. - Vol. 128, Is. 2. - Ст.124. - ISSN 0947-8396, DOI 10.1007/s00339-021-05198-x. - ISSN 1432-0630(eISSN)
Примечания : Cited References: 46. - Funding was provided by Russian Foundation for Fundamental Investigations (20-42-243002)
Предметные рубрики: PHASE-SEPARATION
IMPEDANCE
Аннотация: The structure, transport characteristics, real and imaginary parts of the impedance components and electric polarization of the HoXMn1-XS (X = 0.1 and 0.2) system have been investigated in the temperature range of 80-500 K in magnetic fields of up to 12 kOe. The morphology of synthesized samples has been studied. The influence of the magnetic field on the transport characteristics, on both direct and alternating currents of holmium manganese sulfides, have been established. The negative effects of DC magnetoresistance in the region of the magnetic phase transition and positive AC magnetoimpedance up to 4% in the paramagnetic region have been established. The critical temperatures of the existence of the electric polarization have been determined. At a substitution concentration of X = 0.1, the activation character of the relaxation time versus temperature has been found. The diffusion contribution for the composition with X = 0.2 has been established by the impedance hodograph.
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10.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Ikonnikov D. A., Malakhovskii A. V., Sukhachev A. L., Temerov V. L., Krylov A. S., Bovina A. F., Aleksandrovsky A. S.
Заглавие : Spectroscopic properties of HoAl3(BO3)4 single crystal
Коллективы : Ministry of Education and Science of the Russian Federation for Siberian Federal University; Russian Foundation for Basic Research Grants [12-02-00026, 14-02-00219, 13-02-00825]; Russian President Grant [SS-2886.2014.2]; SB RAS Project [43]
Место публикации : Opt. Mater.: Elsevier Science, 2014. - Vol. 37. - P.257–261. - ISSN 0925, DOI 10.1016/j.optmat.2014.05.036. - ISSN 18731252 (eISSN)
Примечания : Cited References: 30. - The work was supported by Grant of the Ministry of Education and Science of the Russian Federation for Siberian Federal University, the Russian Foundation for Basic Research Grants 12-02-00026, 14-02-00219 and 13-02-00825, by the Russian President Grant SS-2886.2014.2, and by SB RAS Project No. 43.
Предметные рубрики: RARE-EARTH IONS
OPTICAL-PROPERTIES
Ho3+ IONS
ABSORPTION
INTENSITIES
EMISSION
GLASSES
SPECTRA
LUMINESCENCE
PARAMETERS
Ключевые слова (''Своб.индексиров.''): absorption--luminescence--holmium--huntite--judd-ofelt
Аннотация: The Judd–Ofelt theory has been applied to analyze absorption spectra of Ho3+ ion in HoAl3(BO3)4 measured in spectral range 300–700 nm at room temperature. The Judd–Ofelt spectroscopic parameters have been determined as: Ω2 = 18.87 x 10 -20 cm2, Ω4 = 17.04 x 10 -20 cm2, Ω6 = 9.21 x 10 -20 cm2. These parameters have been used to calculate radiative lifetimes and branching ratios of the luminescence manifolds. Three luminescent bands were found in the spectral range 450–700 nm ascribed to transitions from the 5F5, (5F4, 5S2) and 3K8 states to the ground state 5I8. Experimental intensities of these luminescence transitions were compared with those calculated by using Judd–Ofelt theory and the system of kinetic equations for populations of starting luminescing states. Probabilities of radiativeless transitions were evaluated from this comparison.
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11.

Вид документа : Статья из журнала
Шифр издания :
Автор(ы) : Sukhachev A. L., Malakhovskii A. V., Aleksandrovsky A. S., Gudim I. A., Temerov V. L.
Заглавие : Spectroscopic properties of HoFe3(BO3)4, NdFe3(BO3)4 and Ho0.75Nd0.25Fe3(BO3)4 single crystals
Место публикации : Opt. Mater. - 2018. - Vol. 83. - P.87-92. - ISSN 09253467 (ISSN), DOI 10.1016/j.optmat.2018.05.078
Примечания : Cited References: 39. - A.L. Sukhachev thanks for support Project of Russian Academy of Science No. 0356-2017-0030. A.V. Malakhovskii thanks Russian Foundation for Basic Researches (RFBR) Grant No. 16-02-00273. A.S. Aleksandrovsky thanks RFBR Grant No. 17-52-53031. I.A. Gudim and V.L. Temerov thank RFBR Grant No. 17-52-45091.
Ключевые слова (''Своб.индексиров.''): holmium and neodymium ferroborates--judd–ofelt parameters
Аннотация: Polarized absorption spectra of ferroborates HoFe3(BO3)4, NdFe3(BO3)4 and Ho0.75Nd0.25Fe3(BO3)4 were measured at room temperature in spectral range 4000–24500 cm−1 (400–2500 nm). The studied single crystals were grown from solution-melts. Intensities of the f-f transitions were measured and the Judd–Ofelt parameters Ωλ of Ho3+ and Nd3+ ions in the studied crystals were calculated. It was revealed that the crystals content not strongly influences the Judd–Ofelt parameters. The Ω2 parameter for Ho3+ ion is the most sensitive to the crystal content. Linear dichroism of the hypersensitive transitions appeared to be the largest one for both rare earth ions.
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